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By Carlton E. Brown

In 1935 , Brown and Yant / described a microprojector ( microscopic arrangement for projecting images on a screen ) for use in counting and measuring the size of dust particles in Owens - jet dust - counter and simila dry samples of dust collected from the air . In 1938 Brown and others , described a modification of this microprojector that could be used also in counting dust in impinger samples . Microprojectors of this second type have been set up by many mining companies and others and have been made commercially available . Hamly and Pullen5/ described a modification of this microprojector for use in making rapid comparative estimates on konimeter samples and other determinations . This report contains information on still another modification named the "midget microprojector " because of its small size .

Sep 1, 1944

Develop a method for mapping planar geologic features in deep underground mines where the presence of metal interferes with compass readings. Background A fundamental problem of mapping planar geologic features in deep underground mines is the presence of metal (water and air pipes, track, equipment, etc.), which affects the accuracy and consistency of compasses. Present geologic mapping methods include use of transits or theodolites, both of which are cumbersome and time consuming to use. To complicate the mapping, process each planar feature must be surveyed, and if that feature is not apparent on the opposite wall, it cannot be mapped. Another method of mapping is to stretch a tape measure between two survey spads and place a string along a planar feature on one wall and out into the opening until it intersects the tape measure. This method, in addition to being time consuming, is also inaccurate. Because detailed mapping of planar geologic features deep underground involves many repetitive measurements, a quick, accurate, and reliable method for making such measurements was necessary. The geolaser was developed to make such measurements in deep underground mines where metal interferes with conventionally used compasses.

Jan 1, 1990

By Walter W. Fisher

A kinetic investigation of copper cementation in a revolving drum was undertaken by the Bureau of Mines to explore the effects of a porous copper deposit attached to the iron surface and a fluidized slurry of copper particles surrounding the iron precipitant. The rate of cementation was found to be significantly enhanced by the increased cathodic areas provided by a porous copper deposit or the presence of a fluidized bed of copper particles contacting the iron precipitant. The cementation rate was found to be retarded by increased ionic strength, low pH, and the presence of oxygen. The cementation reaction was first order with respect to precipitant surface area. Copper cementation on iron is visualized to occur by two basic mechanisms. Precipitation may occur through a series of shorted electrochemical cells, whereby cupric ion precipitates on a growing cathodic copper deposit, or, deposition may occur via a fluidized cathode of copper particles contacting the ion precipitant.

Jan 1, 1976

To produce industrial-grade titanium castings by processes that are nonpolluting and lower cost than the currently used rammed-graphite process. Approach Foundry-grade zircon and olivine sands, bonded by waterglass or bentonite, are used to make shell or rammed molds which require relatively low-drying temperatures and do not generate noxious fumes during drying or casting. Procedures Three separate processes have been developed which meet the stated pollution and cost goals. These are: 1. Waterglass-bonded rammed zircon or olivine sand molds are dried at 480°F, zirconia washed, redried, and used in an inductoslag or skull-casting furnace. 2. Waterglass-bonded zircon or olivine sand shell molds are formed at 560°F, cured at 620°F, zirconia washed, dried at 480°F. and used in an inductoslag furnace. 3. Rammed zircon and olivine sand molds are bonded with western bentonite, zirconia washed, dried at 980°F, and used in an inductoslag or skull-casting furnace.

Jan 1, 1981

By Robert M. Becker

A thick-wall cylinder solution applicable to the evaluation of anisotropic elastic parameters is derived for the interpretation of stress relief data. For a restricted class of problems, a special relationship among certain orthotropic moduli yields stress distributions for the plane orthotropic problem that are identical to the corresponding isotropic case. A ring or hollow cylinder with these specialized anisotropic properties subjected to uniform radial loads is one of the problems in this class. Consequently, known stress solutions are used to develop the strains and displacements for a specialized orthotropic thick-wall cylinder under uniform pressures. The results are consistent with anisotropic equations used in the evaluation of in situ rock stresses.

Jan 1, 1968

To more rapidly and economically prepare solutions for chemical analysis, of a wide range of ores, slags, minerals, and metals. Approach A Simple pressure-dissolution system was devised using an inexpensive, heavy wall plastic bottle containing a sample in an acid medium. Using the technique, a complex silicate sample can be dissolved in less than 1 hour. How It Works A weighed portion of a sample, ground to minus 100-mesh, is placed into a polycarbonate or polysulfone plastic bottle. A mixture of hydrochloric acid, nitric acid, and hydrofluoric acid then is added. The bottle threads are wrapped with a layer of Teflon tape to prevent leakage, and the bottle cap is screwed on tightly. The sealed bottle is placed in a balling water bath. In the hot water, the plastic bottle acts as a pressure vessel to contain the pressure generated inside it. This technique should only be used by trained experienced people who are familiar with the hazards of hot acids under pressure. After being cooled in cold water, the resulting solution is brought to the final volume by adding 1.5 weight-percent boric acid solution to the bottle. The cap is replaced, and the bottle and solution is reheated. Precipitated fluorides, as well as any residue, are dissolved by the fluoride-boric acid reaction. The resulting clear solution then is suitable for spectro-photometric examination or other analysis.

