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By F. E. Bachman

There is such a great variety of opinion concerning the best method of determining phosphorus in pig iron and steel, that a list of determinations, on a uniform sample of pig iron, together with a short description of the methods used by different chemists, and a few experiments on the accuracy of some of the methods used, [nay be of interest to members of the Institute. All the results given in List A are from the same lot of drillings, thoroughly mixed, except Nos. 8 and 9, and 28 to 32 inclusive, which are from the same pig, but were taken at a later period.

Jan 1, 1882

By R. D. Groves, G. M. Potter, T. H. Jeffers

Experiments on ammonium carbonate leaching of native copper ores crushed to 1-inch size showed that in 30 days 55 percent of the copper was extracted from 0.7 percent copper conglomerate-type ore, and 85 percent was extracted from 2.1 percent copper amygdaloid-type ore. Cupric ions were not necessary to initiate leaching, and dilute solution containing only 2.2 grams per liter NH3 and 1.9 grams CO, was a suitable solvent. Copper was recovered from the leach liquor by solvent extraction and electrolysis of the strip solution. Cyclic testing of the leach-solvent extraction-electrolytic procedure is in progress on a 6-ton charge of minus 12-inch conglomerate-type ore assaying 2.2 percent copper. Oxygen is metered to the closed leach vessel as required by the leaching reaction. Initial copper dissolution was much slower than from minus 1-inch ore, but the leaching rate then markedly improved.

Jan 1, 1974

By Mark E. Smith

To allow recovery of gold values from ore which cannot be economically processed by the mill, Pinson Mining Company has developed a run-of-mine heap leaching facility. In order to estimate production scale recovery rates, reagent consumption and percolation problems, a series of pilot scale tests were performed. These tests typically consisted of 3,630 metric tons (mt) (4,000 tons) leach ore at a grade of .94 to 1.56 grams Au per metric ton (g/mt) (.03 to .05 oz. Au/ton). Test heaps were loader stacked to approximately 4.3 meters (14 feet) high. Information from these pilot scale tests was employed in the design and construction of the production scale facility. Parameters such as spray rate, leach cycle, sprinkler placement, and barren solution chemistry were determined by the pilot tests.

Jan 1, 1984

By Brij M. Moudgil, John P. Bunch

During hydraulic processing of phosphate matrix enormous amounts of phosphate slimes are produced. Significant portions of mined land are utilized to store the slimes. Some dewatering of the slimes is essential before any reclamation of the storage ponds can be undertaken. Dewatering and reclamation of slimes storage ponds pose many problems which are not encountered in reclamation of other mined areas.

Jan 1, 1977

By E. Higgins

It is the purpose of this paper to set forth the relation and function of the various organizations and institutes engaged in the promotion of safety in the iron mines of the Lake Superior region…

Jan 1, 1915

By F. F. Aplan, G. Simkovich

Zinc oxide, an n-type semiconductor, and nickel oxide, a p-type semiconductor, were studied in electrostatic separation experiments in pure and doped forms. In addition, pure potassium chloride and potassium chloride containing one volume per cent silver were also investigated. It was found, in agreement with theory, that the presence of dopants in the oxides could either increase or decrease the electrical conductivity of the base compounds and, thus, control the response of these particles to electrostatic separation. Further, it was shown that the same dopant in the n- and p-type semiconductors produced opposite conductivity effects; again in accord with theory. Finally, it was found that the presence of dispersed silver particles in the normally insulator phase potassium chloride produced sufficient electronic conductivity to cause the silver containing particles to respond as would materials possessing "medium-type" conductivities.

Jan 1, 1980

By V. R. Garfias, R. V. Whetzel

It is estimated that world consumption of petroleum, its products and related fuels during 1935 will reach an all-time peak of 1,592,000,000 bbl. —about 5.4 per cent higher than in 1934. Demand increased within the United States approximately 6.1 per cent during 1935 and in foreign countries about 4.1 per cent. The figures in Table 1 indicate that during the past five years world's production of crude petroleum and related fuels exceeded demand every year and that the aggregate difference is approximately 239,000,000 bbl. The supply in the United States exceeded consumption by some 134,000,000 bbl. over the same five-year period, while outside the United States the excess over demand is shown to be 105,000,000 bbl. Table 2 combines the excess production in the United States with its favorable balance of exports over imports, showing that the United States has reduced its storage over the five years by about 132,720,000 bbl., and indicates that, including its excess of imports from the United States, the rest of the world may have an unfavorable balance of some 371,000,000 bbl. over the five-year period. Such difference in foreign countries is largely due to increase in stocks, and partly at least remains in our imperfect knowledge of consumption statistics as an unfavorable balance. Table 3

