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By S M. C Verryn

Through the application of the Rietveld method, X-ray diffraction analysis has developed into a fully quantitative method for phase analysis of metallurgical products. The Rietveld method itself has progressed from an unstable method that required constant operator intervention to a stable and robust method suited even for routine process control. Knowledge of the crystal structures of the major phases is essential for Rietveld analysis, and these are well known for most minerals and major phases in metallurgical products. It provides the basic structural information necessary for the determination of mineral stoichiometry and for elucidating solid solution behaviour. Modern methods, such as simulated annealing and charge flipping, permits the determination of crystal structures from powder data. Unit cell data can be used where conventional microchemical analysis is unable to provide an answer to the extent of solid solution in ilmenite roasting. Unit cell data (by XRD) is used to determine the amount of roasting necessary for the development of magnetisation to be able to separate chromite from an ilmenite concentrate. Phase quantification is probably the most widely used application of XRD analysis. It is used for materials balance in the minerals and cement industries, and it is finding novel applications in the iron and steel industry. Applications of XRD in high-temperature metallurgical processes are increasing. In this paper the phase chemistry of iron ore sinters, the evaluation of subsolidus reactions in titania slags and the identification of furnace accretions are discussed. Despite the success of the Rietveld method in phase quantification, the method still needs further development in the quantification of closely related or polytypic phases. The quantification of pyrrhotite phases using various Rietveld programs still gives ambiguous results. This is also true for the different SFCA phases in iron ore sinters. Clearly the analysis of similar phases, differing only in the presence of weak superlattice reflections is still problematic.

Jan 1, 2008

By M A. Gontalves, A F. D C Varajpo, S A. Stachissini

Clays from the Santa Elena Peninsula, south-east of the Ecuador coast, were investigated with a view to identifying their main mineralogical, physical, chemical and textural characteristics as well as their potential for industrial use as adsorbents. Identified as calcic bentonites, two representative samples from the Tosagua Formation (Oligocene to Lower Miocene) were selected for acid activation trials. The selection criterion was based on the greatest amount of clay fraction (<2 ¦m fraction) associated with the greatest content of montmorillonite. For the activation treatments, HCl and H2SO4 solutions of 4, 6 and 8 N were used in a stirred glass reaction vessel with the clay sample under reflux during four hours at temperatures of 70¦C for HCl and 85¦C for H2SO4. Mineralogical analysis by X-ray diffraction (XRD), chemical analysis by X-ray fluorescence (XRF), differential and gravimetric thermal analysis and measures of density, surface area and porosity indicated the changes occurred in the crystal structure of the montmorillonite. The acid treated clays were utilised in trials of purification and decolourisation of soybean vegetable oil in a ratio of 2:100 (clay/oil) at 90¦C for 30 min, under constant stirring. After centrifugation of the suspension, the wavelength of the bleached oil was measured by UV-visible spectrophotometer and the bleaching capacity of the clays was determined. The best bleaching capacity of the samples was obtained with 6 N H2SO4 acid-activated clays. The bleaching capacity was compared to Tonsil, a commercial acid-activated clay and similar results between them evidenced the potential industrial application of the Ecuadorian clays to bleaching of vegetable oil.

Jan 1, 2008

By Fitzgerald DE, Taverner MG

The principles, fields of application and equipment design concepts of several new approaches to continuous vacuum treatments of molten metals and alloys are discussed. Partic- ular attention is paid to the results of pilot plant tests evaluating a launder-in-tube method of 1. continuous production of refined zinc from a zinc-bearing lead produced in the lead splash condenser of the Imperial Smelting Furnace (ISF), and 2. continuous refining of crude cadmium. The former trials were not sufficiently encouraging to justify consideration of the process for commercial development. The applic- ation to cadmium upgrading gave very promising results; metal of 99.99 per cent purity was produced continuously at pilot scale (120 lb per hour) from crude metal containing 5.0 per cent Pb.

Jan 1, 1972

Powercoal Pty Ltd operates eight underground coal mines in New South Wales and produces coal for both domestic power stations and the export market. Approximately 40% of total production is from continuous miners. Over the past five years, place change mining methods have been introduced to improve productivity from continuous miners. This has involved utilising the existing coal clearance system from the continuous miner to the ratio feeder using trailing cable shuttle cars.By late 1996 average productivity at Cooranbong Colliery using this system had plateaued at 800 tonnes per eight hour shift. A number of factors were identified to increase average productivity to 1500 tonnes per eight hour shift. An improved coal clearance system was one of the factors identified.