Jan 1, 1980

By D. G. Kuehn

Studies were conducted by the Bureau of Mines to determine the positive ions and neutral species produced in glow discharges of gas streams containing 1.0 percent NO in helium, 29 percent dry air in helium, and 1.06 percent NO in N2, Mass spectrographic measurements were conducted for gas pressures from 2.3 to 10.0 torr and dc currents from 10 to 20 mAo Ion species observed included NO+, N2 +, O2 +, N+, and 0+ with lesser amounts of He+, He2+, and N02+. Variations in various ionic and neutral species with discharge duration were interpreted to be consistent with an electrically induced dissociation of NO to produce N2 and O2. No nitrogen oxides were observed to form in glow discharges of the helium-air mixture.

Jan 1, 1975

By William H. Schiffbauer

This paper details the computer hardware and software integrated to provide computer-assisted control and monitoring of four different coal mining machines. The backbone of each system is a U. S. Bureau of Mines integrated distributed microcomputer control network called BOM/NET. The network provides connections for intelligent sensors and systems that provide for navigation, diagnostics, and computer control. Many different computer systems using various operating systems (including RMX I, UNIX, VXWORKS, DOS and DCX51) have been connected to the network and each have had complete network functionality. A description of the network's integration to Joy' 16CM, a Joy 14CM, a Jeffrey 102, continuous mining machines, and a custom built auger machine is provided. The networks for the Joy 16CM, the Joy 14CM, and the Jeffrey 102 have been installed and extensively tested at the Bureau's surface test facility. The Jeffrey 102 system has also been tested in a highwall coal seam. The Joy 14CM will soon be tested underground.

Improve underground mine roof bolt support systems by alleviating problems associated with certain ground support systems currently being used. Approach Convert a passive resin-grouted roof bolt system into a uniform, tensionable roof bolting system. Background Resin-grouted roof bolts are one of the most common forms of ground support in U.S. underground coal mines. These support systems can be installed with a full-column of grout and be loaded with subsequent roof movements after installation. This is called a "passive" support system. An alternative to the passive support system is the mechanically-anchored, tensioned roof bolt system. This system is installed with resin grout. This system is designed to load or tension the support during installation by using a mechanical anchor, coupling, or threaded nut after the resin has properly cured. It is called an "active" support system and is used extensively for improved strata control in a laminated geologic deposition or in difficult ground conditions. To ensure that active bolts have been properly installed, the bolt loads must be checked by using a torque wrench or other suitable equipment. Unfortunately, this practice presents potential safety hazards and has limited accuracy. Laboratory and field experiments also reveal that the torque-to-tension ratio developed on active support systems can vary by 50% from bolt-to-bolt. Variations in bolt load installations can induce stress concentrations and lead to roof degradation or failure.

Jan 1, 1991

Improve mine refrigeration system efficiency while providing free electrical energy to mines. Approach Convert the potential energy of incoming mine water falling down long vertical shafts into electrical energy by means of a turbine-generator system located at the bottom of the mine shaft. How it Works Converting the energy of falling water into useful work is a well-developed engineering concept. Water flowing down long vertical pipelines into deep mines develops high pressure that can be used to operate a turbine-generator system at the bottom of the pipeline. A thermal energy recovery system of this type offers three advantages: 1. In systems without turbines, the potential energy of the water is converted to heat. The water temper-ture will automatically

Jan 1, 1985

Provide the mining industry with a method for determining the gas content of ore bodies and associated strata for use in mine planning, Approach Samples of various rock types are collected and tested to determine gas content in conjunction with sample size, the collection method (i.e. whether the sample was collected from a core sample or by hand) mine gas emission, and the geologic location from which the sample was taken, such as near a fault, outburst area, or other geologic anomaly. How It Works Two methods were developed by the Bureau of Mines to determine the gas contents of rock samples. The first method developed involved dissolving minerals to measure gas emission. This method, however, can only be used with soluble minerals. A second method, therefore, was developed for use with insoluble minerals. With this method, the sample is crushed in a ball mill. Although the dissolution method is faster and more accurate to use, the crushing method is also advantageous because its use can more closely approximate a mining situation; the sample is crushed as in mining and the amount of gas released relates to the amount of gas that would be released during a mining operation. The dissolution method is applied to soluble minerals, such as rock, salt, or trona, in a sealed chamber. Gases released during dissolution are collected for analysis by gas chromatography. One advantage in using the dissolution method is that the test apparatus is relatively inexpensive. In addition, test can be performed at any scale, from single crystal samples to a solution mining operation.

