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By W. Mostowitsch, H. O. Hofman

The mineral gypsum, CaSO4 + 2 H2O, has been used for many years as a sulphurizing and basic flux in several smelting-operations. Thus, in smelting oxide nickel-ore in the blastfurnace, it is commonly added to the charge to furnish the sulphur necessary for collecting the metal in a matte, and a base for slagging the siliceous gangue. In the concentration of lead-copper matte in the reverberatory furnace it has been used for years at Preiberg, Saxony,1 for a similar purpose, and for producing at the same time a copper-matte with less than 0.15 per cent. of Fe. The latest use gypsum has been put to is in the blast-roasting process of Carmichael-Bradford.2 The term " blast-roasting," given by A. S. Dwight3 to the Dwight-Lloyd method of roasting and agglomerating: is a happy generic term which covers the ground better than the " lime-roasting " of Ingalls5 or the " pot-roasting " of Austin: in that it leaves the operation independent of the character of the flux and the form of apparatus, and retains the characteristic feature of this class of processes—namely, that of using forced draft. In the Carmichael-Bradford process the dehydrated material, mixed with galena-concentrate, acts as a diluent and a flux. The process differs in this from the Huntington-Heberlein7 and the Savelsberg8 processes, in both of which limestone is used.

Jan 1, 1909

By Wolfgang Pietsch

Pressure agglomeration using tableting machines, roll presses, punch presses, isostatic pressing equipment, extrusion presses, and other less common equipment, represents a large share among commercial applications of size enlargement by agglomeration. The paper attempts to classify and describe the equipment and technology, their development and state of the art, as well as their respective applications, advantages, and disadvantages.

Jan 1, 1977

These pages may be used as order sheets. Mark the number desired opposite title of pamphlet wanted, add your name and address, tear out the sheets and mail them to us. Single orders 25 c. Pamphlets 10 c. each in lots of three or more. Pamphlets 5 c. each in lots of fifty or more. These prices prevail for orders for pamphlets of the same or different titles, when cash accompanies order. The pamphlets listed on the following sheets are advance copies printed to facilitate discussion at the meetings of the Institute. They are offered for sale at the reduced prices given above as long, as the supply lasts. This list is published in the Bulletin in order that members may have the first opportunity to secure pamphlets, which sometimes are in such great demand that the supply is exhausted before the wants of members can be supplied. The following list includes only a fraction of the pamphlets-that have been published by the Institute. Any other paper published by. the Institute may be obtained for the price of $1, except those published in Volume XXXI, which are rare. The, Institute is still selling back volumes of Transactions at reduced prices, but some of these volumes are becoming rare. and members who desire to complete their sets of these very important books on mining and metallurgy are advised to send in their orders as soon as convenient. The attention of members is also called to the bibliographical index of the science of ore deposits contained in the Emmons Volume which is selling at $3 in paper and $4 in half morocco. The Posepny Volume is already exhausted and members who do not get in their orders for the Emmons Volume at the present reduced price may soon find themselves unable to obtain it on such favorable terms.

Jan 7, 1917

By Hjalmer Sjögren

AMONG the feldspar-rocks there are certain types which occur constantly in different areas-viz., the aruphibolitic plagioclase- rocks and the granulitic rocks Composed of quartz and alkaline feldspars. Among the latter soda: granulites as well as potash are met with; also the corresponding gneisses occur. GROUP I.-THE ORES OF THE ARCHEAN CRYSTALLINE SCHISTS. The Rocks. The ore-bearing rocks of the ore-province of central Sweden are chemically and petrographically unlike the more monotonous gneiss- and granite-areas which surround them. On the whole, they constitute a quartz-feldspar formation in which purer quartzitic rocks, limestones, " skarn " rocks, and ore-bodies are very subordinate members. (Skarn is the Swedish name for rocks of varying composition, mostly consisting of lime, magnesia, iron, and alumina, silicates of the pyroxene, amphibole, and garnet groups; as secondary minerals, epidote, chlorite, biotite, and talc occur. The skarn is scarcely an independent rock but is connected with the ore-deposits. It is formed through an interchange between the silica of the quartz-feldspar rocks and the basic constituents of the ore-formation.) [A BRIDGED SUMMARY.-The amphibolites must be considered as stretched and dynamo-metamorphosed dioritic rocks. The granulites are divided into two groups, one showing predominant plagioclase, the other equal or predominant orthoclase. Evidently, the iron-ore deposits are connected in some way with the

