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By Tomohiro Yamasaki

"At the pre-construction foundations of the controlled waste disposal site built at the Port of Kinuura, the clayey soil account for the most, and with lesser amounts of sand compaction piles and sand mat. The cement deep mixing method (CDM) was used to improve ground impermeability and to reinforce the foundations on the seawall. Laboratory mixing and testing was performed to determine the appropriate quantities of cement additive for clayey soil, SCP sand, and sand mat. The test results indicated that maintaining the design strength of qu = 1,550 kN/m2 would require C = 100 kg/m3 of cement additive for all three soil types (clayey soil, SCP sand, sand mat). The permeability performance needed to improve ground impermeability assumes a permeability coefficient of K = 1.0×10-6cm/s. And the clayey soil satisfied the performance requirements at C = 100 kg/m3. However, to improve grand impermeability of the SCP sand and sand mat required more than 5% of particles having diameters of less than 75 µm. Thus, in the latter two cases, the required cement adding quantity was C = 250 kg/m3. The test specimens at one to two weeks after the created with a permeability coefficient of K = 10-6cm/s became permeability coefficient of K = 10-7cm/s six week later due to the effects of cement solidification. So the permeability coefficient declined about one order. The permeability coefficient three months later tends to decline continued with a somewhat lower.INTRODUCTIONBetween 2008 and 2011, the Aichi Seaside Environment Center constructed the Kinuura No. 3 offshore controlled waste final disposal site at Taketoyo in Aichi prefecture. (see Figure 1). The disposal site offers a landfill capacity of 5.21 million m3 and measures 472,000 m2 in area, of which some 344,000 m2 is a managed controlled sector enclosed within an impermeable seawall."

Jan 1, 2015

By Kenneth E. Henn, David B. Paul, John D. Rice, Brian H. Greene

"Several laboratory modeling programs have been conducted to investigate the mechanisms associated with internal erosion of dam embankments and foundations. The investigation consists of developing laboratory devices to model three separate mechanisms associated with process: 1) contact erosion along bedrock joints, and 2) piping into an open bedrock defect. The contact erosion device subjects the soil above a bedrock joint to high velocity flows in the joint. The erosion into a bedrock defect device examines a number of static and transient hydraulic conditions to study the mechanisms associated with this type of erosion. Numerous tests have been conducted using both devices. The results of the modeling will be discussed along with a discussion of how this information could be used in future dam design and risk assessment studies.IntroductionA series of laboratory modeling programs were performed to assess the seepage and internal erosion behavior of several man-made and natural structures within dams and their foundations. Each model was performed on a “bench scale” and depicted an isolated location where internal erosion was likely to occur. The models were subjected to hydraulic boundary conditions to simulate the in-situ conditions so that the processes of internal erosion could be observed. Two laboratory devices were developed to model conditions depicting 1) contact erosion along a bedrock joint in contact with a dam embankment, and 2) backward erosion (piping) into an open bedrock defect (joint, solution void, etc.).Embankment dams often have rock foundations containing defects which may detrimentally impact future performance. Further, there are existing foundations which contain rock defects that may already be detrimentally impacting the dams; however, due to the inherent aspects of the mechanism, the signs of distress may not have propagated to the surface and thus not observed during inspections. A better understanding of the mechanisms which are influenced by, and impose their influence upon, rock defects will enhance the ability of dam safety professionals to analyze the risks associated with internal erosion due to rock defects, increase our ability to monitor and successfully initiate earlier detection, and also increase our ability to design remediation methods to contend with rock defect failure modes."

Jan 1, 2016

By N. J. Tannyan

Laboratory bath smelting tests were conducted to determine the feasibility of smelting nickel- copper concentrate directly to a low iron matte in one step. Concentrate, air/oxygen and a silica flux were fed to a matte-slag bath kept in MgO crucibles at 1300°C. Various oxygen enrichments and smelting rates were used to maintain 0.5 to 2 wt"10 iron in the product matte. The slag losses are comparable to those obtained under similar industrial conditions. Due to the highly oxidizing conditions required to produce mattes with low iron contents, it is not recommended to target iron contents below about 2% in the matte. The specific bath smelting rates were equal to or higher than those in various industrial bath smelting processes.

