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By W. K. Collins

Engineered scavenger compounds (ESC's) developed by the U.S. Bureau of Mines are a novel class of compounds that selectively can recover a desired element from a solid or molten alloy. Lithium titanate (L2Ti307 or Li2O?3Ti02) is used as an ESC to recover lithium (Li) from aluminum-lithium (Al-Li) alloys. X-ray diffraction measurements have shown that Li2Ti307 undergoes a phase change during scavenging from an orthorhombic structure to a hexagonal structure. This change is due to the incorporation of lithium in the matrix of the material and the effect of temperature. Although both phases are metastable, the hexagonal phase that forms during the scavenging of lithium from Al-Li alloys appears to be the more stable phase. Recovering lithium from the ESC by electrodeposition does not cause the structure to revert to the orthorhombic phase. The orthorhombic and the hexagonal structures of Li2Ti307 have similar scavenging capacities for lithium. This report proposes a new mechanism for the phase transformation.

Jan 1, 2010

By R. R. Wells, G. M. Potter, A. O. Ipsen

This paper gives results of laboratory and pilot - plant investigations of concentration of western manganese ores during the Bureau of mines manganese-development program initiated in December 1940. The data summarize results obtained from laboratory investigation of concentration of ores from three properties in southeastern Arizona . The high - grade Gray - claims lot B ore , a product of hand sorting , is marketable directly or after sintering treatment . Intermediate - grade lot A selectively mined ore would be marketable after sintering as a plus 35 percent manganese produce , but gravity concentration methods were employed effectively to produce high - grade manganese concentrates with over 80 percent recoveries . Complex association of fine - grained manganese oxides , calcite , and fluorite in a siliceous ground mass limited the recovery of high-grade manganese concentrates obtainable from the low-grade Pyrolusite -group ore . A recovery of 63.7 percent of the manganese was made by flotation in a concentrate that sintered to plus 48 percent manganese grade . The low-grade Davis ore contains iron and manganese oxides too intimately associated to permit production of marketable manganese products . However , good rejection of calcite gangue was obtained by flotation , and the enriched manganese - iron product might have value as a spiegeleisen ore .

Feb 1, 1946

By Wm. W. Adell

"These hydrocarbons belonging to the same chemical series as methane, having the general formula CnH2n have many chemical properties in common with methane and their addition to a lean gas charges the properties and burning characteristics of the gas in the same general direction although to a different extent. The hydrocarbons of this series do not readily enter into chemical reaction with other substances and therefore are incapable of combining with oxygen or polymerizing in the disturbing system and thus cannot cause gum and room troubles commonly met with in the distribution of manufactured gas.As the number of carbon atoms in the molecule increases, i.e. in proceeding from methane throughout the series, the oxygen requirements for the complete combustion of unit volume of the gases also increases; in other words, the calorific values of these hydrocarbons (as gases) increases from methane. Similarly the specific gravity increases from methane in the same order. In Table 1 are shown some of the physical constants and properties of a few of these hydrocarbons which hive bearing on their use for enriching gas."

Nov 1, 1927

By Secretary of the Interior

"INTRODUCTION The Bureau of Mines Synthetic Liquid Fuels Program again forged ahead during 1952, and important technical advances led the way to improved methods of converting coal and oil shale into liquid fuels. Marking the eighth year of activities under this program, the past 12 months brought a new domestic industry nearer realization.The increasing demand for gasoline and oil and the rising cost of finding new petroleum, coupled with America's growing dependence on imports and the unsettled international situation, have continued emphasize the importance of the Bureau's Synthetic Liquid Fuels Program. Oil, the indispensable material of wartime, likewise has critical importance in peacetime, touching as it does the life of every individual. Supplementing petroleum with synthetic liquid fuels will not only conserve this Nation's petroleum reserves but also will bring into greater use its tremendous reserves of coal, as well as the vast deposits of oil shale for which no other practical use has yet been found.The Bureau of Mines Synthetic Liquid Fuels Program is one of the most important and far-reaching of the Government's research projects. Through development, of commercial synthetic liquid fuels, the United States can obtain oil products from its great inland reserves of coal and oil shale to supplement petroleum in any quantity that may be necessary, consistent with economic and other requirements, such as national defense. The use of raw materials from such deposits would be of highest importance in wartime, when shipping lanes are menaced by the enemy. The Synthetic Liquid Fuels Program of the Bureau of Mines and research efforts of industry have advanced American technology to the point where it is now possible to begin the design and construction of prototype plants. Certainly, significant improvements will be made as the program continues, but this prospect in no way alters the fact that the start of prototype plants should be encouraged. These plants, as the first step in the development of a synthetic fuels industry, would serve a threefold purpose:"