Jan 1, 1936

By Akira Yazawa, Alžbeta Gubcova

RECENT lead-smelting techniques have tended toward use of high-grade concentrates with minimum amounts of flu, accompanied by profitable employment of roast reaction.1-5 In order to better understand these smelting processes, thermodynamical calculations have been carried out on the Pb-S-0 system, and the results obtained have been presented in isothermal reaction diagrams in which log Ps, and logPo, were the axes. The diagram thus constructed seems to be more convenient to grasp the equilibrium aspect than those published hitherto.6-8

Jan 1, 1968

By V. H. Wilhelm

Greater stabilization in the petroleum industry was effected during 1934 through stricter compliance with curtailment measures and the establishment of the Pacific Coast Petroleum Agency. Various estimates of individual, company and state reserves revealed the fact that they were inadequate to sustain the present rate of production over a lengthy period, therefore drilling operations were increased during the year both in proved and wildcat territory. This greater activity resulted in the addition to reserves at Mountain View, Mount Poso and Edison in Kern County, Santa Barbara in Santa Barbara County and Playa del Rey in Los Angeles County. Additional reserves were also established in the Long Beach and Santa Fe Springs fields, in Los Angeles County, due to operators being successful in isolating small prolific sand bodies, formerly disregarded during the flush production periods.

Jan 1, 1935

By Donald C. Violetta

LIMITATIONS of the sintering process as applied to the agglomeration of fine iron-ore concentrates are related directly to the sizes and aggregating properties of the ore particles. A normal sintering mixture is composed predominantly of material which ranges in size from 5/8 in. to 100 mesh, whereas concentrate is composed of material which ranges in size from 100 mesh to less than 10µ. Unless the concentrate has high aggregating properties, it is quite impervious to a gas stream and, as such, inhibits the capacity and operability of the conventional sintering process. Material has Poor Aggregating Properties Aggregating properties, in this case, may be defined as the ability to form small agglomerated fragments or accreated masses by a normal mixing action, and the ability to maintain these shapes during drying and firing. Coarse-screened ores are a natural aggregate, and fine, slimey ores have good aggregating properties. However, specular-hematite flotation concentrate has a very low tendency to aggregate, due to its particle sizes, shapes, and surface chemistry and, as such, is readily air borne in a gas stream when dry.

Jan 3, 1958

By E. V. Manlapig, David J. Spottiswood

In recent years great advances in the automatic control of flotation plants have been made, mainly due to the development of reliable sensing instruments to monitor process performance and the development of an adequate understanding of system responses to process disturbances. Some of the control strategies used in flotation plants which apply computer control are presented here. These schemes, which involve the control of collector; depressant, frother, and air and pulp level, are analyzed with respect to their control objectives, control variables, and the instrumentation involved. The knowledge gained in understanding these strategies may be applied in the dew and implementation of control system in other concentrators.

Jan 1, 1981

By Archibald Blue

JUST one hundred years ago, in a paper read before the Royal Society of London and published in its Transactions, Rt. Hon. Charles Greville established and named the mineral species, corundum, the crystalline oxide of aluminum; and we have it on the authority of Professor Judd that in an appendix to Greville's paper the Count de Bournon correctly defined the crystallographic characters of the species. The names of its

Jan 1, 1899

By Edwin H. Olson, Morton Smutz, Charles J. Baroch

IN 1949 an orebody containing some 10 billion lb of recoverable rare earth metals was discovered in the Mountain Pass district of San Bernardino County, California.1 The following year Molybdenum Corp. of America purchased a number of claims at the deposit and a mill on the property which had been constructed to process the district's gold ores. Average composition of ore from the San Bernardino deposit is less than 0.1 pct ThO2, 25 to 35 pet calcite, 10 pet rare earth oxides, 15 to 20 pet silica, and 30 to 40 pet barite.2 Rare earth content of the ore analyzes 50.7 pet CeO2, 4.2 pet Pr6O11, 11.7 pet Nd2O3, 1.3 pet Sm2O3, and 34.3 pet La2O3, and others.2

Jan 3, 1959

By Dirk van Zyl

The paper describes the construction of a clay pad in Southern California. The pad consisted of a mixture of in situ soil and imported clay products. The paper summarizes design considerations. Laboratory permeability tests performed on samples removed from the pad formed part of the quality control requirement of the State of California Water Quality Control Board. The paper presents statistical analysis of the data (about 70 permeability tests in total) and their significance in controlling seepage losses. The results obtained from an investigation of the first pad-area after completion of the leach cycle are presented and discussed. Results from visual observations and laboratory tests are presented.