Jan 1, 1983

By D. Montagna

Large quantities of zinc-base die-cast scrap containing 3 to 4 percent aluminum are presently refined by mixing with other secondary zinc products such as galvanizer dross and distilling in a retort. The Bureau of Mines investigated alternate aluminum removal processes utilizing low-cost fluxes. Basing the investigation on the metallurgical principle that a reactive impurity can be removed from a less reactive matrix metal by melting under a flux consisting of a salt or oxide of a metal less reactive than the impurity, three separate flux mixtures were studied. In the first flux system, [FeCl3] + NaCI (the active component is underlined), part of the aluminum is' eliminated by the formation of volatile aluminum chloride and the rest by the creation of a high melting point iron-aluminum intermetallic compound that can be separated from the remaining molten zinc by filtration. Aluminum removal in the second system, [Fe203] + CaClz + NaCI, is effected by the formation of the iron-aluminum compound and possibly aluminum oxide. The third system, spent sal skimmings--essentially a mixture of [ZnCl2], NH4Cl, and ZnO, depends solely on aluminum chloride formation. Of the three flux systems investigated, the best results obtained were with system 3. Aluminum was reduced in the molten die-cast alloy from 4.10 percent to 0.01 percent when depleted sal skimmings were used.

Jan 1, 1969

Improve ground control in longwall gate entries by developing a practical method for evaluating longwall pillar designs. Background Longwalls have emerged as the most important technology to be applied to underground mining since the continuous mining machine. Longwall mines currently produce more than 30 pct of all the underground coal mined in the United States, up from less than 5 pct just 15 years ago. Safe longwall mining depends on maintaining ground control in the gate entries, the lifelines that provide access to the longwall face. In multientry retreat mining as practiced in the United States, rows of chain pillars are left to protect the gate entries (see figure 1). Chain pillars are subject to severe and complex abutment loads during the process of longwall panel extraction. The design of these pillars is often the single most important element in gate entry ground control and has been the subject of intensive Bureau of Mines research.

Jan 1, 1991

By Kenneth J. Miller

The Bureau of Mines conducted an investigation to improve the flotation response of coals that are difficult to wash by froth flotation. A literature survey and experimentation showed that, for the most part, refractory coals can be floated with oily collectors and frothers. Collector reagent consumption can be minimized and the selectivity of the flotation enhanced by assuring adequate, but not prolonged, reagent conditioning. Where flotation selectivity is especially poor, two-stage rougher-cleaner flotation is recommended. It was concluded that a major problem with refractory coals is predicting when they will appear in a flotation circuit so that supplementary flotation collectors can be added. Coal losses due to variation in the floatability of the feed might be reduced if a nonpolar collector such as kerosine or fuel oil is used along with a frother as general coal flotation practice.

Jan 1, 1977

By Frank J. Susko

The U.S. Bureau of Mines is developing a process for removing metals from mining and mineral processing waste streams by precipitation. The precipitation process is accelerated by flocculation when a high molecular weight polymer is added. Infrared (IR) studies were performed on zinc hydroxide [Zn(OH);J, copper hydroxide [Cu(OH);J, and zinc sulfide (ZnS) flocculated with both non ionic and anionic polyacrylamide (PAM) and polyethylene oxide (PEO). The IR data were compared with general trends in the performance of the polymers observed during flocculation. These studies will help to understand the bonding between the precipitate and polymer and indicate the effectiveness of a flocculant for dewatering. Two types of bands showed up on the IR spectra; one type described the interlayer water of the flocs, the other described the organic bonds of the polymers. A general decrease in the areas of the three water bands, hydroxyl (O-H) stretching (3,200-3,500 cm-1), water bending (1,610-1,630 cm-1), and torsional oscillations (600-700 cm-1), indicate interlayer water being driven off, which is a favorable condition in flocculation. Shifts in the O-H stretching band indicate water bridging between the precipitate and polymer. Shifts in the amine (N-H) deformation, carbon-nitrogen (C-N) stretch band (1,600-1,610 cm-1) indicate the amine group of the PAM is involved in the bonding. Evidence suggests that ether oxygen of PEO is also involved in the bonding process.

