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By Luis Bergh, Juan Yianatos, Luis Vinnett

"Process automation as an engineering discipline is more than control systems since it includes industrial instrumentation, such as sensors, transmitters and actuators, as well as control and supervision systems, collection and transmission of data and real-time software applications to supervise and control the operation of plants or industrial processes. In the last several decades, accelerated technological development has provided a variety of software and hardware tools to aid development, maintenance and continuous improvement of automated systems. These developments however seldom reach their full potential in real plants. There are many factors to be considered, among them human capital specific training and the organization model. In this paper, a methodology for training engineers in advanced control and supervision of flotation plants is presented based on study of the application of these technologies in hybrid pilot plants. Since experimentation in real plants may present undesirable risks and costs, and simulation studies are usually limited to some unrealistic conditions, a laboratory where on-line measurements of the hydrodynamic behaviour of a pilot plant is mixed with phenomenological models has been created. In this form, an environment as close as possible to a real plant can be recreated. A flotation column and a circuit of three pneumatic cells are fully instrumented and connected to a PLC and PC network. In the control room, students learn applications of classical PID control in a DCS environment, advanced predictive control, on-line process operation diagnosis, fault analysis, virtual sensors and expert-fuzzy systems. Several undergraduate and graduate courses and theses are supported by this Process Control Laboratory infrastructure. Examples of these applications are discussed."

Jan 1, 2014

By C. Y. Sun

China is a country with abundant resources of tungsten, taking one of the world?s top-positions regarding both the total reserve and the amount of industrial production. China?s tungsten resources occur mostly in multi-metallic deposits rather than in single-metallic deposits. China?s multi-metallic tungsten ores have the characteristics of coexistence with other valuable components such as molybdenum, bismuth, copper, sulfur and fluorite. These ores are usually low in grade and difficult to process. The technological challenge in mineral processing lies in separation of multi-metallic components in these complex ores and a comprehensive utilization of natural resource. Several cases of industrial practice of processing China?s typical multi-metallic tungsten ores are presented.

Jan 1, 2014

By S. S. Lu

In sodium oleate and salicylhydroxamic acid systems, sequence of floatability of three sulfate minerals is: barite>celestite>gypsum, in lauryl amine system is: gypsum>celestite>barite. XPS and infrared spectrum analysis are used to find that it is chemical reaction between sodium oleate and three minerals, physical adsorption on the surface of minerals for lauryl amine, and it is chelating reaction between salicylhydroxamic acid and three minerals possibly. Theoretical calculation on chemical bonds in crystal structures of three minerals is carried out, finding that breaking degree of Mn+?O2- in crystal structures of three sulfate minerals is closed related with floatability.

Jan 1, 2014

By F. Boylu

In this study, Ca-bentonite was subjected to a series of systematic hydrocyclone tests with the aim of developing separation procedures and in turn achieving optimum recoveries. In hydrocyclone tests, vortex and apex diameters and also feed pressures were investigated. In each hydrocyclone set, vortex diameter was kept constant while the other two parameters varied to produce bentonites con-centrates of various smectite contents. The separation efficiencies were evaluated based on the cation exchange capacity (CEC), particle size and swelling index. The detailed hydrocyclone tests showed that, upgrading of Ca-bentonites require procedures different from the bentonites reported in the literature. Sodium and mixed bentonites are easy- to-disperse and easy-to-separate whereas calcium types need to be scrubbed rigorously for disintegration. Scrubbing properties of ca-bentonite were investigated as a function of scrubbing time and percent solids by weight (PS). The scrubbing conditions at 700 rpm for 1.5 hours and percent solids of 30 % were found more effective for achieving a better quality bentonite. In addition to the parameters mentioned above, the effect of percent solids on hydrocyclone separation was also studied. Although Ca-bentonites permit studying at higher percent solids, increasing solids content of the pulp deteriorated the quality of the clean products. Application of an appropriate separation scheme enabled the development of a unique separation procedure involving stage wise scrubbing followed by hydrocycloning which yielded calcium bentonite concentrates with CEC of 90 meq/100 g and high swelling indexes of 12 mL from the original bentonite of 65 meq/100 g and 7.0 mL, respectively. These results indicate that upgraded bentonite products can be conveniently used in various diverse industrial applications including bleaching earth, desiccant, cat litter, paper etc.