Jan 1, 1913

By C. R. Johnson, R. A. Greenkorn, E. G. Woods

A new method of reservoir evaluation called pulse-testins has been developed for describing formation properties between wells. Pulse-testing utilizes a sensitive differential-pressure gauge at a responding well to measure and record the response generated by a series of flow rate changes (pulses) at an adjacent or pulsing well. Since the pulse-test instruments have a sensitivity of about 0.001 psi, pulses of several hours or less in duration will generate a measurable response in most reservoirs. For this reason, many well pairs can be tested in a short period of time with little interference in field operations. Comparison of pulse-test results to conventional testing methods shows that the pulses obey unsteady-state, compressible-flow theory and thus provide a measure of both transmissibility (kh/µ) and storage (Fch). In additian, the method can be used qualitatively to describe communication across faults and between zones, and direction and tnagnitude of fracture trends. INTRODUCTION To obtain maximum usefulness of new reservoir analysis methods as well as to aid the field engineer in understanding local reservoir anomalies, improved methods are needed to describe heterogeneities in specific reservoirs. Optimum well spacing, equipment specifications, well completion design and especially the economics of pressure maintenance and secondary recovery programs depend on the extent and location of the heterogeneities that affect flow behavior in the field. One method for obtaining a measure of areal reservoir heterogeneity is an interference test. In the simplest interference test. constant-rate production or injection is initiated at one well and the effect of this flow is measured as pressure vs time at another well. Thus, during interference tests the flow characteristics of the formation are determined in situ. Despite their obvious usefulness in reservoir delineation. interference tests have not enjoyed frequent usage. Reasons for this have been the weeks or months required in many fields to obtain a pressure response measurable with conventional gauges, and the interruption of routine field operation during the field-wide shut-in normally required during these long times. Also, only average properties of the relatively large volume of the reservoir disturbed during these long times can normally be obtained — variations in properties between individual wells cannot be delineated. To eliminate these drawbacks of conventional tests, a special reservoir description technique called pulse testing' has been developed. Pulse-testing has several advantages that make it more convenient and practical for field use than interference tests. Valid tests are more certain because use of a series of flow disturbances gives rise to a diagnostic pressure response that can more readily be distinguished from unknown trends in reservoir pressure and other "noise." The time required is only a fraction of that for an interference test because a special, high-sensitivity differential pressure gauge can detect a much smaller pressure change. Variations in properties between individual wells can be delineated because of the relatively small volume of the reservoir disturbed during these short times. Finally, wells other than the pulsing and responding wells do not have to be shut in or carefully regulated.