Jan 1, 2003

By N. J. Tannyan

Laboratory bath smelting tests were conducted to determine the feasibility of smelting nickel- copper concentrate directly to a low iron matte in one step. Concentrate, air/oxygen and a silica flux were fed to a matte-slag bath kept in MgO crucibles at I 300°C. Various oxygen enrichments and smelting rates were used to maintain 0.5 to 2 wt% iron in the product matte. The slag losses are comparable to those obtained under similar industrial conditions. Due to the highly oxidizing conditions required to produce mattes with low iron contents, it is not recommended to target iron contents below about 2% in the matte. The specific bath smelting rates were equal to or higher than those in various industrial bath smelting processes.

Jan 1, 2003

By Stephen C. Blair

Laboratory permeability measurements at elevated pressure and at temperatures ranging from 20º to 150°C have been conducted on samples of Ironton-Galesville sandstone. The purpose of this testing was to identify and characterize important physicochemical processes occurring in association with the injection and withdrawal of heated ground water at the U.S. Department of Energy's Aquifer Thermal Energy Storage (ATES) field site in St. Paul, Minnesota. Results indicate that permeability decreased significantly as temperature was increased and that dissolution of the dolomite and silicate cementing agents and accompanying changes in mechanical properties may occur in the heat storage aquifer at St. Paul. Further, loss of permeability with temperature in laboratory samples may be caused by the change in the mechanical structure of the sample. Tests at ambient temperature to evaluate the effect of particle migration under conditions of reversed flow indicate that this process will not significantly impair formation permeability at the St. Paul site.

Jan 1, 1984

By C. MeCulloch

A NOVEL practice in the bituminous coal industry is the accelerated method of burning coal to ash used in the laboratory of the Fidelity washery of the United Electric Coal Companies, Du Quoin, Ill. Development of this method has supplanted the tedious float-and-sink process for plant control at this plant. In normal operation the plant operators have available within thirty minutes the accurate ash percentage of the coal loaded in the railroad cars and can therefore make adjustments to maintain a practically uniform quality of washed coal, regardless of the variations in washery feed.

Jan 1, 1937

By L. J. Erck, T. E. Ban

A discussion of laboratory procedures used to determine pellet quality and to simulate handling and firing conditions. Strength- temperature relationships in pelletizing; effect of chemical additives on agglomeration; and crushing, abrasion, and impact resistance of the pelletized products are discussed with respect to five different iron ore concentrates.

Jan 8, 1953

By Lewis Martin

Spokane Research Center personnel are currently conducting research on cable bolts to assess their material and support properties, to provide design criteria for roof control systems under various types of underground mining conditions, and to provide background data for computer models of cable bolt supports. Laboratory studies of cable bolts made of conventional steel cables with Garford bulbs and collars resulted in recommendations on characteristics such as embedment length, hole diameter, cable bolt diameter, and configuration of cables. A completed series of laboratory tests has determined the minimum embedment length of resin required for resin-grouted, cable bolt ground support.

Jan 1, 1996

By Patrick R. Taylor

Glass is used for immobilization of radioactive and hazardous wastes due to its durability and ability to accept a variety of waste constituents into its network structure. Alternative high temperature vitrification techniques have the advantage of increased throughput, increased waste loading and being applicable to variable and heterogeneous waste streams. However, the increased processing temperature places further concerns on the increased volatilization of contaminants, and increased corrosion and erosion of me Iter components. A database of melt properties at higher temperatures, such as partitioning, viscosity, density and electrical conductivity, in the temperature range of 1400-20000 K are being developed.