Jan 1, 2014

By Christian O’Keefe, Alex Van der Spek

"Evaluation of inequalities of the partial sums defining cumulative grade and recovery prove that cumulative grade has an upper bound not dependent on the bank number and cumulative recovery possesses an upper bound proportional to the bank number. This explains one observed characteristic of cumulative grade versus cumulative recovery curves. The existence of such maxima combined with the observed shape of cumulative grade-recovery curves leads us to postulate that these curves can be well described by rectangular hyperbolae. Rectangular hyperbolae are characterized by asymptotes at right angles to each other. It is proven that this property can be used to derive an equation for the cumulative mass flow of the concentrate in terms of the asymptotic values of cumulative grade and cumulative recovery. Fitting hyperbolae to experimental cumulative grade cumulative recovery plant data then results in estimates of the maximum grade, the maximum recovery and a constant which may be taken as a performance coefficient of a row. Normalization of the cumulative grade and the cumulative recovery by their respective maxima gives rise to a graphical representation that can be used to evaluate the operating performance of a row of floatation bank cells. The normalization procedure removes the bias that is introduced by inevitable variation in mass flow of the feed and variation in feed mineralogy or feed particle size distribution. Reduction of the normalized data collapses all cumulative grade-recovery data onto one and the same curve. This removes the differences caused by the variation in row performance. The reduced cumulative grade-recovery data scatters around a common hyperbola. This can be used to gauge the validity of the assumptions made. Normalized cumulative mass pull is determined from the fitted values of the maximum recovery and maximum grade. This may serve as an alternative performance indicator of the floatation row."

Jan 1, 2014

By Z. H. Liu

We experimented with slurry which from one of coal preparation plant in Guizhou province and made researches on double hump gradation, one of critical factor of gradation technology, which can influence pulping character in the process of making coal water mixture (CWM). The purpose for it is to find the best particle gradation which can meet the requirements in concentration, viscosity, and stability for CWM. The final result is that the concentration, viscosity, stability of CWM can meet the requirement for industrial use while the rate of fine particle in the slurry is 70%~75% and the maximum concentration of 62%.

Jan 1, 2014

By Dezhou Wei, Cong Han, Shuling Gao, Wengang Liu, Yanbai Shen

The recycling schemes of copper mineral to a copper raw ore produced in China is investigated in this paper, of which is aimed at copper concentrate‘s grade is over 26.00% and recovery is over 90.00%. The primary copper mineral the raw ore is chalcopyrite and the main gangue minerals are quartz, orthoclase, albite, clinochlore and phlogopite. There are four useful metal elements contained in the copper raw ore, which are Cu, Pb, Zn, Au and Ag, and the grade of each is 3.75%, 0.01%, 0.11%, 0.31 and 483.5 g/t. Two floating recycling schemes and its corresponding flotation reagent system were determined. The results show that calcium oxide, sodium carbonate and sodium sulphide were used as regulators, sodium n-butylxanthate was used as collector and terpenic oil was used as frother in two floating recycling schemes are effective. The open-circuit test’s results show that the copper mineral contained in raw ore can be effective collected, and both concentrates gotten through two schemes are up to grade.

Jan 1, 2014

By M. J. Lottering

Gold deposits in South Africa are invariably associated with uranium bearing minerals. Although it is low grade uranium by international standards, averaging around 0.3 kg U3O8 per ton of ore, recovery of uranium as a by-product improves the overall economics of gold extraction. Moreover, the current high uranium prices as well as increased demand due to renewed interest in nuclear power provide significant incentives for dedicated uranium production. An understanding of the uranium leaching response to changes in operating conditions is an important first step to-wards optimisation of uranium recoveries. In South African acid leaching plants, uranium dissolutions higher than 90% are difficult to achieve, and the chemical origin of this limit is not clear. To study leaching behaviour, an important consideration is the mineralogical characteristics of the ores. Typically, a diagnostic leaching approach can be followed. In this paper, a mineralogy-leachability explanation is presented to rationalise the difficulty in exceeding 90% dissolution from low grade uranium ores on the basis of a simple diagnostic leaching method. It was found that brannerite was the main reason for the existence of a dissolution limit in Witwatersrand ore and that chemical liberation was more effective to increase end dissolution compared to physical liberation. The findings from these investigations will form guidelines for developing economically viable flow sheets for improved uranium recovery, at least in a South African (Witwatersrand) context.