Jan 1, 1967

By Donald E. Ackerman, Norman B. Pilling

The solubilities of a series of experimental alloys covering the range 0 to 100 per cent. Ni, 0 to 30 per cent. Cr have been studied under conditions of complete submersion in several fully aerated acid solutions, and in solutions containing sulfurous acid. In nonoxidizing, hydrogen-discharging acids, if the nickel content is below a certain critical amount, chromium increases the rate of solution and nickel decreases this rate; this critical content of nickel is about 13 per cent. Alloys containing more than this corrode at a constant minimum rate independent of iron, nickel or chromium contents. Austenitic chrome-nickel steels may thus have a resistance to these acids equal to that of nickel-chromium alloys. In nitric acid and in unaerated sulfurous acid rather sharp limits of attack occur which are principally dependent on chromium content. In the former the limit of attack is not related to a particular chromium content but varies continuously with acid concentration. The action of sulfurous acid on these alloys is highly dependent on the presence of small amounts of other substances in solution, and many sulfurous acid mixtures rapidly attack alloys to which the pure acid is wholly inert. The observed effects are not compatible with Tammann's theory relating corrosion resistance to lattice structure but are believed to be concordant with current views of the electrochemical nature of corrosion. Introduction The discovery, development and engineering application of iron alloys resistant to corrosion may well claim a place among the important developments in metallurgy of the past two decades. The varied demands of industry coupled with the skill of the metallurgist have resulted in the production of an extensive group of steels and alloys ranging from the now familiar "stainless " chromium steels of the kitchen to special alloys of great chemical complexity for particular, exacting needs. Any adequate description of the important properties of these-— physical, chemical and economic—would be a formidable undertaking.

Jan 1, 1929

By Donald E. Ackerman, Norman B. Pilling

The solubilities of a series of experimental alloys covering the range 0 to 100 per cent. Ni, 0 to 30 per cent. Cr have been studied under conditions of complete submersion in several fully aerated acid solutions, and in solutions containing sulfurous acid. In nonoxidizing, hydrogen-discharging acids, if the nickel content is below a certain critical amount, chromium increases the rate of solution and nickel decreases this rate; this critical content of nickel is about 13 per cent. Alloys containing more than this corrode at a constant minimum rate independent of iron, nickel or chromium contents. Austenitic chrome-nickel steels may thus have a resistance to these acids equal to that of nickel-chromium alloys. In nitric acid and in unaerated sulfurous acid rather sharp limits of attack occur which are principally dependent on chromium content. In the former the limit of attack is not related to a particular chromium content but varies continuously with acid concentration. The action of sulfurous acid on these alloys is highly dependent on the presence of small amounts of other substances in solution, and many sulfurous acid mixtures rapidly attack alloys to which the pure acid is wholly inert. The observed effects are not compatible with Tammann's theory relating corrosion resistance to lattice structure but are believed to be concordant with current views of the electrochemical nature of corrosion. Introduction The discovery, development and engineering application of iron alloys resistant to corrosion may well claim a place among the important developments in metallurgy of the past two decades. The varied demands of industry coupled with the skill of the metallurgist have resulted in the production of an extensive group of steels and alloys ranging from the now familiar "stainless " chromium steels of the kitchen to special alloys of great chemical complexity for particular, exacting needs. Any adequate description of the important properties of these-— physical, chemical and economic—would be a formidable undertaking.

Jan 1, 1929

By C. L. Mantell

Although so common and well known a metal, tin is really a less abundant element than many of those less familiar and usually ranked with the scarce or rare elements, such as cerium, yttrium, lithium, beryllium, titanium, zirconium and vanadium. The color of tin is white, with a slightly bluish tinge. When it is compared with nickel, the latter metal is brown. When placed alongside of tin, chromium is definitely blue. Tin is whiter than silver or zinc. Exceedingly thin films of tin show various shades of brown by transmitted light. The metal has a brilliant luster, and when mirror-polished, has high light reflectivity. The luster depends to a large extent upon the pouring temperature at which the metal is cast. If the temperature be too high, iridescent colors may show on the surface. These are the result of oxide film formation. If the pouring temperature be too low, the surface is dull. Small amounts of foreign metals, such as lead, arsenic, antimony and iron, decrease the luster of tin and impart a yellowish tinge to the metal. The structure is decidedly crystalline. The cast metal is a mass of crystals. When a bar of tin is bent, it emits a characteristic creaking sound. This is called the "cry" of tin, resulting from the grinding of the crystals one against the other during the bending of the metal. Tin metal may lose its crystalline structure by cold working, but grain growth occurs rapidly under the influence of heat. Metal which has been cast at a low temperature may become amorphous as the result of mechanical work. If such material be heated to temperatures well below the melting point, say at 110° C. for a half hour or for a few minutes at 150" C. recrystallization occurs. If the surface of tinned plate, tin foil, or tin meta1 in cast form be etched with hydrochloric acid containing a little free chlorine, attack occurs at the intererystalline faces. The surface shows patterns resembling the frost flowers on window panes in winter. The etched appearance is called moire metallique. Fine dendritic surface crystals of tin may be obtained by casting the metal on a surface of polished steel. In commercial tin plate, the intercrystalline boundaries are shown by fine grooves or channels, .which result from the method