Jan 1, 2000

By Tang Chaoho

Laboratory research on the reducing and matte smelting of Jamesonite concentrate has been carried out. The influence of the process conditions such as the smelting temperature, the amount of pyrite cinder (the agent of fixed sulfur) and the amount of additives on the smelting process have been studied. Under the optimum condition the direct recovery ratios of antimony and lead are 83.26% and 68.50% respectively. The ratio of fixed sulfur is 98.97% but more than 15% lead and 30% silver remained in the ferrous matte. The key problem to be solved of this new process is how economical and effective is the recovery of silver and lead in ferrous matte.

Jan 1, 2003

By Tang Chaoho

Laboratory research on the reducing and matte smelting of Jamesonite concentrate has been carried out. The influence of the process conditions such as the smelting temperature, the amount of pyrite cinder (the agent of fixed sulfur) and the amount of additives on the smelting process have been studied. Under the optimum condition the direct recovery ratios of antimony and lead are 83.26% and 68.50% respectively. The ratio of fixed sulfur is 98.97% but more than 15% lead and 30% silver remained in the ferrous matte. The key problem to be solved of this new process is how economical and effective is the recovery of silver and lead in ferrous matte.

Jan 1, 2003

By D. A. Wheeler, Rémi Tremblay

"INTRODUCTIONDuring the last few years, through Column Flotation Company of Canada ltd, the Centre de Recherches minérales has worked on the column flotation of coal, phosphate, feldspar, talc, graphite, copper, lead-zinc and diamond ores. The operating companies and prospective deposits were located in Canada and in other countries. Since these projects were financed by the concerned mining companies, all results remain confidential unless we obtain permission to publish. Three companies have graciously allowed us to use their information which I will describe in this text. These are the Polkowice copper mine in Poland, the North Coast Industries ltd graphite deposit and a talc company which preferred to remain anonymous. I will also describe our 2 inch column which was used for all tests. Data is also given on how to scale-up the 2 inch column to industrial size.Figure 1 presents a schematic of a flotation column. Feed, at a controlled rate and pulp density, enters at about 1/4 of the height of the column from the top. A controlled rate of air is bubbled into the bottom of column through a fine-holed sparger. The column volume between the feed point and the top of the sparger is called the recovery zone. Tailings, at a controlled rate, always slightly greater than the feed rate, discharges from the bottom of the column. This difference in feed and tailings flowrates is called the bias. The floated mineral is carried through the recovery zone on air bubbles which rise into the cleaning zone which is that column volume between the feed point and the overflow at the top. As the bubbles rise in this zone they are washed of gangue material by wash water which enters over the top of the froth layer. The froth layer is maintained at a given depth during flotation but this depth will depend on the froth cleanliness, for quite a bit of cleaning by wash water is accomplished in this layer."

Jan 1, 1988

By Andrew Artzer, Michael Moats, Jack Bender

Antimony and bismuth in copper electrorefining electrolytes can cause cathode contamination, leading to the careful control of their concentrations. This study examined the laboratory scale removal of bismuth and antimony from an electrorefining electrolyte using a solvent extraction mini-pilot plant. The ability of a proprietary phosphonic acid ester extractant (REX-2) in a commercial diluent was studied in a simulated commercial setting. Antimony and bismuth were both extracted effectively from the electrolyte (72% Bi and 70% Sb removed) and Bi was effectively stripped (92% Bi recovered) with 400 g/L sulfuric acid. A final strip solution was obtained from the SX circuit containing 0.36 g/L Bi, 0.043 g/L Sb, 1.3 g/L Cu, and 0.18 g/L As. Unfortunately, most of the extracted Sb remained in the organic phase. Following the pilot study, experiments were performed to examine the precipitation of bismuth from the aqueous strip phase and the removal of antimony loaded on to REX-2. INTRODUCTION For many years, antimony and bismuth have been some of the most problematic impurities in copper electrorefining (ER) (Bardwell & Lapee, 1933). Along with surface roughening, high concentrations of Sb and Bi can contaminate the copper cathode and precipitate at the copper grain boundaries. This drastically reduces the drawing ability of the metal (Bender & Emmerich, 2016). For these reasons, it is necessary to control Sb and Bi concentration in the cathode, which is done by controlling their concentration in the electrolyte. Conventionally, Sb and Bi concentrations are controlled by maintaining a proper As/(Sb+Bi) molar ratio in the anode and arsenic concentration in the electrolyte. Antimony and bismuth are removed during electrolyte purification using liberators (electrowinning cells) and/or ion exchange. Liberators treat an electrolyte bleed stream from the ER circuit and electrodeposit increasingly impure copper as the copper concentration of the solution decreases. Traditionally, first stage liberators reduce the copper concentration from ~45 g/L to ~15 g/L and produce saleable copper. Second stage liberators decrease the copper concentration to ~8 g/L (Biswas & Davenport, 1980) which results in contaminated cathode that is returned to anode production (Biswas & Davenport, 1980; Wang, 2004). Further electrolyte purification is not always required but third stage liberators can be used to reduce copper concentration below 2 g/L which results in significant removal of As, Sb and Bi and very impure deposits which are recycled to a smelter or used for As production. However, liberators do not have very high energy efficiency (Acharya, 2014; Ando & Tsuchida, 1997) and below 0.5 g/L copper, highly toxic arsine gas may form (Biswas & Davenport, 1980).

