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By Wesley T. Holmes

This report describes the first phase of an investigation aimed at obtaining a wider knowledge of the problems involved in smelting titaniferous magnetites. Liquidus temperature measurements were made on selected slag compositions in the titania-alumina-silica-calcia-magnesia system. Both the melting-holding-quenching method and the hot-stage microscope method were used in the tests. Liquidus temperatures of slags studied ranged from 1,217° to 1,667° C. The lowest liquidus temperature of the slags occurred when the difference between CaO plus MgO and Si02 was less than 12 weight-percent. Liquidus temperatures were also lowered when Si02 was substituted for Ti02 plus Al2O3 when CaO and MgO levels were held constant. Improved methods for the measurement of liquidus temperatures on very small samples are described.

Jan 1, 1968

By E. C. Tarpley

An acid-extraction procedure developed in Germany for determining mineral matter in coal was investigated by the Bureau of Mines to determine its application to American coals. It was found to be suitable for all ranks of coal from anthracite to lignite if modified slightly for coals containing considerable quantities of calcium compounds, such as calcite or calcium humate. The precision of the method is satisfactory, and the results are probably closer to the true content of mineral matter than those obtained by empirical formulas. The method requires considerably more analytical data than the Parr or approximation formulas but is no more time consuming than obtaining the necessary data for the King, Maries, and Crossley formula (theoretically the most comprehensive empirical formula used). An appendix to this report includes a detailed description of a recommended procedure.

Jan 1, 1959

By W. M. Deaton

[The formation of gas hydrates in natural-gas pipe lines depends on temperature and pressure conditions in the lines as well as on the presence of condensed water. The operating pressure in a pipe line may be determined easily and usually is available from the records of operation, but the temperature seldom is known. In cooperation with the American Gas Association, the Bureau of Mines, in its investigation of gas hydrates, conducted a pipe-line-temperature survey and studied underground temperatures at depths at which pipe lines ordinarily are buried and the relationship of these temperatures to prevailing atmospheric conditions. A similar but more limited study of this type was, conducted by engineers of the Bureau of Mines a number of years ago.4/A summary of the earlier findings was included in a general report by the Bureau on the flow of natural gas through high-pressure transmission lines.5/ In the present study, data on temperature variations were obtained at several places widely separated geographically. This information should assist pipe-line engineers in designing and operating natural-gas pipe lines. In the pipe-line-temperature survey here resorted, a study was made along a 22-inch natural-gas pipe line: originating near Amarillo, Tex., and extending northwestward through New Mexico into Colorado (fig. 1). Some data also were collected along a 16-inch line extending southward from Amarillo. In the study of underground temperatures and their variation with atmospheric temperature, recording; equipment was installed at the]

Jan 1, 1941

By John R. Rhodes

The objective of this project was to investigate the feasibility of analytical techniques potentially capable of determination of Mg, Al, Si, S, Ca and Fe in 1 to 2 mg samples of respirable coal mine dust, in a total analysis time of not more than 10 minutes per sample, using equipment capable of being truck mounted for field-laboratory operation. It was not essential that the technique be non-destructive, but the chosen technique is, and this enables the analysis to be performed directly on the 37 mm diameter membrane filter on which the respirable dust sample is normally collected. The sensitivity requirements are therefore quoted in terms of the units of measurement, µg/cm2. The detection limit (3o of the background criterion) should be 0.5 µg/cm2 or less. The precision should be 5% or better, at concentrations above which the detection limit is not the determining factor.

Jan 1, 1972

By G. W. Jones

Fires in anthracite refuse banks are troublesome and may become exceedingly costly to combat. Instances are known in which refuse-bank fires have grown to such magnitude that entire mining properties have been endangered. In one instance4/ a refuse-bank fire cost the mine management several hundred thousand dollars to extinguish. The exact number of fires formerly existing or now active in the anthracite region of Pennsylvania is not known. There are hundreds of anthracite refuse banks in this region, some very high and large in area, that have never caught firs, although a few are over 50 years old. This would indicate that spontaneous ignition of the material in these banks is improbable, a conclusion confirmed by recent laboratory research.

Jan 1, 1939

By John C. Machisak

This publication, for the calendar year 1959, contains statistical data on injuries and employment pertinent to metal mines, ore-dressing plants, and primary nonferrous smelters, refineries, and reduction plants. The Bureau of Mines is authorized to request data on injuries and employment in the metal-mining industry, and the information, voluntarily submitted by the operators, contributes immeasurably to the promotion of safety in the metal-mining industry. Every effort has been made to make the annual canvass as complete as possible. The data presented are classified according to the hind of ore mined and includes information on copper, iron, lead-zinc, gold-silver lode, placer, uranium- vanadium, and miscellaneous metals. A breakdown of miscellaneous metals by commodity is shown in tables 17 and 18.