Jan 1, 1990

By T. A. Henrie, D. C. Fleck, D. G. Kesterke

Uranium metal was electrowon from uranium dioxide dissolved in fluoride melts . The UO₂ was fed directly to the cell in a continuous manner . Electrolysis was performed at 1 , 200 ° to 1,300 ° C in electrolytes composed of UF4 , LiF , and BaFa . A single regulus of metal was collected in a confined area of the crucible . Product purity of 99.8 percent was attained . Carbon was the major contaminant . Compartmented cells were studied as a means of confining the oxide feed to the vicinity of the anodes .

Jan 1, 1964

By G. R. Hopkins

A fifth successive record in fuel efficiency was established by the petroleum-refining industry in 1937, when the average heat requirement per barrel of crude oil run to stills was 554,000 B. t. u. compared with 597,000 B. t. u. in 1936. These amounts represent roughly the heat obtainable from a tenth of a barrel of fuel oil (see fig. 1). Innumerable factors can influence heat consumption at refineries, but only a few are important enough to be subject to statistical measurement. Foremost of these is the ratio of runs to capacity, it being generally recognized that because the fuel demands for other than stills are comparatively inelastic, total heat requirements do not increase in direct proportion to crude runs. Thus, in 1937, crude runs of 1,183,440,000 barrels were 11 percent higher than in 1930; the average operating ratio was 83 percent compared with 79 percent in 1936; but the total heat requirement increased only 4 percent, or from 638,149 billion B. t. u. in 1936 to 663,966 billion B. t. u. in 1937.

Jan 1, 1938

Develop a cost-effective diesel aerosol sampler that can be used by industry and regulatory agencies to determine the diesel exhaust aerosol concentration in mine atmospheres. The sampler must be easy to use, wearable by mine personnel, compatible with current personal sampling protocols, and inexpensive. Approach The University of Minnesota (University) and the U.S. Bureau of Mines (USBM) have developed and tested a prototype diesel exhaust aerosol sampler. The sampler, however, was complicated and expensive to fabricate. Consequently, the USBM redesigned the sampler to simplify both manufacturing and use, and the sampler was evaluated to ensure equivalency with the prototype. Background The National Institute for Occupational Safety and Health (NIOSH) has recommended that "whole diesel exhaust be regarded as a 'potential occupational carcinogen,' as defined in the Cancer Policy of the Occupational Safety and Health Administration." In addition, the U.S. Mina Safety and Health Administration (MSHA) has been directed by an advisory committee to establish a diesel exhaust aerosol standard and regulations to minimize exposure to diesel pollutants in underground coal mines.

Jan 1, 1992

Rank the dust knockdown (airborne capture) ability of six different types of water spray nozzles, Approach A fixed quantity of dust is released into a large, closed chamber in a laboratory. Water sprays are turned on inside the chamber and their effectiveness on the dust cloud is evaluated from the rate at which the dust disappears. This method better simulates dust suppression underground than methods tried earlier. The results of the laboratory test were confirmed by conducting tests on a full-scale mod-el continuous miner face where dust levels were measured in the return airway. Results of the Closed Chamber Tests The graph indicates that atomizing nozzles provide the best use of water for dust scrubbing. However, use of these nozzles is limited by their susceptibility to damage and clogging. Hollow-cone nozzles perform almost as well as atomizing nozzles. Test results also indicate that full-cone, venturi-assisted, and flat-fan spray cones are about two-thirds as effective as hollow-cone nozzles. The least effective were venturi nozzles designed for moving air. The most significant advantage of hollow-cone nozzles over other nozzles tested is reduced clogging due to larger orifice size. The hollow-cone nozzle used in the test and depicted by the graph was type BD-3 manufactured by Spraying Systems Co., Wheaton, IL. This nozzle is already used on many continuous miners. Other hollow-cone nozzles of

Jan 1, 1982

By H. B. Carroll

The Bureau of Mines investigated the adaptability of the Meteorology Research Inc.2 (MRI) nephelometer and the Sinclair-Phoenix smoke meter for use in routine, analytical, smog-chamber experiments and to compare their responses to aerosol during these experiments. Both instruments' sampling systems were modified--smaller size sample input systems were studied using the nephelometer and a secondary sample system was added to the smoke meter to allow measurement of Aitken or condensate nuclei. Both instruments were easily adapted for use with small smog chambers and both displayed good precision and sensitivity to aerosol. A correlation was shown to exist between the two instruments' responses to aerosol. This correlation makes it possible to report the Sinclair-Phoenix measurements in visibility and/or mass units if desired.

Jan 1, 1973