Jan 1, 2019

By Robert Vidal

The performance of a laboratory-scale cell for the electrolysis of an aqueous chrome alum solution was studied. Electrode potentials, pH, and Eh were recorded. An optimum catholyte pH of about 2.5, consistent with information from the literature was observed. Values exceeding this range resulted in a precipitate formation and are detected by wavering cathode potentials. The role of anodically produced dichromate ions was investigated by chemical analysis. It was found that the steady state concentration of dichromate ions varies inversely with fluid flow from catholyte to anolyte. This concentration was also reduced with the use of precious metal coated titanium anodes.

Jan 1, 1994

By J. A. Beukes, M. Marais

TICOR South Africa is a new titanium feed stock producer. In the Ticor South Africa plant the ilmenite feed to the smelter plant is roasted to enhance its magnetic properties. This allows for the magnetic separation of chromite from the ilmenite. The magnetization reaction relies on partial oxidation with both under- and over-oxidation causing insufficient magnetization. To subject the roaster plant feed material to the required physical conditions a circulating fluid bed (CFB) roaster is used. This paper describes the development of a laboratory model that will aid in the control of the CFB roaster.

Jan 1, 2003

"Successive seismic waves may cause progressive weakening of a fault zone, which has been recognized as the mechanism of earthquake aftershocks. However, it is unclear that how a fault zone slips under each wave cycle and how slip displacement accumulates under continuous wave cycles. This laboratory study provides direct evidences on the slip process of a simulated granular fault zone dynamically induced by an incident wave without the effects of late-arriving and reflected waves. The experimental observations show forward and backward slip paths of the fault zone and partially recovered slip displacement after a wave incidence. The unrecovered slip displacement after each wave cycle can be accumulated until it reaches a critical slip distance for seismic faulting, which may reinterpret delayed triggering in earthquake dynamics. The limited interseismic period restricts fault self-healing in strength. The experimental results also indicate that the dynamically induced frictional slip on the fault zone is associated with a complex frictional system, including seismic wave radiation, frictional slip initiation and normal stress vibration. Different from the dynamically induced frictional slip on the fault zone, the statically induced frictional slip causes a permanent increase of slip displacement along the shear loading direction. INTRODUCTIONAn earthquake mainshock may induce aftershocks by suddenly changing external stresses applied to another fault zone in the near field (Kilb et al., 2000) and by slightly perturbing a fault zone from a critical steady state to stick-slip faulting in the far field (Gomberg and Davis, 1996). The dynamically induced frictional slip on a fault zone has been recognized as the mechanism of earthquake aftershocks (Marsan and Lengliné, 2008; van der Elst and Brodsky, 2010). Although earthquake aftershocks have been extensively studied by many seismological methods, a simplified laboratory fault zone can provide possible interpretation on real faulting and detailed analysis on a friction process (Dieterich, 1979; Nielsen at al., 2010). According to a few laboratory experiments related to the dynamically induced frictional slip on a simulated fault zone (e.g., Uenishi et al., 1999; Johnson et al., 2012), the slip process induced by successive seismic waves exhibits continuous motions. However, it is unclear that fault slip response under each wave cycle and slip displacement accumulation under continuous wave cycles."

