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By Richard D. Hagni

The character of phosphorous-bearing minerals in the Birmingham red Iron ores and iron-bearing minerals in the Eufaula bauxite deposits in Alabama has been Intensively studied by petrographic, ore microscopic, luminescent microscopic, scanning electron microscopic, electron microprobe, and x-ray diffraction techniques. A total of 15 types of phosphorous-bearing mineral grains have been recognized in Birmingham iron ores by their characteristic sizes, shapes, and distributions. Size measurements, modal analyses, and texture analyses have permitted an estimate of potential liberation of phosphorous from the iron ores by beneficiation to be 27% In areas of previous mining and 60% in areas of current iron reserves. Fine grinding, selective flocculation, and flotation may constitute the best beneficiation technique for future research. Hematite and goethite are the most important iron minerals in Eufaula ferruginous bauxites, but pyrite, marcasite, and siderite are Important iron minerals in some varieties of ferruginous bauxite, and lepidocrocite and ilmenite occur locally in minor quantities. Although simple screening will remove the coarsest iron-bearing grains, research on the utilization of high gradient magnetic separation to reduce the amounts of iron-bearing grains is recommended.

Jan 1, 1981

By Ambarish Ghosh, Rituparna Dey, Indrajit Chowdhury

"In port and harbor facilities, jetties and cargo berth terminals are usually installed on piles that remain partially embedded in soil, while a part of it behaves as columns supporting top deck. Technology in vogue adapts a pseudo static analysis in computer where the top deck including piles are analyzed as an integrated system based on finite element method when the piles are modeled as beam elements, while the soil in which it is embedded is modeled as linear or nonlinear springs. Typical berthing force of the ship is considered as a pseudo static force where the dynamic characteristics of the force is taken into consideration by an equivalent impact factor and little study exists on the actual behavior of these type of piles under the transient shock due to berthing impact. Present paper proposes an analytical solution based on which one can compute the dynamic response of such jetty piles considering shear modulus of soil constant with depth. Considering the solution is analytical in nature no special software is needed and can well be adapted fordesign office practice using generic utility software like MATHCAD, MATLAB etc. that makes theproposed model computationally very efficient.INTRODUCTIONResponse of piles under dynamic load has been an important study in the realms of civil engineering, where significant research has been carried out on its dynamic behavior under harmonic loads like one experienced in a machine foundation or under seismic force.A number of researchers have given solution to this problem like Parmelee et al (1964), Tajimi (1966), Penzien (1970), Novak et al (1974, 1983), Banerjee and Sen (1987), Dobry and Gazetas (1988),Chowdhury and Dasgupta (2008).However, most of these theories are based on piles loaded under harmonic load and valid for long piles where structural failure precedes the soil failure considering the piles are long and flexible."

Jan 1, 2015

By B Crowdey, J Wall

The particular underground operation relating to this paper is a gold producer and has an orebody predominately consisting of rhyolite and marcasites pyrite. The ore has been identified as being reactive to nitrates.Operations currently utilise two twin boom Tamrock™ Super-Drill Jumbos for development mining. Capital (waste) headings have a nominal size of 7 m wide × 6 m high, while ore headings are designed at 5 m wide × 5 m high, with the lower reaches of the mine narrowing down to a 4.5 m × 5 m design. Production drilling is currently undertaken with an Atlas-Copco L6 Solo. Due to the reactivity of the ore, inhibited emulsion phase bulk explosives are used for all blasting activities, with electronic detonators utilised in the production sequence.Sublevel shrinkage stoping is utilised when the orebody is stronger than the host rock. After blasting the ore, and during extraction, the surrounding host rock cannot maintain integrity and it ‘collapses’ on top of the ore. Gravity forces this collapsing rock to follow the blasted ore through the drawpoints.The highest risk involved with sublevel shrinkage stoping is the necessity for charge crews to work upon ‘rills’ at the drawpoints, which are occasionally unstable, to charge the next blast ring to be fired. To overcome this issue a loading technique called ‘precharging’ is used whereby two to three rings are charged, but only the first ring is fired. This technique can minimise risks by taking the charge crew away from the rill and brow.As this mine contains hot and reactive ground, strict guidelines from the Australian Explosives Industry and Safety Group Inc (AEISG) are adhered to. These guidelines relate to the sleep time for the precharged rings.This paper describes the issues faced with precharging in hot and reactive ground, the monitoring required and the systems and procedures that were put in place to enable a successful outcome.CITATION:Crowdey, B and Wall, J, 2014. Precharging sublevel shrinkage production rings in hot and reactive ground with electronic blasting systems, in Proceedings 12th AusIMM Underground Operators’ Conference 2014 , pp 283–288 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Mar 24, 2014

