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By W. H. Eddy

The Bureau of Mines conducted laboratory batch-and small-scale continuous flotation processing tests on waste granite fines from Georgia, to determine the feasibility of recovering usable feldspar and quartz products by flotation. Two flotation methods were utilized for the removal of biotite and other iron-bearing minerals: One was in an acid-cationic circuit, and the other in an alkaline-anionic-cationic circuit. Feldspar was recovered using an acid-cationic method. To produce commercial-grade feldspar and quartz products it was necessary to employ either two sequential froth flotation circuits or one froth flotation circuit supplemented by wet-magnetic separation techniques to remove iron contaminants. Continuous flotation processing yielded a commercial-grade feldspar concentrate containing, in percent, 3.8 Na20, 5.4 K20, and 1.10 CaO, with recoveries of 77.8, 70.3, and 64.4, respectively. The feldspar tailing was high-quality glass sand containing 98.2 percent SiO2 and 0.024 percent Fe2O3. About 42 percent of the quartz was recovered at glass sand specifications. An effective separation of, potash feldspar from the bulk feldspar concentrate was achieved by batch flotation in a mineral separation cell.

Jan 1, 1974

By F. S. Crawford

Untreated timber in a mine or elsewhere may fail prematurely because it may "rot out before it wears out." If such timber is treated with a satisfactory preservative, decay will be retarded for many years, and it's serviceable life will beg prolonged to several times that usually obtained from untreated timber.4/ Treated timber has many advantages, and although it has been used extensively by railroads and other large consumers of structural timber, the relatively small use in mines seems strange indeed. Timber does not decay if it is kept dry, cool, and well-ventilated or if it is kept constantly wet or sumberged in water. At a mine in Canada the temperature in the upper levels was only 44° F., and the timber did not decay. As operations deepened, however, warmer ground was opened, and, with high humidity, conditions favored timber decay. The life of untreated timber may be only 2 to 3 years under such conditions.

Jan 1, 1951

Lower costs associated with hands-on training in donning and using a CSE ,self-contained self-rescuer (SCSR). Background In June 1987, the Mine Safety and Heath Administration (MSHA) issued an Emergency Temporary Standard (ETS) requiring that all persons entering underground coal mines must be given bands-on SCSR training. The ETS will shortly be replaced by a new standard requiring this hands-on training. Bureau of Mines research has shown that the most effective means of delivering this training is to have the trainee go through a six-step training procedure while in a kneeling position. Once the miner has looped the neckstrap over his or her head, he or she completes the donning sequence in this order: 1) activate oxygen; 2) insert mouthpiece; 3) put on nose clips; 4) put on goggles; 5) adjust neck and waist straps; and 6) replace miner's cap and prepare to move out. This procedure is repeated until the miner demonstrates that he or she is proficient at the task.

Jan 1, 1988

By W. P. Yant

Public interest in atmospheric pollution by automobile exhaust gas and in the ventilation of vehicular tunnels makes it desirable to ascertain whether the use of modern automobile fuels is tending to change the amount and composition of the products of combustion. The Bureau of Mines, in cooperation with the Ethyl Gasoline corporation4, has completed a series of testis to determine whether any significant difference exists in the carbon monoxide content of the exhaust gas produced by an internal-combustion engine when its fuel is changed from straight gasoline to the same gasoline containing Ethyl fluid whose active ingredient is tetraethyl lead. In the tests data was sought relative to the composition and mount of the gas produced by ordinary comparatively low-compression motors as well as by higher-compression motors in which distinct detonation occurred with straight gasoline, but which operated without detonation when using the same gasoline containing tetraethyl lead.

Jan 1, 1929

By Anthony Iannacchione

One of the more pressing engineering problems for deep longwall mines in the Southern Appalachian Basin is to design longwall systems that will eliminate catastrophic coal pillar failure from the working environment. The purpose of this study is to quantify the behavior of a particular size abutment pillar prone to burst or bump. Because the 24.4-111 (80-ft) square abutment study pillar is within the pillar size commonly used in this region, understanding the behavior of this pillar should aid in future efforts to design optimum mining strategies. This research has attempted to construct the pillar stress and roof-to-floor convergence profiles in order to evaluate the ultimate strength, deformation modulus, visco-elastic deformation, and violent failure characteristics of the pillar during longwall mining. This information reflects the overriding influence of the local geologic characteristics on bursts, provides the field measurements needed to verify concurrent modeling studies, and suggest some basic mechanisms associated with the coal pillar bursts discussed in this paper.