Jan 1, 1953

By F. S. Crawford

It has been said that safety promotion passes through four stages--the band-playing, the machine-guarding, the protective equipment, and finally the educational stage; the last is the most important in the development of the safety program. It has been estimated that only 15 percent of accidents can be pre- vented by machine guarding and protective equipment; the other 85 percent must be stopped by the safety efforts of the individual workers and their supervisory officials, and one of the fundamentals of safety work is the education of workers to develop safety consciousness or safety mindedness. One way of educating men to think about safety is by the use of posters. Safety engineers at the Calumet 2 Hecla mines in Michigan have been conduct- ing a safety contest among the men by the use of posters of an unusual type in addition to those usually employed to illustrate bad practices and to display the number of days without a lost-time accident. The first requisite for the success of the safety poster is a good artist or draftsman; in the poster contest instituted at the Calumet & Hecla mines two sheets were prepared illustrating various conditions in the slope workings, including a large number of unsafe practices. The object of the contest was to get the men to think about safety through criticism of the unsafe conditions displayed on the posters. The following notice accom- panied the posters:

Feb 1, 1935

By Robert W. Freedman

As part of a continuing effort to reduce the weight and bulk of equipment that mining personnel must carry underground, the Bureau of Mines and the Mining Enforcement and Safety Administration (MESA) investigated accurate and convenient gas samplers for use by mine inspectors in sampling mine atmospheres. The samplers are septum-stoppered glass vials commonly used for routine blood sampling. These lightweight, compact samplers yield results comparable with those obtained with conventional bottle samplers of 250-ml nominal capacity.

Jan 1, 1975

By Ross. C. Barkley

A computer program has been written to simulate ground vibrations induced by multiple-hole surface blasts. The program is an inexpensive and relatively easy to use tool for predicting the principal blast vibration characteristics that determine damage and annoyance potential: peak particle velocity, frequency content and pulse duration. The program generates a complete ground motion history by superposing, at any surface position, the vibrations induced by each individual explosives charge. It requires specification of (hence allows accounting for) the blast geometry, initiation sequence (including random delays), position with respect to blast, pulse characteristics induced by each charge, and propagation laws. A methodology is outlined to determine the necessary variables either on the basis of site investigations (e.g. velocity, attenuation, pulse), or by backcalculation from measured blast vibration records. The latter procedure has been applied to blasts from two coal strip mines. Main difficulties are backcalculating individual pulses, propagation (especially dispersion) parameters and delays. A normal distribution of delays, based on published results, has been shown to influence the results and the response of a single degree of freedom structure significantly. Broadening of the wave types included and additional verifications with field results are required.

Jan 1, 1983

By J. W. Lyman

The U.S. Bureau of Mines investigated methods of separating valuable rare-earth materials from Fe in neodymium iron boron (NdFeB) magnet scrap. A selective oxidation treatment of the scrap oxidized the rare-earth portion while leaving elemental Fe. Magnetic and leaching procedures were tried for separating the metallic Fe and rare-earth oxides, but the extremely fine grain size of the oxidized scrap prevented recovery by either technique. The best separation of rare earths from bulk NdFeB magnet scrap was obtained by dissolution with H2S04 followed by precipitation of recyclable rare-earth salts. By precipitating neodymium-alkali sulfate double salts as an intermediate that can be converted to a variety of useful products, many materials-handling and economic disadvantages found with direct precipitation with fluoride or oxalate were avoided. Iron was removed from magnet leach solutions by precipitation as a jarosite, eliminating a major disposal problem. Research was also conducted with contaminated mixed SmCo5 and NdFeB swarf. Using a flotation-leaching technique allows the SmCo5 to concentrate in the froth, while the grinding-medium contaminant sinks and is removed as tailing. The NdFeB is dissolved by H2S04 during the process.

Jan 1, 2010

By James A. West

Near East region countries continued to supply a large share of the world's energy requirements in 1965. The area accounted for nearly 27 percent of estimated total world crude oil output and for about 60 percent of world exports of this commodity. Also, it was the source of more than 40 percent of the world's petroleum refinery products exports. Although other mineral industry activities remained relatively in? significant in comparison with petroleum, regional production and export of certain metallic and nonmetallic mineral commodities were of world significance. Of these commodities, chief in importance were chromium, copper, mercury, antimony, boron, potash, and phosphate Tack. The Near East region contains the largest and most productive oil resources in the world. Petroleum exploration and development operations during 1965 resulted in crude oil reserve additions of almost 8 billion barrels to increase proved reserves to 219 billion barrels at yearend, an amount equal to nearly 68.5 percent of the world's proved oil reserves. Near East countries' production of crude oil averaged a record 8.337,575 barrels per day in 1965, an increase of nearly 11 percent over that of 1964. On an annual basis, Kuwait continued as the leading oil producer in the Near East; however, Saudi Ayabia was a close second and its rate of production in late 1965 exceeded that of Kuwait. The major oil producing nations and their percentage of total area crude oil output was Kuwait, 26.0; Saudi Arabia 24.3; Iran, 22.3; and Iraq 15.9.