By R Millar

A frequent challenge in mine water management and mine design is estimation of precipitation and extreme rainfall given a short record of site meteorological data. For remote mine projects, typically only a few years of rainfall data are available, which is far too short for estimation of design rainfall event, such as the 1-in-100 year storm. A frequency-paired approach is presented for comparing daily precipitation records from a mine site with a long-term regional station and provides the basis to transpose the long-term record to the mine site. This allows a long-term synthetic precipitation record to be developed for the mine site that can be used to undertake site water balance studies, determine pond storage requirements, assess water supply options and address other surface water management issues. Conventional approaches are based on chronologically-paired data and when applied to daily data generally yield poor correlations between stations. In the frequency-pairing approach, statistical distributions (two-parameter gamma distribution) are fit to daily data from two stations and used to calculate daily and extreme precipitation values for the short-term site (which is typically a mine or other project site). The method is demonstrated using data from two meteorological stations located along the south coast of British Columbia, Canada. Use of a fitted two-parameter gamma distribution (or other distribution) provides a sound theoretical approach to comparing precipitation data from two sites and the basis for transposing a long-term record to generate synthetic precipitation series and extreme rainfall values at mine sites.CITATION:Millar, R, 2013. A statistical approach for deriving project design rainfall, in Proceedings Water in Mining 2013 , pp 273-276 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Nov 26, 2013

By E. Goris Cervantes

"A theoretical framework based on a detailed analysis of mine operations data from an oil sands mine in northern Alberta and the static simulation of truck cycle times are developed, verified, and validated in this paper. Implementation of this framework provides better results than existing tools that rely solely on manufacturer data. This, therefore, aids in efficient equipment planning for the life of the mine. The use of this framework to modify existing productivity curve estimation methods currently in use at the mine site is also proposed. This method replaces “loaded flat haul” with “loaded effective flat haul” in the productivity estimation. Validation of the model results in a 4% overestimation of productivity, versus an underestimation of more than 10% when using the existing in-house method. ¦ KEYWORDS Equipment planning, Life-of-mine (LOM) planning, Oil sands, Productivity, Truck cycle times RÉSUMÉ Un cadre théorique fondé sur une analyse détaillée des données relatives aux activités minières d’une exploitation de sables bitumineux dans le nord de l’Alberta et la simulation statique des temps de cycle des camions sont développés, vérifiés et validés dans cet article. La mise en oeuvre de ce cadre offre de meilleurs résultats que ce que proposent les outils existants, lesquels se basent uniquement sur des données des constructeurs. Ceci contribue donc à une planification efficace de l’équipement pour des projets relatifs à la durée de vie de la mine. On propose également de se servir de ce cadre pour modifier les méthodes d’estimation de la courbe de productivité actuellement utilisées sur le site minier. Cette méthode remplace le concept de loaded flat haul (la distance parcourue par des camions avec un chargement du point de collecte jusqu’au point de déchargement des résidus miniers) par celui d’effective loaded flat haul (la distance relative parcourue par des camions avec un chargement du point de collecte jusqu’au point de déchargement des résidus miniers) dans l’estimation de la production. La validation du modèle résulte en une surestimation de 4 % de la productivité, par rapport à une sous-estimation de plus de 10 % avec la méthode actuellement utilisée en interne. ¦ MOTS CLÉS planification de la durée de vie de la mine, planification de l’équipement, productivité, sables bitumineux, temps de cycle d’un camionINTRODUCTION One aspect that differentiates oil sands mines in northern Alberta from conventional hard-rock mining is the environment in which they operate. Due to ground characteristics, producers in the region experience roads with very high rolling resistance (RR) that, in turn, negatively affect haul-truck performance and greatly increase fuel consumption and emissions. Oil sands mining companies use some of the largest haul trucks in the world. In addition, oil sands mines cover more extensive areas than hard-rock pits, resulting in longer haul distances on roads made of comparatively more viscous material."