By Frank D. Lamb

Pyrophyllite, a hydrous aluminum silicate (Al2 Si4O10 (OH)2 ) has been mined in North Carolina and marketed without beneficiation for the past 100 years, but recent demands for higher-grade material indicate that an economical concentration method is needed for at least a part of the pyrophyllite production. Past production has depended upon selective mining and hand sorting, which is often unsatisfactory because of the finely disseminated character of the ores. The major impurity in North Carolina pyrophyllite ores is quartz, which accounts for the abrasiveness of the commercial product. Since pyrophyllite is only slightly heavier than quartz, those ores cannot be beneficiated by simple gravity-concentration methods. Some separation can be attained by differential grinding and air classification because of the difference in hardness of the two minerals) but the separation is not sharp. Froth flotation of pyrophyllite from Quartz has never been attempted commercially, but if the demand for high-grade material is sufficient, it would seem that this process offers the most premise of being economically feasible.

Jan 1, 1950

By T. J. Ballard

"The Hog Creek mine, in lot 92 of the 17th district in Towns County, Georgia, was examined in 1890 by F. P. King, who reported the existence there of a 4-foot vein of corundum. The mine is about 2 miles west of Hiawassee, on the southern side of Ramey Mountain. Ed Burch, of Hog Creek, holds the surface rights, and the mineral rights appear to be vested in the heirs of William R. McConnell, who formerly owned and prospected the property.Examination by the Bureau of Mines showed the workings to be caved, but it was thought advisable to open the mine and uncover the reported vein. The Bureau's work consisted, of trenching and cleaning out the pits and shaft.William R. McConnell, the former owner, prospected the property in about 1890. At some tine during that operation, the prospect was visited by Francis P. Kings a geologist with the Georgia Geological Survey.3/King reported that a 4-foot vein of corundum was exposed g feet below the surface in the main cut and was opened for 20 feet along the strike. He also reported that the so-called ""Georgia rubies"" were taken from this mine.The main mine is about 2,000 feet- north of Hoc Creek on a timbered southern slope of Ramey Mountain. It lies at an altitude of about 2,100 feet, approximately 100 feet above the high-water level of the Catuga reservoir, which floods Hog Creek to a quarter of a mile above its confluence with the Hiawassee River. The nearest water is a small branch about 1,000 feet to the west.Chlorite schist is the principal host rock. It has been intruded by irregular masses of a very herd periodtite rock possibly troctolite. The schist near the surface is extremely weathered, presenting white and red laminations parallel to the schistosity. At a depth of 40 feet in the cross-cut it appears as a fine-grained green-chlorite schist. The schist strikes about N. 350 E. and dips 800 to the southeast.No corundum vein was found, and if any existed it must have been mined out after King's visit. In the pit, about 15 feet west of the shaft, approximately 150 pounds of zoisite and an occasiona1 small crystal of corundum were found imbedded in schist about 18 feet below the surface, near hard, dense troctolite."

Mar 1, 1946

Studies on coal mine drainage sludge densification have led to the following conclusions: 1. Coal mine waters containing iron principally in the ferrous (Fea+) state can be treated by a modification of the commonly practiced lime neutralization process to yield a ferromagnetic sludge. The sludge, presumably composed in large part of a hydrated ferrosoferric oxide (Fe304.xH20), is much denser and faster settling than the ordinary "yellowboy" sludge obtained by lime neutralization and aeration at ambient temperatures. 2. The magnetic sludge preparation technique involves (quantitative) precipitation of iron (largely as Fe(OH)2) by the addition of hydrated lime to a pH of 8.5, separation of the resulting sludge from the aqueous phase, and heating of the sludge concentrate to at least 80 C (176 F), preferably higher, followed by mild aeration. 3. Magnesium, present as Mg2 in most coal mine drainage waters, inhibits the formation of the magnetic sludge. This inhibition can be adequately minimized by keeping the pH below 9.6 during lime addition (thus avoiding the coprecipitation of Mg(OH)2) and by separating the sludge from the bulk of the aqueous phase before the heating step, as indicated in (2) above. 4. Aluminum, commonly present in coal mine drainage waters, also inhibits the formation of the magnetic sludge. This inhibition is of practical significance when the molar ratio of aluminum/total iron is greater than 0.18. Below this value, sludges are still appreciably magnetic, but are bulkier and slower settling than those obtained when aluminum is absent. Unlike magnesium inhibition, aluminum inhibition cannot be minimized by the scheme indicated above, since aluminum precipitates as Al(OH)3 near pH 4 and remains dispersed within the sludge. 5. The limitation on aluminum content is probably the most serious restriction affecting the feasibility of the magnetic sludge process as presently conceived. Nevertheless, a limited review of available water quality data has indicated that, in terms of relative acid and iron loadings, a significant number of major coal mine discharges in the eastern Ohio River basin may be amenable to treatment by a magnetic sludge process. 6. Data from tests on the use of magnetic seeding materials indicate that seeding did not enhance the formation of a magnetic sludge under the experimental conditions employed.