Jan 1, 1929

By C. L. Mantell

Although so common and well known a metal, tin is really a less abundant element than many of those less familiar and usually ranked with the scarce or rare elements, such as cerium, yttrium, lithium, beryllium, titanium, zirconium and vanadium. The color of tin is white, with a slightly bluish tinge. When it is compared with nickel, the latter metal is brown. When placed alongside of tin, chromium is definitely blue. Tin is whiter than silver or zinc. Exceedingly thin films of tin show various shades of brown by transmitted light. The metal has a brilliant luster, and when mirror-polished, has high light reflectivity. The luster depends to a large extent upon the pouring temperature at which the metal is cast. If the temperature be too high, iridescent colors may show on the surface. These are the result of oxide film formation. If the pouring temperature be too low, the surface is dull. Small amounts of foreign metals, such as lead, arsenic, antimony and iron, decrease the luster of tin and impart a yellowish tinge to the metal. The structure is decidedly crystalline. The cast metal is a mass of crystals. When a bar of tin is bent, it emits a characteristic creaking sound. This is called the "cry" of tin, resulting from the grinding of the crystals one against the other during the bending of the metal. Tin metal may lose its crystalline structure by cold working, but grain growth occurs rapidly under the influence of heat. Metal which has been cast at a low temperature may become amorphous as the result of mechanical work. If such material be heated to temperatures well below the melting point, say at 110° C. for a half hour or for a few minutes at 150" C. recrystallization occurs. If the surface of tinned plate, tin foil, or tin meta1 in cast form be etched with hydrochloric acid containing a little free chlorine, attack occurs at the intererystalline faces. The surface shows patterns resembling the frost flowers on window panes in winter. The etched appearance is called moire metallique. Fine dendritic surface crystals of tin may be obtained by casting the metal on a surface of polished steel. In commercial tin plate, the intercrystalline boundaries are shown by fine grooves or channels, .which result from the method

Jan 1, 1929

By H. C. George

THE Wisconsin. Zinc District, or the Upper Mississippi Lead and Zinc District as it is often called, lies in the southwestern corner of Wisconsin, in, Grant, Iowa and Lafayette Counties, and it includes adjoining parts of Illinois and Iowa. The district is about 70 miles long, north and south, and about 40 miles wide, east and west. It lies wholly within what is geologically known as the non-glaciated area of the Upper Mississippi Valley. HISTORY OF THE DISTRICT The district was first opened up as a lead producer in 1822. From this time until 1860, about 205,000 tons of cog lead (galena) and washed lead (galena) was produced from shallow crevices and openings. From 1860 to 1900, about 74,500 tons was produced, and since that time, from 5000 to 7000 tons has been produced annually. Since-1900, most of the lead concentrate produced has been as a byproduct of the zinc mines. The first zinc ores were mined about 1862. These were the carbonate ores, locally known as " drybone." Very little zinc blende was mined in the district, previous to 1875. The zinc blende ores mined from 1875 to 1900 were mostly of the high-grade, hand-cobbed, sheet-ore class, which usually contained from 45 to 60 per cent. metallic zinc. Such nines as the "Sallie Waters," ? Quinlin," "Lead Mine," "Benton Blende" and "Ida Blende," located near Benton, Wis., were mines which produced ores of this type, during this period. The mines located at Highland, the "Coker Mine" located at Livingston, Wis., and the "Opencut Mine" located at Shullsburg, Wis., were mines that were heavy zinc carbonate producers, previous to 1900.