Jan 1, 2014

By J. A. Marts, R. C. Gilmore, S. Saki, J. F. Brune

El modelamiento de la dinámica de fluidos computacional (CFD por sus siglas en inglés) implica la creación de un dominio de cálculo llamado malla o rejilla para resolver las ecuaciones que definen la física del flujo de fluidos. Este proceso comprende a menudo emplear la mayor parte del tiempo en esfuerzos de modelamiento. En un proyecto patrocinado por el Instituto Nacional de Seguridad y Salud Ocupacional (NIOSH), los investigadores de la Escuela de Minas de Colorado utilizaron un enfoque innovador de mallas, el cual permite una fácil adaptación del modelo CFD para adaptarse a una variedad de geometrías de minado de tajos largos ventilados por canales (bleeders) y progresivamente sellados (referidos a menudo como bleederless en los Estados Unidos), con la porosidad y la permeabilidad de la cámara escalables en un amplio intervalo. En este trabajo se presenta la metodología del enfoque de enmallado y escalado junto con las recomendaciones para el uso de modelos CFD en aplicaciones de ventilación para las cámaras en tajos largos. La nueva técnica de enmallado se utilizó para evaluar la función de un retorno hacia atrás en una cámara progresivamente sellada y otra cámara ventilada por canales.

Jan 1, 2014

By David Leidel

A revolution in hydrocarbon well completions within the last thirty years has enabled drillers to tap the resources of known gas plays in an economically viable manner and deliver to market natural gas supplies for industrial, transportation and domestic use without the importation of liquefied natural gas from verseas. An added benefit has been the convenient location of one of these gas plays, the Marcellus Shale, in the Northeastern states strategically close to a major natural gas market, namely the cities and towns of the New England and Mid-Atlantic states. As a sidelight, the development of the tight gas reservoirs and their subsequent production has created thousands of jobs in an otherwise lackluster economy.

Jan 1, 2014

By Ruilin Yan, Kameron Ray

This paper reports a simple approach to model the waveform change due to travel distances based on the field measurement. A linear interpolation is used to estimate the waveform at a distance from two vibration waveforms recorded at two different distances. The resulted waveforms are compared with actual recorded waveforms at the point in both time and frequency domains. It shows that the proposed method to estimate the waveform change yield reliable results. The advantages of the proposed method are that it does not require assumptions that a transfer function does and that it is based on purely the measured waveforms that are encoded with in-situ rock properties. The method could be more reliable for far field seismic waveforms and could be an approximation for near field waveform estimation.

Jan 1, 2014

By G. Frithum

In the present paper a new and highly economic route for Fe-separation from HCl leaching processes in hydrometallurgical applications is described. In most ore leaching processes, Fe is involved and needs to be separated; HCl has become an interesting leaching agent, because it can be recycled. Usually a mix of Fe2+ and Fe3+ is obtained which can be hydrolyzed directly (in case only Fe3+) or roasted via pyrohydrolysis (in case of Fe2+) to ferric oxide. Economic oxidation of Fe2+ to Fe3+ is described, and potential technologies for regeneration of HCl with separation of Fe are shown and compared.

Jan 1, 2014

By Yang Xiao, Zhang Yimin, Bao Shenxu, Liu Chun

Stone coal is a unique vanadium-bearing resource in China. Many techniques, such as salt roasting-water leaching, blank roasting-acid leaching, direct acid leaching etc. have been developed for vanadium extraction from stone coal. The vanadium leaching rate can reach 74.9% for stone coal from Jiangxi, but only about 27% of vanadium is leached for Hubei ore by applying salt roasting-water leaching technique. This paper investigats the vanadium occurrence in stone coal by microscope observation and electron probe, and compares the minerals components of stone coal from Jiangxi and Hubei. Although most vanadium exist as an isomorphism by replacing Al(III) from dioctahedral structure in mica group minerals in stone coal from two regions, the free vanadium is remarkably abundant in Jiangxi stone coal than in Hubei stone coal, which results the fact that vandium is relatively readily extracted from former. Moreover, the content of calcite in Hubei stone coal is much higher than that in Jiangxi stone coal. Calcium can react with V2O5 to form water insoluble calcium vanadates during roasting and this may be the reasone why the water leaching rate of vanadium is low for Hubei ore. Acid leaching is more beneficial to the vanadium leaching but other extra methods, such as adding aid-leaching agent and/or increasing acid concentration is need for the ore where vanadium is embeded firmly. This study can effectively guide the selection of vanadium extraction techniques for stone coal from different regions.