Jan 1, 1963

By G. W. Jones

Fires in anthracite refuse banks are troublesome and may become exceedingly costly to combat. Instances are known in which refuse-bank fires have grown to such magnitude that entire mining properties have been endangered. In one instance4/ a refuse-bank fire cost the mine management several hundred thousand dollars to extinguish. The exact number of fires formerly existing or now active in the anthracite region of Pennsylvania is not known, There are hundreds of anthracite refuse banks in this region, some very high and large in area, that have never caught fire, although a few are over 50 years old. This would indicate that spontaneous ignition of the material in these banks is improbable, a conclusion confirmed by recent laboratory research.

Jan 1, 1939

By John C. Machisak

This publication, for the calendar year 1959, contains statistical data on injuries and employment pertinent to metal mines, ore-dressing plants, and primary nonferrous smelters, refineries, and reduction plants. The Bureau of ,Mines is authorized to request data on injuries and employment in the metal-mining industry, and the information, voluntarily submitted by the operators, contributes immeasurably to the promotion of safety in the metal- mining industry. Every effort has been made to make the annual canvass as complete as possible. The data presented are classified according to the hind of ore mined and includes information on copper, iron, lead-zinc, gold-silver lode, placer, uranium- vanadium, and miscellaneous metals. A breakdown of miscellaneous metals by commodity is shown in tables 17 and 18.

Jan 1, 1963

By J. R. Nettle

The purpose of these studies by the Federal Bureau of Mines was to determine the feasibility of refining low-grade hafnium by an inert-gas-shielded molten-salt electrorefining technique to produce a hafnium metal meeting reactor specifications. The techniques were adapted from those used success-fully for titanium electrorefining. Three electrolytes containing hafnium chlorides were developed from which deposits having a Brinell hardness of 170 or below were recovered. A KC1 + NaC1 + HfC14 electrolyte produced deposits in the hardness range of 140 to 165 Brinell. Deposits with a hardness range of from 132 to 152 Brinell were pro-duced from an electrolyte composed of KC1 + LiC1 + HfC14. A third electrolyte composed of NaC1 + K3HfC17 produced deposits with a hardness as low as 139 Brinell. In a fourth electrolyte, composed of NaC1 + K2HfF6, a measure of refining was accomplished, but under the test conditions no metal meeting specifications was recovered; none was softer than 174 Brinell. A number of metallic impurities were reduced in quantity by the electro-refining process, notably iron, which normally was reduced from 250 p.p.m. to less than 50 p.p.m. Magnesium generally was reduced from 680 p.p.m. to less than 80 p.p.m. Manganese content was also reduced by the electrorefining process. Sponge containing 90 p.p.m. Mn yielded deposits containing a maximum of 50 p.p.m.; some deposits contained only 10 p.p.m.

Jan 1, 1961

By Gloyd M. Wiles

The property of the Park City Consolidated Mines Co. is situated in the northeast part of the Park City dining district 1 mile east of the town of Park City. The elevation at the collar of No. 1 shaft is 7,250 feet. Park City is a town of approximately 4,500 population lying about 30 miles east of Salt Lake City. The two are connected by an oiled State Highway, which is cleared of snow in winter and maintained in first-class con¬dition by the State throughout the year. The district is served by branches of the Denver & Rio Grande Western and Union Pacific Railroads, each operating on a daily' schedule, except Sunday. These two railroads have constructed 1 ½ miles of joint track from the town to the Park City Consolidated Mines Co. loading tipple, located 200 feet from the portal of the adit that leads to No. 1 shaft.

Jan 1, 1936

By Harry Dobroski

Communications with moving tracked vehicles in a rail haulage mine pose a difficult problem. These communications take place from dispatcher to vehicles or from vehicle to vehicle via the trolley line, which is a very poor communications line. As a result, deadspots and high-signal areas can occur anywhere along the line, or signal can decrease simply as a function of distance. An analysis is made of the trolley line as a communications line, and methods of improving its characteristics are discussed. Data from inmine experiments are presented, showing actual improvements in communications. Recent Bureau developments in new hardware are also discussed. These include an adaptive speaker control for existing carrier phones and a new generation of improved carrier phones.