Jan 1, 2015

By M. C. Bétournay

Strainbursts are common in overstressed brittle rock around deep mine openings. Such failures are characterized by a biaxial state of stress in the plane of the opening boundary. A zone of compressive stresses imposes initial failures near or at the surface of the opening that results in spalling of thin slabs of rock roughly parallel to the free face. While the failure of rock under biaxial loading conditions is increasingly common in deep underground mines, only a few representative laboratory studies have been reported in the literature, without emphasis on rockbursting aspects, and none in the last decade. This paper presents the results of a testing program on a granite rock type. Biaxial testing, conducted on 100 mm cubic samples, was carried out to examine the influence of lateral confinement and loading rate on the rock’s ultimate strength. The paper reports the test results in terms of normalized biaxial failure envelope s1/sc-s2/sc. A discussion of the failure mechanisms observed is presented. Les coups de toits de déformations sont choses communes dans le rock cassant surcontraint en place autour des ouvertures minières profondes. De telles ruptures sont caractérisées par un état de contraintes biaxiales dans le plan de la périphérie de l’ouverture. Une zone de contraintes compressives impose des ruptures initiales à ou près de la surface de l’ouverture, qui produit des relâchements de minces plaques de roc plus ou moins parallel à la surface. Bien que les ruptures de roc sous des conditions biaxiales sont de plus en plus communes dans les mines à grandes profondeurs, il n’y a eu que quelques études représentatives en laboratoire de publiées, sans emphase sur des aspects de coups de terrains, et aucunes publiées depuis la dernière décennie. L’article présente les résultats d’une campagne d’essais appliquée à un type de granit. La campagne d’essais biaxiaux, sur des échantillons cubiques de 100 mm, avait pour objectif d’examiner l’influence du confinement latéral et le taux de chargement sur la résistance ultime du roc. Cet article fait part des résultats en terme de l’enveloppe de rupture biaxiale normalisée s1/sc-s2/sc. Une discussion sur les mécanismes de ruptures observés est présentée. Dehnungsbrüche findet man häufig in übergespannten spröden Felsen um die Öffnung von tiefen Minen. Solche Brüche sind von einer zweiachsigen Spannung in der Ebene der Grenze der Öffnung charakterisiert. Eine Zone von Druckspannungen verursacht initiale Brüche, entweder an der Öberflache der Öffnung oder in der Nähe. Davon scheiden sich dünne Felsplatten mehr oder weniger parallele mit der freien Wand. Obwohl Felsbrüche unter zweiachsiger Beanspruchung immer mehr häufig in tiefen Minen beobachtet sind, hat man über nur einige repräsentative Laborversuche in der Literatur berichtet. Diese Studien diskutieren das Thema ohne Betonung auf Felsbrüchen, und keine sind in den letzten zehn Jahren erschienen. Die vorliegene Arbeit gibt die Ergebnisse eines Testprogramms auf einem Typ von Granitfels. Durch zweiachsige Prüfungen von kubischen Proben mit Seitenlangen von 100 mm sollte man den Einfluss von seitlicher Ermittlung und der Beanspruchungsrate auf die Bruchfestigkeit des Felsen studieren. Man findet auch die Prüfergebnisse in bezug auf das normalisierte, zweiachsige Bruchkriterium s1/sc-s2/sc. Die beobachteten Bruchmechanismen sind auch diskutiert.