Jan 12, 1917

By Richard L. Coleman

Metallurgical testwork to develop a flowsheet is described, beginning with background information required right through to a final process flowsheet. Both laboratory and pilot plant testing are reviewed with emphasis on the former.

Jan 1, 1978

By Robert Glass Cleland

THE CONNECTING link between Phelps Dodge and the copper mines at Bisbee and Morenci was a Canadian-born mining engineer and metallurgist named James Douglas. Judged by almost any standard, Douglas was an extraordinary man. Like John Muir of the California red- woods, he had in his blood "the heather and bog juices of Scotland," and the rugged virtues of a singularly great race. His father, for whom he was named, was a graduate of Edinburgh University, a member of the Royal College of Surgeons in London, and a man of rash and adventurous spirit. Extremely catholic in his intellectual interests and attainments, he was unusually skilled in his profession, certain-sometimes to the point of disastrous stubbornness--of his own judgments and decisions, careless of life or fortune where duty or moral issues were involved, and always deeply moved by the sufferings and misfortunes of his fellow men. The career of the senior Douglas included a curious medley of novel and adventurous experiences-prolonged hunger and cold while acting as surgeon on a Greenland

Jan 1, 1952

By W. R. Hibbard

Pole figures, torque curves, and coercive force have been determined for the following rolled and annealed permanent magnet alloys: Cunife, Cunico, Silmanal, Vicalloy I, Vicalloy II, and Heusler's Alloy. IN the general category of precipitation-type permanent magnet alloys there is a group of ductile alloys, including Cunife, Cunico, Silmanal, Heusler's Alloy and Vicalloy, which can be extensively rolled and annealed to develop a preferred orientation in the crystals of the matrix material. The rolling and annealing textures of Cunifel and Vicalloy' have been previously investigated qualitatively, but no pole figures are available in the literature. In addition, the role of precipitation in these permanent magnet alloys is still somewhat controversial. It

Jan 1, 1957

By Paul A. Farrar, Louis P. Stone, Harold Margolin

The Ti-Mo-0 system was investigated in the region 0 to 45 wt pet Mo and 0 to 10 wt pet 0, from 600° to 1400°C. Solidus data are also presented. Isothermal sections at 700°, 900°, 1100°, and 1300°C, and vertical sections at 1 and 28 wt pet Mo, and 1 and 10 wt pet 0 are included. STUDY of the Ti-Mo-0 system has been carried out as part of a general study of titanium phase diagrams. The binary Ti-Mo system has been investigated in whole or in part by several investigators.1-8 It was found that molybdenum and ß-tita-nium form a complete series of solid solutions and that the ß/a + ß transus is depressed to below 600°C at approximately 30 pet Mo.* The Ti-O system has been investigated partially or fully in the range 0 to 30 pet 0 by several investigators." Extensive solubility of oxygen occurs in the field. While a is

Jan 1, 1957

GENTLEMEN: Submitted herewith are the report of the Treasurer for the year 1940 and reports for the same year of the following standing committees: Admissions, Membership, Pa¬pers and Publications, Mining and Metal¬lurgy (Magazine), Library, and Student Relations. These reports present additional details. MEMBERSHIP For the third year in succession member¬ship reached a new high level for all time, as indicated in the accompanying tabula¬tion in which "Members" includes all categories except Student Associates.