By Robert R. Perron

The U.S. Bureau of Mines is engaged in many diverse programs fur improving mine safety. One area of interest to the Bureau is new and improved means for minimizing the hazards of accidental gas ignition or electrical shock should the frame of an off-track machine assume potential above ground. Various means presently used to prevent such occurences are the use of ground fault detectors for phase to ground faults in ac machines, and grounding conductors and diodes in dc machines. In a three phase ac power center, a phase to ground fault may be detected by monitoring the current in the grounding resistor which is required between the power center neutral on the load side of the power center transformer and ground. Another method for detecting a ground fault is to pass the three load conductors through a toroidal core transformer. The phase currents vectorially add up to zero if none of the phases are faulted, and hence the voltage of the transformer secondary is either zero or not zero if one of the phases is unbalanced or faulted.

Jan 1, 1976

By K. E. Tame

Pollution from radioactive nuclides, principally Ra226, in liquid waste from uranium mills can be minimized by reusing the waste solution within the mill. Such reuse of waste solution in the Vitro Chemical Co.-type process was investigated in the laboratory. Vitro employs an acid leaching process for dissolution of the uranium, countercurrent decantation for liquid-solid separation and washing, and amine solvent extraction for recovery of the uranium from solution. The simulated reuse of barren raffinate in the mill circuit was carried through two separate laboratory campaigns of 29 and 31 cycles. Conventional chloride stripping of the amine was employed in the first campaign, whereas nitrate stripping was used in the second campaign. Dissolution of uranium from the are in the acid leaching circuit averaged 96 percent. Washing efficiencies of 98 to 99 percent were attained by using 4 volume tons of combined raffinate and makeup water per ton of ore. Uranium recovery from the pregnant solution using a 5-percent solution of amine LA-1 in kerosine ranged from 99.3 to 99.9 percent.

Jan 1, 1962

By S. J. Broderick

[Xuge d-mp heap co:lt:.ini9: tilcu?:na3s of tons of cad ~eP~se 2r3 a failiar sight in coal-mininc regior@:. T5ey reprecei~t considergole economic 1083, are very l.u.,si~hC,ly, ?:ld t?ke un m-lch vaL-x3le qace. Cor.sequentl;r thelr remcval i~ geatlyr dezir36, ax2 my ret-sn t?-at c,m be obtained would be er;pecic.llj .a~elconre&apos; t.7 the cod ir.S..r; kry. T?.e vaste rk.t~ri..tl conpl-ises large pieces of slr.t.e, hi~h-2s&apos;. bore c~al., luqs cf cle:., ,ad finer refuse conin,= fro3 the vrtskery, Tilt 1:zshcr:r refilsn contnins sone yood coal. Rig coal and the &apos;better p~lcs of bore ere the zat~rla2.s ~15:;~itiered in this in- vest ig:?.tion. 7% Il~avter frnctions of the w~~sherjr ref;lw aizd tts large 2ieces of slcte ?,".:I rgck contilin 1it:lei ccai-i-bcna.c~o~s caterial ad are vir- tu<dly worthiess nc, rz:. ::atcrin!. for .*=irin,= zct,iv?*teb cCvb~n. 13 the 3irniingh.m district, i13br.12, a-c.ju",P p?rcccn",f the c3sl r?.ir?ed is washed, ,md in tkis c?i.;trict nlz:~c rcfilce ecc;:?:lletcs ~t the r%tg of 1 to 2 million .! tons 2 yew.]

Jan 1, 1941

The principle activities of the Explosives Research Laboratory from July 1, 1961 to June 30, 1962, are described briefly in part 1. Part 2 gives short abstracts of publications that appeared during fiscal year 1962; in general, the research reported in these publications antedates the report period. Part 3 gives the results of an investigation which, although too limited to warrant separate publication, merits presentation in some detail because of current interest in ammonium nitrate-fuel oil compositions.