Jan 1, 1998

A methodology for the fatigue life estimation of load haul dumpers, employed in underground platinum mines, has been developed and applied. This method entails the quantification of operating conditions by means of stress measurements. The measurements are then translated into a fatigue loading factor for a finite element model. The results of this analysis are then used to compare all the critical connections in the structure to detail categories in relevant fatigue codes, and predict a life in operating hours for the vehicle structure. The method was applied on a specific model and the results of this analysis were compared to actual failure occurrences with reasonable accuracy. It is intended that the methodology be embedded into performance specifications and purchasing contracts and that technology transfer to OEMs be achieved. Based on the experience of this project and other similar exercises it is estimated that structural life expectancies may be increased across a typical fleet of trackless mining vehicles (LHDs, drill rigs, utility vehicles, dump trucks) by at least 20 per cent.

Jan 1, 2005

In the past few years the Rietveld method emerged as a routine tool for quantitative phase analysis (QPA) from X-ray diffraction data. Fast and reliable results became possible by combining modern computer technology and optimised mathematical algorithms with the fundamental parameters approach in the Bruker AXS TOPAS software. Here the routine analysis of bauxite raw material and of aluminium bath electrolyte is presented. The accuracy of bauxite quantification was tested by analysing the IUCr round robin sample. An agreement of better than one per cent was obtained for minor constituents and a maximum deviation of 2.5 per cent for the major phases. This is excellent agreement with expected results from weighting. Ten different phases were quantified in natural samples from Turkey with a precision better 0.5 per cent for the major phases and one per cent for the minor phases. Additionally, crystallite sizes were obtained from the peak profiles that give valuable information for the processability of the material. XRD data from solidified aluminium electrolytes were rapidly measured using silicon strip detector technology. With the LynxEyeTM detector full patterns were collected in 90 seconds and analysed with TOPAS. It is shown how to derive well-established measures such as bath ratio and excess AlF3 from the Rietveld results. These measures are widely used in aluminium production and readily available with very high precision. The excellent agreement with ALCAN reference data demonstrates the outstanding accuracy of the method. The mean deviation between here presented results and reference data is below 0.5 per cent for total CaF2, below 0.25 per cent for excess AlF3 and 0.02 for the bath ratio. The precision of the method was evaluated by repeated measurements.

Jan 1, 2008

By Bhattacharyya A. K

The current methods for predicting pillar strengths are reviewed. A two-dimensional model, based on the Mohr-Coulomb failure criterion, is proposed for determining the compressive strength across the width of a long pillar. The model can be used to determine pillar strength and the depth of the crushed (ie yielding) zone from the pillar edges. The values of the parameters in the model, namely the cohesion and internal friction angle of the coal seam, friction angles at the contact of the coal seam with the roof and floor are determined by matching the strengths predicted by this model with the Bieniawski pillar strength formula for pillar width to height ratios up to 5. It is found that the derived values of these parameters are quite close to the results from laboratory tests. Based on the model, a preliminary analysis of pillar stability is made.

Jan 1, 1995

By P O. Andersson

Mining of sill pillars is more difficult than the ordinary mining. The sill pillar mining is performed under more difficult conditions and the mining of the sill pillar itself produces more problems; failure of the rock due to high stresses, difficulties in controlling the fill above, overall stability of the stope and special requirements on the technique for backfilling. Altogether this makes sill pillar mining technically difficult and often not profitable. A project was therefore initiated with the aim to increase the mineable ore reserve by making sill pillars mineable, both technically and economically. The project aimed at developing technique for already existing sill pillars as well as planned sill pillars. For the existing sill pillars a technique would have to be developed for mining beneath unstabilised fill. For sill pillars that would be created in the future, the most suitable mining method and methods of supporting or stabilising the fill in the stope above was to be chosen within the project.

Jan 1, 1998

The accuracy of an ore reserve is only as good as the geologist's understanding of the deposit. The methods that are applied to resource and reserve estimation reflect that understanding. At the Olympic Dam copper-uranium-gold deposit in South Australia, evolution in the understanding of the controls on mineralisation coupled with the changing demands of the project have led to changes in the approach to reserve estimation. The project has moved into a phase where detailed stope mining reserves are now required as distinct from global ore reserves. The complex nature of the mineralisation and the large amount of data demand that all available information be readily accessible in a flexible format. To enable the selective manipulation of geological and assay information and its characterisation, a relational database has been developed. For reserve calculations themselves, initial computations were based on a system derived from that used for the Kambalda nickel orebodies. The Olympic Dam system differed mainly in the use of statistical analyses in the estimation of grade instead of the previous polygonal area of influence weighting method, Three dimensional weighting techniques are now being used for local reserve estimates. Flexible facilities for raw data handling combined with grade estimation techniques which are commensurate with the mine geologist's understanding, produce detailed gridded and contoured ore zone models suitable for reserve calculations and stope designs.