Jan 1, 1967

By Louis A. Turnbull, JOSEPH J. SHIELDS

The Bell & Zoller Coal & Mining Co. recently completed construction of two slopes at Mine 3 near Zeigler , Ill . The slopes are in the Big Muddy River Valley , and construction was particularly difficult because the strata from the surface to a depth of 70 feet comprise water saturated sandy clay and sand . Many mining companies have similar shaft- and slope - sinking problems , and because these slopes were satisfactorily completed and now are in use the methods followed during construction are described in this information circular . It is believed that other companies with similar problems . will benefit by adopting the methods followed at Mine 3 .

Apr 1, 1949

By J. D. Ramsdell

The object of this investigation by the Federal Bureau of Mines was to evaluate the workability, recrystallization characteristics, and mechanical and physical properties of high-purity electrorefined vanadium. The low level of interstitially soluble elements in electrorefined vanadium results in a soft ductile metal which responds readily to cold working by rolling, swaging, and press-forging. Hardness, strength, and resistivity increased with an increase in impurity content, but thermal expansion was independent of impurity content. The work-hardening of vanadium occurs rapidly. Most of the hardness increase occurs in the first 15 pct. of reduction in area. When vanadium is annealed, its hardness increases to a maximum when the annealing temperature is between 200° to 400° C. A sharp decrease in hardness develops as the annealing temperature is increased. An anomaly in the hardness versus annealing temperature curve is present in the 600° to 800° C. range, while all evidence of cold-work is removed at annealing temperatures above 900° C.

Jan 1, 1961

This report is the first in a "final" series of publications on the Juneau Mining District (JMD). This volume summarizes the results of Bureau of Mines (Bureau) investigations in the JMD during the period 1984-1988. Volume 2 consists of a detailed description of Bureau investigations of mineral de-posits, prospects, and occurrences. Volume 3 is a report on industrial minerals within the district. This study has identified and examined more than 300 mines, prospects, and occurrences containing gold, silver, copper, zinc, lead, nickel, cobalt, tungsten, molybdenum, chromium, and PGM. More than 20 of these were discovered during this study. An additional 20 prospects not mentioned in the literature were rediscovered during the JMD study.

Jan 1, 2012

By G. A. Savanick

The Bureau of Mines has designed, fabricated, and field tested a water jet cutting device capable of perforating nonmetallic well casings for the purpose of completing or stimulating in situ uranium leaching wells. The device is lowered into the wellbore, where it issues a high-velocity water jet that penetrates either a polyvinyl chloride or fiberglass casing, cement, and from 1 to 4 feet into the surrounding uraniferous sandstone. The resulting perforations allow leaching solution to pass between the sandstone and the wellbore. This report describes the water jet perforator, tells how it is used, presents cost data, and discusses the results of laboratory and field tests. The tests were designed to (1) determine the optimum operating conditions for water jet perforation, (2) assess the effects of changes in these conditions, (3) evaluate the performance of the water jet perforator under actual conditions, and (4) compare this method with other methods of well completion. These tests showed that water jet perforation is superior to conventional well completion methods for selectively achieving communication between the well-bore and adjacent sand while maintaining sand control, for restoring permeability lost through wellbore damage, for stimulating poorly performing wells for completing wells with casings that have inside diameters as small as 2 inches, and for extending the effective well diameter.

Jan 1, 1981

By K. B. Rojiani

Surface mining activities disturb large tracts of land resulting in the potential for greatly increased downstream sediment loads. The Surface Mining Control and Reclamation Act of 1977 places increased emphasis on the protection of the environment from the adverse effects of surface mining operations. Surface mining activities must be planned to minimize disturbance to the hydrologic balance, erosion and sediment contributions to receiving streams. Sediment ponds must provide a sediment storage volume equal to the accumulated sediment volume from the drainage area as determined by the Universal Soil Loss Equation (USLE) or other empirical methods established by the regulatory authority. It has thus become extremely important for the mining industry to secure more accurate estimates of potential erosion losses and sediment yield. Accurate estimates of sediment yield are required for the planning, design and successful operation of sediment control systems such as detention ponds and other alternative control structures and for evaluating the effectiveness of land management practices. The principal soil loss prediction procedure available for use is the LISLE. The USLE procedure is inadequate for use in predicting soil loss from surface mine regions for a number of reasons. These include: 1. The USLE was developed to estimate average average annual loss from agricultural soils. It cannot predict accurately soil loss for specific storm events. In surface mine regions a major portion of the soil loss occurs during the initial six months to one year of active mining. Accurate estimates of soil loss over short periods are thus required for the design of control structures. 2. The slope length and gradient factors used in the USLE were obtained from data or cropland having slopes ranging