Jan 1, 2014

By DeVerle P. Harris, David E. Euresty

"Potential metal supply refers to metals to be produced from as yet unknown deposits. Naturally, to measure potential supply requires, among other things, inference to the number of deposits, their tonnage, and their grade Thus, probability distributions were constructed for each 400-square mile cell in Northern Sonora, Mexico. A computer system was developed that simulated the occurrence of deposits for each cell, exploration for the deposits, and their exploitation. Evaluation was performed for each deposit by discounted cash flow analysis.An objective of this study was to explore the effect of the transportation network and required road or railroad construction upon potential supply. Consequently, the evaluation system was designed to consider the spatial location of a simulated deposit to the existing transportation network and the market destination. The construction of linkages to connect the deposit to existing transportation arteries as well as the carrying of the concentrates to the intended market were simulated. in terms of cost. The selection of the path took into account the existing terrain. This was done by digitizing topographical maps and representing the topography of the area by an orthogonal grid of elevations. The optimum route was selected by dynamic programming, meeting a prescribed gradient constraint. The potential supply of each cell was determined, allowing for the infrastructure effect."

Jan 1, 2014

By Chen Dong, Yang Wenwang, Liu Zhineng, Tan Ming

"To meet the requirement of production expanding of a certain potash ore dressing plant in Xinjiang province of China, industrial test of XCF/KYF-50 flotation machine was performed to process potash ore. The tank of XCF/KYF-50 flotation cell is in U shape, 50m3 of volume. This flotation cell is able to suck slurry by itself, and can be arranged on the same base level without high difference. In this paper, two sets of XCF/KYF-50 flotation cells were adopted to replace 8 sets of 8m3 flotation cell in original flow sheet of flotation. Aeration rate, slurry suction capacity, power consumption and slurry suspension are investigated. The measuring results show the slurry suction capacity of the flotation cell is larger than 12.80m3/min and solid particles disperse evenly in the tank without deposition. Industrial test result indicates that the final grade of concentrate is 26.69% at the recovery of 90.95%, which is up to expected performance. XCF/KYF-50 flotation cell has advantages of high flotation efficiency, significant energy saving and reasonable configuration of automatic control system, this kind of flotation cell can meet the requirement of production expanding of this potash ore dressing plant well."

Jan 1, 2014

By Paolo Cavalcoli, Marco Ziller

"ABSTRACT: In the year 2010 the State of Denmark together with the Municipality of Copenhagen, launched a very important and complex Project : the complete construction of a new double Subway Line :the CITYRINGEN.Copenhagen is the capital with a metropolitan population of 1,9 million.This line is like a ring placed in the very town center which includes all the most historical and monumental buildings and churches, with a total length of 17 km, and the presence of 17 stations plus 4 service shafts.The buildings have been built in the last centuries in an area where the groundwater is near to the surface and there are lakes and channels: the techniques adopted were advanced for those times, but limited as far as regards settlements and resistance to horizontal movements.The soil consists in 2 main groups.1.Upper sediments of the glacial ages : thickness total = 5-20 m composed by clay- silt-sand-gravelcobbles- granite boulders and flint in blocs and in layers : frequency and size of these obstacles wherenot determined.2.Limestone layers : 2a. upper limestone : highly fractured ,highly permeable2b.Itermediate limestone : less fractured, medium permeability.2c. Lower limestone : almost not fractured, low permeability.2d Bryozoan limestone : composed by fossils with microscopic dimensionsIn all the limestone formations there are important layers of flint , having thickness variable up to 3 m and important extensions. Water : in a part of the areas of the Cityringen the water is drinkable and utilized in the public waternet.Pollution: there are polluted zones due to previous industrial activities. Benzene areas have been identified, and for those areas special protections against pollution have been implemented.METROSELSKABET ,the public owner of the Cityringen,has set as priority to operate for the construction of the Cityringen the full protection of the environment and the respect of all the stakeholders :Very strong limits for the exhausted gas emissions have been introduced, by far stronger than those applied from the State of Denmark, very strong limits for the acceptable noise emission. And last but not least very important safety measures and procedure to avoid any accident on site."