Jan 1, 2003

By Wright J. K

A description is presented of the results of reduction experiments using a laboratory reduction apparatus in which simulation of the gas and temperature profiles which occur in direct reduction shaft furnaces is achieved using microcomputer control. The apparatus allows continously changing reduction conditions to be impressed on lump or pellet samples to simulate the environment that is experienced by iron ore burdens during their transit down the shaft of a direct reduction furnace. Three pellet samples and three lump ore samples were reduced in the apparatus. Comparative reduction curves and strengths after reduction for the materials were obtained over a range of reduction temp- eratures using Midrex-type gas compositions. The resulting reduction and strength curves show considerable variation in behaviour and reflect the physical and chemical variations in the individual ore and pellet types. A comparison is made of the reduction rates and modes of reduction of the samples reduced under "conventional" test conditions using a single unchanging gas composition and the simulated shaft furnace reduction conditions. It was observed that the course of reduction is very different in the two procedures and the major influence of temperature on the strength of the reduced product is noted.

Jan 1, 1987

By E. Bane Kroeger

For many years, researchers around the world have been investigating coal pillar stability. Many have focused on trying to optimize the size of the pillars by examining stable and failed pillars in underground coal mines. For mines that are already in operation or companies that are opening a new mine adjacent to an existing mine where the pillar dimensions and stability can easily be determined, this is the preferred technique. However, when a new mine is planned for an area where there has been relatively little mining, then samples of the coal need to be drilled and tested for strength. Because of the fractured nature of coal, this lab testing is often problematic and may often yield poor results because of the limited size and number of samples that can be obtained from the core. To remedy this problem, research was conducted in the labs at SIUC to determine if improvements could be made when optimizing the size of pillars for underground coal mining in Illinois. Through a greater understanding of the relationship between dimensions and strengths of coal samples tested in the lab, it was hoped the in situ strength of coal pillars could be determined with greater accuracy. This could allow the extraction ratio to be increased and more of the coal resources in Illinois recovered without impacting the safety of the mine workers. Many different agencies around the world have published recommended minimum numbers of samples for strength determination based on the size of the coal samples. For two inch cubes, uniaxial testing of at least seven samples is recommended and this minimum number decreases to four when testing four inch cubes. However, the laboratory testing of coal from two seams thus far has suggested this number should be almost doubled to accurately determine the coal strength. Testing also showed there is a pronounced decrease in the variation in the strength of the samples tested as the dimensions of the sample were increased. From the testing results thus far, it is recommended that a sample size versus strength curve be constructed for every coal seam for Illinois. Creating such a curve will better determine both the minimum number of samples and minimum sample dimensions for that seam or region of a particular scam. A second set of tests were conducted in the laboratory to determine the increase in strength with reduction in height for samples with the same width and length. In Illinois, typical pillar dimensions are 40 to 80 feet (12.2 to 24.4 m) wide and long, with coal thickness varying from about 4 to 9 feet (1.22 to 2.74 m). This provides width/height ratios ranging from 4.5 to 17.5. Coal samples having width/height ratios ranging from 0.5 to 13 have been tested thus far. As with most pillar design formulae, the strength of the Murphysboro coal versus width/height ratio was linear and closely matched shape factors published by other researchers. The laboratory testing thus far has identified three factors that affect the strength of laboratory samples, the number of discontinuities, the angles of critical discontinuities, and the shape of the samples. The factor that probably had the most pronounced effect on the strength of the coal samples was the angle of critical discontinuities. This testing has confirmed that there is still a gap that needs to be bridged between the strength obtained from laboratory testing and the in situ coal strength predicted.

Jan 1, 2004

By Quast K. B

Samples of limestone and micaceous hematite have been ground in a laboratory batch mill using equal weights of either rods or balls. Values of the Schuhmann distribution modulus, a, have been shown to depend on grind time and do not remain constant as often reported. The linear reduction in a with grind time was attributed to a change in grinding mechanisms with time. The product sizing from ball milling limestone showed a bimodal distribution, but rod milling produced a unimodal size distribution. The product sizing from milling micaceous hematite was difficult to interpret due to the major influence of the shape factor on the transition from screen sizing to cyclosizing.

Jan 1, 1995