Jan 1, 1964

By Alvin Kaufman

To aid industry and Government in planning water developments the Bureau of Mines in 1963 canvassed mineral producers to determine water use in 1962. Water use by the mineral industry comprises only 2 percent of the water withdrawn by industry as a whole. The major water-using mineral industries are natural gas processing, phosphate rock, sand and gravel, and iron ore. Analysis indicated the following conclusions: 1. Total water use and new water intake is dependent on the quantity of material processed and the process water requirements of the particular industry or commodity. 2. Recirculation is dependent on the processing requirements of a particular commodity, the manner in which the water is used, cooling and condensing requirements in certain large industries, the quality of new water intake, and the need to treat new and discharged water. 3. Consumed water is dependent on the quantity of water recirculated, the temperature and humidity in the area, and the proportion of water used for cooling and condensing. 4. A threefold increase in water use by the mineral industry by 1985 is forecast

Jan 1, 1966

By S. J. Broderick

[Huge camp heaps coat. in-.n,- ta._ur nd o tons of coal :&apos;efuse are a familiar sight in coa).--:1&apos;_ni`l ; res io The;;&apos; repre£e: t considerable economic loss, are very ~JZ&apos;:Si~i,tly, and tr:_ e u.: mach v lua-ble :price. Consequentl;;* their remcva7. is ,-,reatl:r de sir^~t~ a_." ar return that c,-u? be obtained would. be especially rel.co c to the coal T,-e "a_ste nat(~ria1 commrioes large pieces of bore cca1., lumps rf c12;&apos;, -)nd finer refuc3 coming from the &apos;acxcor~-, Tnc e&apos;-:s: rr;I refuso contains some Food coal. Th1S coal and the better crams of _,)ore Pre t&apos;--:e na.torials considered. in ohis in¬vestigotion. T&apos;.-.r, heavier fractions of the vas ier,,refuse a rd. the large pieces of slate a n i roc _r contain little carbcnacaous r..aterinl -.nd axe ~vir¬ tually worthless ra&apos;., :,atcria1. for activated carbon. In the E i 1i 11?&apos;ar 1 dictrict~ n1ab a :1 ut irfl percent of the&apos; coal mined is wa^,hed., and in district rc_a e -c-cnuatcs at the r..-ate of I to 2 Million tons a year?]

Jan 1, 1941

By David J. Kusler

This Bureau of Mines study is an appraisal of the demand for platinum, should this strategic metal be used as a. catalyst in the National abatement of automobile exhaust pollution. The Clean Air Act 0f 1970, as amended, requires that automobiles produced in 1975 and thereafter be provided with antipollutive measures to control automotive exhaust emissions. The study considers the need for automobile pollution control, the methodology for such control, the annual primary (new) platinum demand for automobiles produced from 1975 to 1990, primary platinum availability, and supply-demand forecasts and outlook. The correlative demand for platinum for the production of the required unleaded gasoline is also considered. Methodology for the study included a forecast of new automobile production from 1975 to 1990, development of automobile survival and retirement data, estimates of new platinum demand under various conditions of salvage, and data on recycling the precious metal from the catalytic converters of scrapped vehicles and existing vehicles when their spent converters are exchanged for replacement units. The new platinum demand for automobile exhaust converters, based on a converter service life of 50,000 miles, is estimated to be 1.41 million troy ounces initially in 1975, rising to 1.68 million in 1980, and declining curvi-linearly to 0.94 million in 1990. The platinum demand for converter longevities other than 50,000 miles can be derived from the tabular data presented. An appendix to the report presents a comparison between longevities of 50,000 miles and 25,000 miles. The petroleum industry&apos;s demand for new platinum for the production of lead-free gasolines could total as high as 1 million troy ounces between 1972 and 1981, just for expansion of isomerization and reforming capacity, and is in addition to normal operating demand for this metal.

Jan 1, 1972

By Louis Schaffer

The purposes of the research were to assess the applicability of new accident investigation methods to mining accidents, and to adapt those found to be applicable in the development of a new methodology for use in mining. The development included field testing, evaluation and modification of the new methodology. The report is in two volumes. Volume one discusses the background research, the design of a methodology for field evaluation, preliminary field tests in Utah mines, and work done to prepare for a formal, complete evaluation by federal government mine safety officials. This, volume 2, discusses the field evaluation done by the contractor and cooperating mines after the program was re-directed by the Bureau of Mines. It relates to research done during a period of approximately eighteen months, ending in April, 1983.

Jan 1, 1986

By Albert L. Toenges

A phase in strip mining of bituminous coal is the overturning of the surface of the land. The purpose of this report is to acquaint the operators and others interested in stripping with the work that has been done in certain States to reclaim the surface of land from which the coal has been removed by this method of raining. The preparation of this manuscript follows an extensive study of the subject in the field in the course of which a large number of strip mines were visited. ACKNOWLEDGMENT The information used in the report was obtained through the courtesy and cooperation of the operators of the mines visited, State officials and educational institutions, and others interested in the subject.

Jan 1, 1939