Jan 1, 2014

By A. Otsuki

This paper describes the evaluation method of dispersion and coagulation of silica nano-particles by means of interactive force apparatus. The apparatus measures the size of fine particles in aqueous solution or organic solvent of high concentration and/or low optical transparency. Other conventional apparatus for size measurements (such as, apparatus utilizing dynamic light scattering) are difficult to measure the size of particles in such conditions accurately, due to multi-scattering of light in the sample solution or solvent. The apparatus measures the interactive force between two surfaces, i.e. the gold-coated glass hemisphere and the brass flat plate, (which is fixed at the bottom of the sample cell). The apparatus has three parts, i.e. main part (which consists of electric balance, hemisphere and flat plate), control part (i.e. personal computer, piezo-stage controller and voltage supplier), and detecting part (i.e. multi-meter and oscilloscope). During the measurement, electric field is applied between the hemisphere and flat plate, and thus dielectric particles are arranged toward the direction of electric field in the area between two plates. When the two plates are close to each other, two different forces (i.e. repulsive force and attractive force) will alternately act on particles due to the structure change of the particles. The repulsive force occurs when the structure of particles is stretched by compressive force; whereas the attractive force occurs when the aggregate structure is broken. The cycle of the repulsive and attractive forces is a primary size of particle or size of aggregate, which depends on the degree of agglomeration. The measured size of particles, which is varied depending on their degree of dispersion and coagulation, determined the characteristics of the silica particles. In this research work, the effect of size and concentration of particles in aqueous solution on the degree of dispersion and coagulation of the silica particles were investigated. Spherical silica particles were selected for this investigation due to their variety of size. This apparatus can be used to evaluate the degree of dispersion and coagulation of other nano-particles in various solvents in many process industries.

Jan 1, 2014

By D. Auerswald, M. Kotze, V. Yahorava, T. Udayar

Uranium can be recovered from lower grade uranium ores (<800 mg/kg U3O8), leach residues, and waste dumps cost-effectively via resin-in-pulp (RIP). Using this technology, no solid/liquid separation or washing of the leach residues are required. Furthermore, the uranium recovery can be higher than with conventional methods. RIP technologies have, however, been perceived negatively due to concerns around potential resin fouling and losses. This paper highlights the advancements made in RIP and discusses a number of potential applications where the technology could deliver economic and consequential environmental benefits by reducing the uranium levels in the waste.

Jan 1, 2014

By H. Y. Ran

Magneto-flotation is a recently developing technology of mineral processing. This technology combines the traditional magnetic separation with flotation and provides a magnetic and buoyant force compound field to separate different minerals based on the differences of magnetism and floatability between useful minerals and gangue minerals. Magneto-flotation is applicable to separate ferromagnetic from nonmagnetic minerals, especially to separate magnetite from floatable gangue minerals. This magneto-flotation column is equipped with pulse electromagnetic field in the middle upper part, a bubble producer and upwell water inlet in the bottom. The pulse time of electromagnetic field in the column can be optionally adjusted and the maximum intensity of pulse magnetic field can reach 35mT. Pulse magnetic field can not only restrain magnetic minerals from entering into the froth layer, but also destroy the magnetic agglomeration to ensure a higher recovery and a higher concentrate grade. The results of experiments with magnetite show that pulse magnetic field has remarkable influence on flotation process. Compared with single flotation, magneto-flotation column can improve the recovery of magnetite by ten percent. After one time?s magneto-flotation processing, the grade of iron concentrate can increase from 65.4% to 69.5%, the content of silicon oxide in iron concentrate decreases from 7.4% to 2.8%, and the total recovery is above 96%.

Jan 1, 2014

By Claude Bazin, François Robichaud

The control of the operation of a semi autogenous grinding mill is mainly based on power and bearing pressure measurements. Image based sensors can provide on-line measurements of the size distribution of the ore feeding a SAG mill allowing the control of this variable that impacts the operation of this equipment. This paper investigates the potential of using the information from such type of sensor to maintain a SAG mill feed target size distribution by manipulating the speed of the ore extractors below an ore stockpile. A PID and adaptive predictive controller for the size distribution are studied using a simulator for a stockpile and the equipments used for ore withdrawing from the pile. The proposed controller is found to give a good performance while remaining easy to tune.

Jan 1, 2014