Jan 1, 2019

By B. C. Jago, H. Derbuch

"The Freightrain kimberlite is located on the Brodeur Peninsula, Baffin Island, Nunavut. Twin Mining is exploring the pipe and adjacent land (79 claims/655 km2) using a combination of airborne geophysics, soil sampling, diamond drilling, trenching and bulk sample processing. The pipe originally was discovered by Cominco Limited in 1975, re-evaluated in 1993 by Lumina Investment Corporation, when it was staked as the Zulu pipe, and subsequently covered by three claims in 1998 by Helix Resources who called it Freightrain.The Freightrain pipe coincides with a strong, ovoid-shaped aeromagnetic anomaly. It is the only surface exposure of kimberlite within a 30 km long linear trend of fourteen aeromagnetic anomalies that are up to 600 m in diameter.The pipe is exposed in the crater facies, near the transition into diatreme facies as indicated by the occurrence of pyroclastic kimberlite characterized by abundant olivine macrocrysts, juvenile lapilli and kimberlite autoliths set in a serpentine-calcite matrix. Olivine, Cr-pyrope garnet and chromite are the most abundant macrocrysts; clinopyroxene, ilmenite and phlogopite mica occur in minor to trace amounts. Garnet and chromite harzburgite, garnet lherzolite, garnet-spinel lherzolite and rare eclogite dominate the xenolith population.Garnet and chromite mineral chemistry indicate encouraging diamond prospectivity and that potentially diamondiferous garnet and chromite harzburgite were the principal sources of diamond in the mantle at the time of kimberlite eruption.Single clinopyroxene grains define an ~42 mW/m2 sub-continental geotherm that is rooted in the diamond stability field. This compares to a slightly hotter geotherm (~48 mW/m2) for adjacent Somerset Island kimberlites with an origin in the graphite stability field. This data accords with the general lack of sub-calcic Cr-pyrope garnet, diamond inclusion chromite and diamond in Somerset Island kimberlites."

Jan 1, 2002

By P. Favreau

"This paper describes the progress accomplished at the Noranda Technology Centre in the field of three-dimensional computer-aided underground blast design. Traditional methods of laying out underground blasts are reviewed, and the new computer-aided approach is described. Time savings achieved through the use of BLASTCAD can be advantageously used to better engineer blasts, using models and blast vibration analysis. Future work involving the attachment of blast models directly to the system is also addressed.IntroductionThe Noranda Technology Centre's (NTC) Environment and Mining Laboratory, in cooperation with the mining operations of the Noranda Group, is committed to the development and implementation of new technologies in the field of mineral extraction . Within the frame of its research program, the Blasting Technology Program is developing computer "" tools"" designed to assist the blasting engineer or technician. These computer "" tools"" are regrouped under a global software system called BLASTCAD.The BLASTCAD project started in 1990 at NTC. At that time computer programs designed to calculate and model various blasting parameters had been accumulated. These programs cam e from different sources and were mutually incompatible. Furthermore, they were developed as research programs with tittle effort spent on user interface. These programs are very useful, but are highly specialized, need large input files and can be quite tedious to use as ""standalone"" packages .Therefore, the situation being faced was one where all these programs were available at the Noranda Technology Centre, but not a t the operations. The two following options were then considered: 1. continue to run all the models and programs at the Noranda Technology Centre, and present results through reports to the mines, or2. regroup all the different programs under a single one that would make them share the same data base and be transported to the user. This second option is the one that was adopted; the result is BLASTCAD."

Jan 1, 1993

By Charles H. Bucknam

A gold sampling optimization study was carried out in support of open pit gold mining operations for the Newmont Gold Company Bootstrap-Capstone deposits in Northeastern Nevada. Six bulk samples were tested using fire refining techniques at field particle size, to determine coarse particle heterogeneity of the ores, and by gravity .concentration methods at 10 mesh particle size, to observe any particulate gold liberation. An overall sampling model is presented for the deposit based on the pooled test information, to reconcile the results of coarse particle heterogeneity testing and the fine particle 'liberation testing. The sampling model is used to recommend procedures to control the variability of gold grade estimation due to the fundamental error (nugget effect) during sampling, sample preparation and assaying of the ores and other fundamental variances. The technique of simplified quantitative risk analysis (SQRA) is used to provide an economic justification for implementation of. recommended improvements to field sampling practices.