Jan 1, 1941

By B. L. Landrum, P. B. Crawford

The rise of a new laboratory model for studying tran-sient fluid flow problems, is described. The theory of he model is based on the analogy between the equa-ions which describe the flow of compressible fluids in porous media and the conduction of heal m solids. The "thermal model" is used to study the Iransient Pressure distributions during fluid displacement in five Standard well patterns. The studies indicate quantita-ively how die pressures change with lane at any poit in the reservoir. It was found that, in general, the equipressure contours are more radial about the wells early in the program than after steady-state conditions are established. In addition two studies of fractured five-spot patterns are presented to illustrate the opplicability of the model for a wide range of reservoir conditions. INTRODUCTION In reviewing the oil recovery techniques involving fluid displacement it was found that a very considerable quantity, if not all of the fluid within the pattern, mav be displaced (during a time-dependent or transient period rather than the usually applied steady-state conditions. Since the oil is displaced during a transient period, it was believed desirable to study the nature of the transients for several of the commonly used fluid displacement patterns. A literature review indicated fairly complete studies of the streamlines and isopotentials for steady-state: yet few data were available on the transient displacement process. Several simulated steady-state multiwell displacement programs were carefully mapped by Foster and Lodge on an electrical conducting sheet as early as 1875, hut the more recent work of Muskat provides the best source for steady-state phenomena having direct petroleum production applications. In order to study the transient phenomena a new lab-oratory model was developed which is based on the similarity of the equations that describe the flow of fluids and the conduction of heal. The equations describing heat flow were developed early in the nineteenth century. Regorous solutions tor most transient problems are in gcneral complex and usually limited to fairly restricted houndary conditions.2 the thermal model may be used to obtain approximate solutions for many transient problems without some of the restrictions required for analytical solution. The application of the analogy between heat conduc-. tion in solids. electrical flow and fluid flow, in a porous media has long been recognised. Techniques originally developed for the solution of heat conduction prol?lems have in many instances proved useful in ohtaining solutions to fluid flow prohlcms. Ir is not surpri5ing then that a heat conduction or thermal model might bf usefull in sludying transient fluid flow. As an example ol the problems suitable for the study with the thermal model, transient pressure distributions during fluid displacement programs are studied for the five-spot, line-drive, staggered line-diibe. seven-spot 211 two fractured patterns. A model was constructed of an iron plate of geometry similar to the reservoir patterns under study. The principle of mirror images as suggested by Bryan was employed in shaping the model. A temperature differential was obtained by soldering two sections of copper tubing to the plate at points analogous to the well location in the field. Hot and cold water was passed through the tubing. The temperature distribution, analogous to the pressure distribution in the field. was obtained a a function of time from thermocouplcs distributed over the plate.

By Laurence C. Hicks

Consideration of the past work on the subject of the diffusion of chromium into iron suggested that additional information might be given by the use of X-ray spectroscopy in following the concentration changes through the diffusion zone. Grube and Fleischbeinl packed rods of electrolytic iron in a mixture of alumina and chromium. These specimens were heated in an atmosphere of purified hydrogen for varying lengths of time. After treatment the specimens were examined metallographically and showed the usual structure, consisting of a border of radially oriented columnar grains ending in a sharp boundary line. Reference is made to the fact that etching with certain reagents will attack only the material inside the border of columnar growth and also to the fact that polishing seems to develop a ridge at the position of the boundary between the etched and unetched areas. By chemical analysis of thin layers turned off on a precision lathe, the authors were able to obtain depth-concentration curves. These curves, reproduced in Fig. 1, show that in most cases a pronounced change of slope occurs, corresponding to the position of the boundary of the columnar grains. In a laler paper Grube extends his work to other systems which show the same characteristics.~ He concludes that the reason for the break in the curve is that a hindrance of diffusion occurs at the place where the regularly oriented grains of the diffusion zone meet the random grains of the interior portion, on the assumption that the diffusion velocity in one direction in a grain may be greater than in another direction, and that the grains in the diffusion zone orient themselves so as to give the maximum diffusion rate. Kel1ey" points out that Grube has failed to note that the boundary line does not consistently cross all grains and