Jan 1, 1983

By Edward L. McHugh

In 1984, at the request of the Bureau of Land Management, the U.S. Bureau of Mines studied an 84,165-acre portion of the 84,935-acre Clover Mountains Wilderness Study Area (NV-050-139) in order to evaluates its identified mineral resources. The area studied is in Lincoln County, NV, about 90 miles north of Las Vegas, NV. No mineral resources were identified in the study area. Volcanic rocks are the most common in the study area, consisting mainly of a thick sequence of ignimbrites in a cauldron complex. Cambrian to Triassic marine sedimentary rocks and Cretaceous to Oligocene clastic rocks are along and partly inside the west and south sides of the study area. No mineral production ha s come from the study area, but gold, silver, copper, and fluorspar have been mined nearby. Eleven mines and prospects in or adjacent to the study area were examined. Workings inside the study area include two shafts, 10 and 60 ft deep, and eleven shallow prospect pits at four sites along the west edge.

Jan 1, 1987

By C. D. Litton

This Bureau of Mines report presents a set of guidelines for determining the distribution of product-of-combustion fire sensors in underground mines. Sensor spacing is defined in terms of sensor alarm threshold, ventilation flow rate, and mine entry dimensions. Sensor spacing guidelines are presented for detection of fires from two primary combustibles, coal and wood, which are common to the majority of underground mines. The guidelines are based on data from full-scale and intermediate-scale fire tests conducted by the Bureau of Mines.

Jan 1, 1983

By H. R. Pierce

Bureau of Mines engineers end others have endeavored to deter-nine a fundamental method for gauging the capacity of gas wells to deliver gas under different pressure conditions. Their studies show that for accurate gauging two factors must be determined: (1) The actual pressures at the face of the sand in the well (usually referred to as "at the sand"), acid (2) the relation between such pressures and the rates. of flow of c as through the sand. This paper, the first of a series, describes a method of attacking the problem of determining the actual pressures at the sand by means of observations of pressures and volumes at the well head.

Jan 1, 1929

By A. M. Evans

"INTRODUCTION Exploration of the Iron Mountain and Bader iron-ore deposits in Llano County and the Gamble deposit in Mason County, Texas, was begun by the Bureau of Mines in January and completed in May 1944. The deposits had been examined by A. B. Needham, district engineer of the Bureau, in November 1942. Detailed geophysical studies by the gravity method as well as with a dip needle were made by the Bureau of Economic Geology 3/ of the University of Texas and the Federal Geological Survey. 4/ACKNOWLEDGMENTSIn the program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy., It is the policy of the Bureau to publish the facts developed by each exploration project as soon as practicable after its completion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final report. The Metallurgical Branch, R. G. Knickerbocker, chief, analyzes samples and performs beneficiation tests."

Apr 1, 1947

By Jack Mantel

The goal of this 42-month contract was to increase safety in low-seam underground coal mines through development and in-mine evaluation of a temporary roof support system for roof drills and floor-riding operator compartments for a loader and shuttle car. The program was performed in three phases. During Phase I, state-of-the-art canopy technology was investigated, and preliminary design and mock-up evaluations were performed for temporary roof supports for single-and dual-boom bolters and for transverse-mounted floor-riding canopies for a shuttle car and coal loading machine. The shuttle car and loader canopies were approved for further development, and the design, fabrication, testing, and certification were completed in Phase II. In Phase III, the Bureau of Mines furnished an FMC 6L shuttle car fur use in the evaluation of the canopy for 45 shifts. The shuttle car canopy was evaluated at Virginia Crews Coal Company in West Virginia. Efforts to secure an evaluation site for the loader canopy were unsuccessful. The loader canopy was shipped to Bruceton for possible future evaluation.

Jan 1, 1985

By H. E. Powell

Basic data were recorded on the decompositions that take place during thermal decomposition of siderite (FeC03). Both the naturally occurring and a synthetically prepared mineral were studied by differential thermal, thermo-gravimetric, X-ray-diffraction, and chemical (including gas) analyses. Thermal decomposition was studied in the media of dry air, moist air, dry carbon dioxide, dry helium, and dry carbon monoxide and at atmospheric and at reduced pressures. Results showed the thermal decomposition of FeC03 to be an extremely complex process, dependent on environmental factors and side reactions that cannot now be completely controlled. Therefore, full understanding of the reaction involved must depend on additional research with advanced evaluation techniques.

Jan 1, 1965