Jan 1, 1984

By B. C. Mariacher, I. Hoffman

In 1952, beneficiated phosphate ore first began to move from the Oron plant of Negev Phosphates Ltd. in the Negev Desert to the super-phosphate plant at Haifa, Israel. Since that time this company has continually sought to overcome its natural handicaps affecting the operating efficiency and quality of the product in an effort to bolster the agricultural program of Israel and the development of an exportable commodity. The most serious deterrent to the development of a beneficiation process was the total absence of water. The Oron plant lies approximately 30 miles south of the irrigated regions of Israel with the nearest producing water well located about 10 miles to the northwest. The urgency of early phosphate production made it necessary to consider only dry processes in the initial operation. Fortunately, the ore was amenable to a dry process which yielded a usable concentrate assaying about 28.5 pct P2O5; but phosphate recovery was low. A description of the characteristics of the Negev ore should help to clarify the principles upon which the dry concentration is based.

Jan 5, 1961

Jan 1, 1925

By Werner Langguth

SINCE the introduction of the improved method of precipitating gold from chlorine solution by SO2 and H2S at the Golden Reward chlorination-works, Deadwood, S. D.,* this modern method has been further adopted in the chlorination-works of the Portland Consolidated Company at Deadwood, and in those of the Black Hills Milling and Smelting Company at Rapid City, S. D. It has proved practically most successful in the handling of large quantities of gold solution, and constitutes up to date, with Mr. John E. Rothwell's most important improvement, namely, barrel-leaching under hydraulic pressure, the principal progress made in gold chlorination. The method of refining the gold sulphides which result from this method of precipitation, was introduced by me in 1890 at the Golden Reward works, and in 1892 at those of the Black Hills Company. It has not suffered any changes during the last three years, and is substantially as described below:

Jan 1, 1895

By H. H. Wade, N. F. Schulz

The large quantities of iron-bearing materials, including taconite, semi-taconite," and other low-grade ferruginous materials occurring in Minnesota and elsewhere, constitute an important potential source of iron. Satisfactory grade and recovery of iron ore concentrate cannot ordinarily be obtained from these ferruginous materials by simple methods of beneficiation. Iron is distinctive in that the free metal and two of its oxides [magnetite (Fe,O,) and maghemite (gamma-Fe,O,) ] are strongly ferromagnetic. The successful magnetic separation of natural magnetite from taconite has already been established on a commercial scale. The iron in semi-taconite, how- ever, occurs largely as goethite (Fe,Os.H,O) and hematite (Fe90,) which do not respond to ordinary magnetic separation methods. Magnetic roasting converts these iron oxides to magnetite, which can, after liberation, be magnetically concentrated.

Jan 11, 1960

By Edward Halse

Normal banded structure,* exhibiting bands or layers of mineral symmetrically arranged from the sides to the center of the vein, appears to be by no means common in the Republic of Mexico. When the bands of quartz form interlocking crystals in the center (" comb-structure "), the evidence that the filling has taken place in an open space is complete. This also applies in the case of any mineral the fibers of which are perpendicular to the walls, and which presents here and there, in a central line, cavities or vugs lined with crystals (geodes); but it does not follow that the whole width of the banded vein represents that of the original open fissure. The opening and filling may have been slow and gradual processes, advancing

Jan 1, 1902

By D. M. Hausen

This study identifies and describes various crystalline phases of the V205-Na20 system, and relates their properties to metallurgical aspects of vanadium production. Phase equilibria and stability ranges of sodium vanadate phases of varying molar ratios of Na20/V205 were investigated in a variety of plant products, ranging from fused "black cakes" (V20 melts) to "salt roast" calcines. Crystalline compounds, Including vanadium pentoxide, V205; sodium vanadyl vanadate, 6 phase, Na2O.V2O5.5V2O5; sodium vanadyl vanadate, y phase, 5Na20.V204.12V205; sodium metavanadate, Na20 .V 05; sodium pyrovanadate , 2Na20 .V205; and sodium orthovanadate, 4Na20.~2~5, have been characterized with the aid of X-ray diffraction patterns, infrared spectra, and optical properties in addition to chemical analyses, as a guide to mineralogical "troubleshooting" of plant problems and processes in vanadium pyro- and hydrometallurgy.

Jan 1, 1984