Jan 1, 1934

C. W. GENNET, JR.,* Chicago, 111. (written discussion?).-Since the Lehigh Valley accident, transverse fissures have become a source of constant anxiety to railroad officials, because such defects, only infrequently detected by the trackmen, may appear under a moving train entirely without warning. The number of actual accidents resulting from rails containing fissures is no doubt a small proportion of the total, but the serious losses that have been directly attributable to fissures, coupled with the continual possibility of repetition, creates an alarming situation which demands a full investigation of the cause of fissures; apart from other types of rail failures. Mr. Howard's position gives him a field for action and an opportunity for laboratory examination and research that are unsurpassed, and the results. of his investigations must be received with the utmost attention and respect. His admirable paper, summarizing his previously published studies and analyses of the transverse fissure problem, constitutes a convincing treatment of the subject chiefly from the standpoint of stress and strain to which rails are subjected. The intricacies of the problem are so great that seemingly any theory advanced for the cause of fissures may be attacked from some angle; and although Mr. Howard's deductions are logical in the direction followed, it is apparently necessary for considerable work to be done along other lines before his theories can be fully accepted. It is generally conceded that fissures, whether fundamentally clue to fatigue or something else, are of a progressive character, their ultimate size' being the result of growth from an originating nucleus or point of rupture. Abundant proof of this lies in the variable sizes of the fissures found, and there can be no doubt that their development or growth is the result of the strains to which rails are subjected in the track. Obviously, therefore, the most important factor in investigating the cause for fissures lies in determining the conditions that exist at the point or

Jan 4, 1918

By M. H. Forester, John D. Cooner

ALTHOUGH the unmined anthracite will last for approximately 150 years, most of the thicker and cleaner coal beds have been almost entirely first-mined and pretty well robbed, leaving much of the present and future production to come from thin and dirtier beds. Herewith is a section of one of the dirty beds being mined in the Wyoming region [ ] This section shows that 45.8 per cent of the bed is made up of impurities and that the 45 in. of coal in the bed is in five benches, the thickest of which is 19 in. In some localities of the anthracite region there are 14 beds of minable coal. Orderly and proper mining of the coal makes it necessary to rob or second-mine--almost all beds have already been first-mined-in sequence from the top downward. Therefore the robbing of the few remaining portions of the thicker and cleaner beds is in many instances being held up by the mining of the overlying thin and dirtier coal beds. Impurities Impurities consist of fire clay, slate, rock, and bone. The latter, which is black, contains 40 to 60 per cent carbon and often resembles good coal. In some beds there are also bands of "blue" coal, which, as the name implies,

Jan 1, 1950

By R. L. Stegman, M. R. Achter

Nickel, fatigued in vacuum, shows intragranular crack initiation and growth at low temperatures. An increase in temperature initially prolongs fatigue life due to a more homogeneous distribution of slip. With a further temperature increase, the mode of failure undergoes a transitiotz to intergranular crack initiation with concurrent recrystallization which results in a shorter life. The transition temperature varies with bending strain and specimen purity. UNTIL recently, very little work has been done on the effect of temperature on the mechanism of fatigue and the resultant variation in fatigue life. Except for mild steel, where strain aging raises the strength at moderate temperature, fatigue lives had been shown to decrease with an increase in temperature. In their review article, Allen and Forrest' summarized the work of McCammon and Rosenberg and of Forrest and Mann on the fatigue of copper from -269" to 325°C. The fatigue life vs stress curves remained roughly parallel over this temperature range, the fatigue strength decreasing progressively with increasing temperature. When testing was done in vacuum, the present authors' found the results for nickel were different from those quoted above. Initially, the fatigue lives increased with temperature and then decreased as a grain boundary mode of failure was observed. The initial increase was attributed to a more homogeneous distribution of slip, a condition which was not as conducive to crack initiation as the bunching of slip lines observed at 20°C. Ronay, Reimann, and wood3 observed a similar change of slip line distribution in brass, tested in air, with rising temperature. Our previous observations were based on preliminary work with relatively few specimens, fatigued at comparatively low strains. To learn more about the mechanisms, the present investigation was undertaken for the purpose of studying systematically this effect over a wider range of strains and as a function of purity of the nickel. EXPERIMENTAL PROCEDURES The testing equipment, procedures, and specimen geometry have been described elsewhere.' An optical technique to measure bending strains was used as de-

Jan 1, 1968