Jan 1, 1999

By Jaeheon Lee, Jae-Chun Lee, Doyun Shin, Minseuk Kim, Hyunsik Park

"The appropriate treatment of cyanide waste water is becoming an emerging issue because of the toxic residue and large quantity produced from gold processing plants. In the present article, we designed and operated a continuous biological cyanide treatment system using domestic sewage sludge and various microorganisms including a cyanide-producing and degrading bacterium, Chromobacterium violaceum. The synthetic wastewater containing 50 mg/L of cyanide was pumped continuously into the reactor at a flow rate of 500 mL/d for 21 days. When 50 mg/L of cyanide was fed, the cyanide concentration in the effluent of the reactor inoculated with activated sludge (S-50) decreased by 7.5 mg/L in the effluent. The other reactors did not show significant cyanide degradation and the reactor inoculated with C. violaceum showed increased cyanide concentration in the effluent. The microbial community in the reactors was analyzed by 16S rRNA-gene based pyrosequencing technique to investigate microbial response to cyanide addition and operation time. The microbial community analysis shows that the phylum Proteobacteria was detected in the reactors showing significant cyanide degradation (S-50), while Firmicutes and Bacteroidetes was dominant in the other reactors with very low cyanide degradation. Proteobacteria could not compete when the other phyla Firmicutes or Bacteroidetes were inoculated. This study shows the feasibility of the biological cyanide treatment system for gold processing plants and contributes new fundamental knowledge about the microbial community in the biological cyanide treatment system. INTRODUCTION Cyanidation has been widely used to recover gold from ores or secondary resources since first proposed by MacArthur and Forrest in 1888 (MacArthur et al., 1888) and it is used in many states of the USA, including Nevada, Arizona, California, Colorado, and Idaho (Laitos, 2012). Cyanide compounds are highly toxic and create serious problems for wildlife and water management (Solomonson, 1981; Donato et al., 2007). Furthermore, because many countries have imposed strict standards for cyanide discharge (USEPA, 1985), it is essential to develop a cost-effective and environmentally friendly technology for treating cyanide-containing wastewater."

Jan 1, 2018

By B. E. Davis

The Bureau of Mines conducted tests on samples of two Florida phosphate slimes t6 devise a technique to recover phosphate currently dis-carded because of its fine size. A flotation technique was devised to recover the phosphate contained in two fractions of each slime: the plus 37um fraction and the plus 20-um fraction. The technique involved conditioning the flotation feed with sodium silicate and a fatty acid-fuel oil emulsion, floating a rougher phosphate concentrate, and cleaning the concentrate in two cleaner stages with sodium silicate added to each for gangue depression. Concentrates containing 21.0 to 32.3 pct P20S were produced with recoveries of 68.1 to 84.2 pct of the P20S con-tained in the flotation feed.

Jan 1, 1987

By A. W. Deurbrouck

The separations achieved by eight conventional cyclone washers have been evaluated to determine their performance when processing intermediate size coal of 28 mesh bottom size. The dense-medium cyclones provided efficient, sharp separations in treating feeds of up to 44 percent of near-gravity material at separating specific gravities ranging from 1.42 to 1,55 (one separation of a secondary feed was made at 1.63). Complete washability analyses are shown by sizes of the composite feed to these cyclones. The magnetite losses per ton of coal processed ranged from 0.6 to 2.0 pounds; however, of the eight plants reporting losses, seven indicated magnetite losses were 1.1 pounds or less per ton of coal processed.

Jan 1, 1972

By Roy L. Grant

The Bureau of Mines investigated the up-and-down method with factorial designs to determine if shorter, and therefore less costly, trial sequences could be used. Although sequences of 50 trials are usually recommended, sequences of 20 trials were arbitrarily chosen for the experiments with permissible coal mine explosives described in this report. These explosives were fired from a cannon pointed into a flammable natural gas-air atmosphere at the Bureau of Mines Explosives Research Center gallery to ascertain their safety properties. The investigation demonstrated that the shorter sequences led to useful conclusions with a reduction in cost of the experimental program.

Jan 1, 1967

By Pedro Henrique da Rocha Silva

Os tratamentos de borbulhamento de gás nas panelas são parte essencial para melhoria da cinética de todas as reações, diminuição de zonas mortas e remoção de inclusões. O presente trabalho teve o objetivo de caracterizar as bolhas da pluma na panela usando fotos tiradas por uma câmera de alta velocidade e assim avaliar seu diâmetro e sua área superficial. Foram utilizados três plugues porosos situados no fundo da panela, com áreas de injeção diferentes e testadas diferentes vazões de injeção. A partir dos valores encontrados, foram feitas considerações sobre os processos de refino dentro da panela.