Jan 1, 1971

By L. C. IlsLey

The observations made by Bureau of Mines engineers of permissible equipment installed in about 40 mines have indicated a chance for improvement in designs calling for the use of bolts , screws , studs , etc. , especially with respect to bolt sizes and protection from mechanical injury .

May 1, 1931

By G. R. Palmer

The Bureau of mines evaluated the elution of uranyl carbonate from a strong base resin with a mixed carbonate eluant in a fluidized system. The system consisted of a multiple-compartment ion-exchange (MCIX) elution column with a continuous flow of solution, except for short periods when the resin increments were withdrawn. The exchange of uranyl carbonate from the mill-loaded strong base resin with an eluant composed of 1.0 [M] NaaCOs plus 1.0 [M] NH4HCO3 was studied. The effects of solution flow rate, aqueous-to-resin flow ratio, column diameter, compartment height, initial resin concentration, and column length were examined. The experimental data indicate that for the eluant examined, a resin residence time of 240 minutes is necessary to attain 90-percent elution efficiency. Also provided is a technique for sizing an elution MCIX column form pilot plant experimental data.

Jan 1, 1979

By J. M. Stuve

Calorimetric data for the dissolution of scandium sesquioxide and scandium trichloride in 4.360 molal hydrochloric acid were used to evaluate the standard heat of formation of ScCl3(c). The heat of reaction for Sc(c) + 1.5Cl2(g) = ScCl3(c) at 298.15° K was computed as -225,440 ±340 cal/mole.

Jan 1, 1965

By J. M. Stuve

Heat of solution measurements of high-purity neodymium metal and neodymium trichloride (NdCls) in 4.360 molal hydrochloric acid (HCI) were used to determine the standard heat of formation (6EPr) of NdCls? From solution data obtained, the heat of formation of NdCls (c) was computed as -248,970 ±260 cal/mole at 298.150 K.

Jan 1, 1965

By D. S. Kingery

The control of coal dust on coal tipples and cleaning plants has not been given the consideration that is afforded underground dust hazards. This apparent oversight is undoubtedly due to the general opinion that coal-dust accumulation in tipples or cleaning plants does not present the same type of hazard that it does underground. That this opinion is at least in part a fallacy has been proved many times, and the Bureau of Mines has on record many examples of explosions in tipples and cleaning plants.3/ In addition to this explosion hazard, coal dust is considered by sonic authorities to be injurious to the health of individuals exposed to it.4/ Obviously, it reduces visibility and contributes materially to accident hazards and the discomfort of the employees. Several companies have recognized this dust hazard and the advantages derived from controlling it; consequently, they have installed equipment to allay and control the dust on, their cleaning plants and tipples. The object of this paper is to. Summarize briefly some of the methods new in effect.

Jan 1, 1943

By Philip W. Holland

The U.S. Bureau of Mines has developed an improved method for determining dissolved helium in water in the concentration range of 4.0 x 10-8 to 270 X 10-8 cm3 He (STP)/cm3 H2O. The method is a modification of a previously reported method that was developed for analrzing surface and subsurface waters in geochemical survey work. Water samples are collected in SOD-cm stainless steel cylinders, and the dissolved gases in a sample are extracted into an evacuated cylinder of equal volume. After addition of 30 psig of nitrogen containing less than 2 ppb helium to the extracted gases, the resulting mixture is analyzed for helium using a helium-tuned mass spectrometer. The helium content of the water sample is determined from an empirical calibration that is established by analyzing standard solutions of helium in water. The accuracy of the method is ±7 pct for helium-in-water concentrations above 10 x 10-8 cm3 He (STP)/cm3 H2O.

Jan 1, 1989

By H. C. Ko

As part of the Bureau of Mines effort to provide thermodynamic data for the advancement of mineral technology, the standard enthalpies of formation for ZnO?2ZnSO4 and COS04-6H20 were determined by HC1 acid solution calorimetry. The values are -550.31 ±0.28 and -641.33 ±0.15 kcal/mot, respectively.

Jan 1, 1982

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

C. 4 Hoist Assemblies (not man-rated) A large number of manufacturers supply materials handling winches. These units are predominately electric powered while a limited number of vendors supply air powered equipment. Air powered units are currently used extensively for underground materials handling purposes. Suppliers of materials handling equipment normally include a disclaimer statement in their published literature which clearly states that the equipment "is not designed or suitable for lifting or lowering persons " This category of commercially available equipment can be adequate for emergency man hoisting provided that its' capacity is suitably derated and provided also that the necessary safety features are incorporated. Section C. 5 details the equipment which could be added to a commercial materials hoist to meet these needs. Four commercially available hoist assemblies, two electric and two pneumatic are discussed in the following paragraphs. This equipment is typical of what is commercially available and three of the units are currently used extensively in mining applications. Each hoist description includes a remarks paragraph which identifies the additional equipment each hoist would require for emergency hoist use.