Oct 30, 2017

By Olli Haavisto, Lauri Koresaar, Navid Khajehzadeh

In recent times sustainable minerals processing is an important topic in research. Sustainable mining is linked with efficient use of energy and human resource in all process stages including beneficiation of the ore. Controlling and optimizing the recovery while preserving the grade of the concentrate is extremely important in flotation plants. This development requires new technological solutions and has given rise to the multitude of application areas for lasers. X-ray Fluorescence (XRF) and Laser-Induced Breakdown Spectroscopy (LIBS) are currently two of the predominant non-contact and direct analysing methods in industry. LIBS and XRF measurement techniques both have high capabilities for measuring elements. LIBS has a very simple and easy-to-implement spectroscopic setup, wider range of elements can be detected with online LIBS and measuring light elements is simpler by LIBS compared with XRF. It is of great interest to extract mineralogical information from the elemental results with no modification on the measurement setup. In order to achieve this, more advanced interpretation of the elemental peaks of LIBS spectra is required. Therefore, the major focus of this research is about measuring mineral concentrations from the elemental lines of LIBS spectra using advanced statistical methods. This accomplishment provides knowledge about mineral concentrations from the real-time assay data of the slurry LIBS analyzer. Consequently, this paper first discusses an analytical method called partial least squares regression leading to rapid mineral identification from the elemental contents of the LIBS technique. Then the technique is employed to analyze the mineral contents quantitatively through the information acquired from an on-stream LIBS slurry analyser. This can lead to many benefits such as rapid control of concentrate quality, enhanced recovery, saving time, energy and manpower.

Jan 1, 2016

By Fengmei Chen, Na Liu, Bingrui Li

A quantitative analysis method based on the airflow influence factors is proposed to evaluate airflow stability and discriminate airflow directions in complex ventilation networks. The law governing the changes in airflow caused by changes in branch resistance is revealed based on simulations of the airflow state in a ventilation network and a statistical analysis of the results. Then, three evaluation indices (airflow sensitivity, airflow influence factor, and critical airflow) are determined, matrices of the airflow influence factors and critical airflows are constructed, and a quantitative evaluation method for ventilation system stability and an airflow directional discriminant are proposed. The results show that the stability of a ventilation system can be reliably evaluated based on the airflow influence factors. The sensitive branches and dominant branches in the ventilation network can be determined based on the matrix of airflow influence factors, and the reversed branches, the trigger branches, and the reversal conditions can be determined based on the critical airflow matrix and the matrix of airflow influence factors. The proposed airflow directional discriminant is suitable for evaluating arbitrarily complex networks.

Nov 15, 2023

By Tedd B. Bodimer

Why complicate an already complex machine such as a continuous miner by adding roof drills? Immediate permanent roof support is an immediate thought of the mining engineer just as elimination of frequent time-consuming places changes is a thought of the methods engineer. The realization of those two objectives has the potential for improved safety with increased production is the thought of the general manager. Miner-Bolters Used a Generation Ago These are not new thoughts as the 1CM continous miner equipped with two integral roof drills was introduced twenty-five years ago. Approximately two hundred of these machines were sold in the next five years for use in medium and high seam operations. The 1CM miner chassis that remained stationary in the center of an entry or room while the ripper bar was swung and sumped hydraulically provided an ideal platform for mounting two roof drills that could be operated during the continuous miner's production cycle. Two roof bolts could normally be installed in less time than required for the mining cycle. A typical roof drill unit is shown in Figure I.

Jan 1, 1981

By S. C. Sethi

The WIPP (Waste Isolation Pilot Plant) Project near Carlsbad, New Mexico, is a research and development project sponsored by U.S. Department of Energy, designed to demonstrate the safe containment for disposal of radioactive waste. A mine (repository) is currently being developed 2150 feet below the surface, in a thick salt bed which will serve as the disposal medium. Provision of a proper ventilation system at the WIPP Project is a major priority of those responsible for its design, management, and operations. As an ongoing effort towards this goal, it was decided to simulate the mine's ventilation system using Dravo's MINEVENT computer program. Specifically, the work included the development of the following simulation models: 1. Simulation of the current ventilation system 2. Simulation of the designed ventilation system for the following modes: o Mine Construction mode/shift o Waste storage mode/shift o Fire or exhaust filtration mode These computer models are useful in solving complex ventilation problems likely to be encountered in an R&D project, like WIPP. They are particularly helpful for the development of contingency plans to incorporate during emergency situations, such as fires, fan stop- pages, radiation leaks, etc. Also, they can be utilized when considering expanding certain underground areas to ensure the availability of adequate ventilation.