Jan 1, 1976

By M. P. Ristenbatt, E. K. Holland-Moritz, K. Metzger

A new post-disaster signalling system for the Bureau o Mines, using through-the-earth EM propagation, was successfully field-tested in the Lake Lynn test mine. Successful detection at an estimated input SNR of -30dB was accomplished using a coherent integration time of 4.46 minutes. The transmitted waveform consisted of a repeating pseudonoise maximal length sequence phase modulating a 1950Hz carrier. The receiver used a sliding-window matched filter, optimal for signal known exactly except for phase and starting time, implemented via a special purpose processor. Parallel processing permits adaptive signalling, where the detection (integration) time is determined by the actual input SNR encountered. This field test demonstrates a trapped miner detection system that is about 36dB more sensitive than a current pulsed system. This increased sensitivity permits some desired combination of increased range, shorter detection time, and reduced transmitter power or antenna-size. The combination of pulse-compression-type-signal, coherent integration, parallel-processing, and output peak-detection algorithms permit implemention of an ultra-reliable detection system. The same combination is compatible with digital Pulse Position Modulation and Emitter position location strategies.

Jan 12, 1983

By M. R. Geer

The ever-increasing need to guard against stream pollution has intensified interest in the problems of handling and disposing of flotation tailing. Therefore, the Bureau of Mines investigated the possibility of using crushed washery refuse to adsorb the free water in thickened flotation tailings on a bench scale and then in a pilot plant because the conventional methods of disposing of coal flotation tailings--impounding them or filtering them so they are dry enough to be conveyed to the refuse dump--are sometimes either impractical because of space limitations or costly because of low filter capacity. Most of the refuse samples tested were of similar mineralogical composition and exhibited similar water retention capability. The amount of crushed refuse required to adsorb the water in a particular tailing was influenced greatly by the fineness of the solids in the tailing and hence the percentage of solids to which it could be thickened. The ratio of crushed refuse to tailing solids required to provide a mixture dry enough to be carried on an inclined conveyor belt varied from 2.4 to 6.4. Several chemical agents that were tested were very effective in turning the free water in tailings into a stable gel. Fly ash also was very effective in adsorbing water.

Jan 1, 1968

By Robert B. Schluter

The Bureau of Mines investigated separating copper-nickel mattes to recover a copper-rich fraction suitable for processing by conventional copper metallurgical processes and a nickel-rich fraction suitable for processing in a hydrometallurgical nickel circuit. Distribution of cobalt and precious metals between the copper and nickel fractions was also determined. A matte containing a nominal 65 pct Cu, 9 pct Ni, 4 pct Fe, and 20 pct S was separated into a copper fraction that comprised 80 pct of the matte weight and contained 70 pct Cu and <1.5 pct Ni, plus a nickel fraction that contained 40 pct Ni and 30 pct Cu. Recoveries of copper and nickel into their respective fractions were 90 pct and 87 pct. These results were obtained in a laboratory flotation cell at a matte grind of 90 pct minus 500 mesh and a pH of 12.4, using 1.7 pounds DPG (diphenylguanidine) per ton of matte as collector and frother. Magnetic separation was used to remove metallic iron-nickel alloy from the copper fractions. Distribution of cobalt was about 70 pct to the nickel fraction and 30 pct to the copper fraction. Silver reported predominately to the copper fraction, while Au, Pt, and Pd were essentially entirely recovered in the nickel fraction.

Jan 1, 1982

By A. L. Murray, D. Harrington

From 1870 to the end of 1929 the coal production of Utah has been some- what less than 110,000,000 tons. During this period at least three major disasters have occurred with fatalities totaling about 380, establishing a decidedly bad record of approximately 3.5 persons killed by major mine explo- sions per million tons of coal produced. Even during the period when there have been no disasters, such as the years 1914 to 1920, inclusive, the fatalities in ordinary working were about 5.4 per million tons produced, against 3.7 per million tons for the whole United States for the same years. The 5-year period following the World War, 1918 to 1922, inclusive, had 4.7 fatalities per million tons; hence, the fatality record in the coal mines of Utah has uniformly been in excess of the average of the coal mines of the entire country. Notwithstanding this poor record, Utah has given to the coal-mining world many excellent safety methods and practices, and Utah coal mines in general take greater measures toward safe mining than do the coal mines of any other State; if practices and methods allowed and pursued in coal mines of other States were tried in Utah coal mines, there would be a succession of disasters.

Nov 1, 1931