Jan 1, 1986

In connection with the recent visit of the Special Mission of British Ministry of Munitions to the United States, the United Engineering Societies gave a dinner to the members of the. Mission on Tuesday evening, Nov. 13. This was the only public function on behalf of the visiting commissioners while they were in New York. During the remainder of their visit they were in daily conference with bankers, merchants' associations, labor federations, and other organizations. The result of these conferences will doubtless have an important influence on the manufacture of war supplies in the United States, since it will enable our business men and manufacturers to avoid a good many of the mistakes that unfortunately occurred in England at the beginning of the war. At present, fully 90 per cent. of the employees of British munition factories are omen, and the problem of employing women in the industries of the United States will doubtless soon be encountered with increasing frequency.

Jan 1, 1918

By Fitterer, G. R.

The impact of the work of Herty "et al" on modern liquid steel technology can only be evaluated by first setting the stage as it existed in 1926. It is important to briefly review not only the steel making process and viewpoints regarding methods of refining, but also to describe the tools which were available for research at the time. One must recall that only 15 years before the beginning of this program, the open hearth production exceeded that of the Bessemer in the United States. Many open hearths were still operating on producer gas (a very inefficient fuel), although some plants were converting to the use of natural gas and very few to oil. Continuous rolling of wide strip started this year. The Faraday Society in England held a World Conference on Physical Chemistry in Steel Making in 1925 and the contributions to this work created considerable interest throughout the world and it appeared that physical chemistry might convert the art of steel making into a science. These papers, however, attempted to solve the problems through the use of the older physical chemical concepts such as Nernst's numbers, etc. and considerable data were missing. In 1923, Lewis and Randall had published their book Thermodynanzicsl and this was later to establish and standardize the steps which are now accepted for the calculation of physico-chemical equations. At the time this research work was started, there were no small high frequency induction furnaces. Northrup had just invented his high frequency furnace and a few large units had been instilled in plants. The vacuum fusion method lor the determination of oxygen in steel was

Jan 1, 1957

By M. Smutz, C. J. Baroch, E. H. Olson

IN 1949 an orebody containing some 10 billion lb of recoverable rare earth metals was discovered in the Mountain Pass district of San Bernardino County, California.' The following year Molybdenum Corp. of America purchased a number of claims at the deposit and a mill on the property which had been constructed to process the district's gold ores. Average composition of ore from the San Bernardino deposit is less than 0.1 pct Tho2, 25 to 35 pct calcite, 10 pct rare earth oxides, 15 to 20 pct silica, and 30 to 40 pct barite.' Rare earth content of the ore analyzes 50.7 pct CeO2, 4.2 pct Pr6O11, 11.7 pct Nd2O3;, 1.3 pct Sm2O3,, and 34.3 pct La2O3 and others.' By floating the barite and depressing the bastna-site, Molybdenum Corp. of America produced a concentrate that contained 60 to 70 pct rare earth oxides. More than 25 pct of the rare earths, however, was lost in flotation. It seemed likely that a more economical method could be found. At the present time most of the rare earths in the concentrates are converted to rare earth chlorides, which are either fed to ion exchange columns for separation of the individual rare earths or reduced to misch metal. Current investigation shows that solvent extraction may achieve this separation more economically than ion exchange. The study reported here was undertaken to develop an economical method of preparing a pure rare earth nitrate mixture from California bastnasite ore. Results indicated that more than 98 pct of the rare earths could be recovered. Several possibilities were considered for processing bastnasite ore, but only the method outlined in Fig. 1 was investigated. This involved leaching the calcined ore with nitric acid. The nitric acid process is discussed under the following headings: 1) calcination of the ore, 2) leaching of calcine, 3) filtration studies, 4) solvent extraction, and 5) nitric acid recovery. Calcination: Since California bastnasite ore contains 25 to 35 pct calcite and about 10 pct bastnasite, calcination was needed to reduce the violence of reaction with nitric acid. Weight losses of 26 to 30 pct were obtained by calcining the ore at 900°C for I hr or at 800°C for 4 hr. Longer periods resulted in no further weight loss. Leaching the Calcine: When the bastnasite calcine was leached with 30 pct nitric acid for 8 to 10 days, rare earth recoveries of only 45 to 50 pct were

Jan 1, 1960