Jan 1, 1987

The Project Financing Industry is currently being expanded en- compassing greater competition due to the improved worldwide economy. This has meant that money is in greater supply than demand for both loan and equity investment and is available for larger and higher risk ventures. The consequence of this is that the Project Financing Industry should be better able to provide more innovative forms of financing to meet the needs of mining and petroleum companies, regardless of size. Large mining and petroleum companies in Papua New Guinea should therefore be looking for ways to raise equity funds for exploration in greenfield areas, diversifying their risks through acquisition, and seeking to reduce their costs of borrowings. The small to medium sized mining sector should be looking to raise equity for increased ex- ploration on tenements and, where possible, to raise borrowings to fund expansion and further development of their projects. In summary, it is a period during which companies should take ad- vantage of available funding to augment their strategic plans and increase their long term returns to shareholders.

Jan 1, 1997

By M Heidari, M Ataei

Today, the selection of a mining method is a multi-criteria decisionmaking process, with many factors in this process connected to each other. These trends do not have a high degree of confidence. In this study the analytical hierarchy process was used to select the suitable mining method for anomaly No 3 of Gol-Gohar iron mine of Iran. The results of this study show that gathering all existing information from the exploration stages and using AHP technique, the open pit mining method is the mining method for this anomaly.

Jan 1, 2003

About 60 persons are admitted to the graduate course every year after passing the entrance examinations. The entire course of studies is free of charge and the universities provide accommodation for the students who need it. The five years of studies are divided into 10 semesters. One semester lasts 15 weeks. Automatics can be studied at three separate faculties. At the University of Mining and Metallurgy, it is offered by the Faculty of Electrical Engineering, Automatics and Electronics as well as the Faculty of Mining and Metallurgical Machines (metrology can also be studied there); at the Silesian Technical University in Gliwice, the Faculty of Mining offers the course. The educational plans and programmes comprise 3 groups of subjects: common for a given course of studies (foreign languages, political science and the basic technical knowledge) common for the speciality and subjects of diploma courses. The whole time of studies covers about 4400 hours excluding 3 periods of professional training and the physical training. The classes, laboratory classes, seminars and design classes are obligatory and the attendance is strictly checked. Students may extend their knowledge by participating and working in the Science Clubs. The students' work is checked not only during the classes but also by the examinations held at'the end of respective semesters. Those who fail the exams can repeat them only if very important reasons are presented. At the very end of the studies there is a diploma examination together with a discussion on the diploma thesis, written by the student. The successful result entitles the student to recieve the title of "magister inzynier",M.Sc. of his speciality. The graduates, after working for 2 years, can attend another course of studies lasting 2 semesters and called "Postgraduate Course", or start "Doctoral Studies" finished by the defence of a doctor's thesis. In'these cases the expenses are usually covered by the graduates' employers.

Jan 1, 1985

By E M. Rykaart

The design of soil covers as part of the remediation initiatives for mine waste facilities is common practice and more and more engineers are faced with designing these facilities. The design issues associated with these soil covers are complex and requires a good understanding of unsaturated flow. More engineers are making use of numerical models to predict how cover designs would perform, and this has been necessitated by the high non-linearity associated with solving unsaturated flow problems. There are numerous numerical models available to the prospective users and they are all simplifications of reality using different assumptions. The users of these models often do not understand the limitations of the models but rather select a model based on ease of use, and that lends to increasingly erroneous designs being proposed for construction. This paper describes a comparative evaluation of a cover design using four different codes available today; SoilCover, SWIM, HYDRUS-2D and HELP. The paper does not propose to measure these codes up against each other and make statements about which is better than the other but rather illustrates how the assumptions in each code affect the outcome. The data set used for the comparative study is a well calibrated data set that that has been collected over a long period in time and that has been collected according to strict controls. The authors present the pitfalls of numerical modelling of the surface flux boundary conditions, as well as present guidelines towards appropriate use of these modelling tools.

Jan 1, 2003

By Smith E. L

The Ore Reserve/Exploration System implemented at Mount Isa for M.I.M. Holdings Limited is a comprehensive computer system designed to process assay, geological, structural and survey data input via special purpose logging sheets from daily activities at Isa Mine, Hilton Mine and various Carpentaria Exploration Company prospects. The system performs two basic functions; (1) data acquisition, validation and file maintenance to prepare the data for retrieval, and (2) generation of routine and optional reports. The types of reports available range from masterfile detail printouts and retrieval of data by key items to survey computations, structural analyses, cutoff calculations, statistical analyses and ore reserve calculations by the polygonal, inverse square or moving average techniques. The use of various optional reports available through the system is illustrated by several examples, and planned future development is discussed.

Jan 1, 1973

By G W. Wilson, C Panidis

Potentially acid forming (PAF) waste rock contained in dumps formed as a result of open cut mining of metalliferous orebodies are conventionally sealed or covered using a near-saturated, low permeability compacted clay layer, protected with a mulch layer and/or vegetated growth medium. The purpose of the compacted clay layer is to limit oxygen diffusion and the infiltration of rainfall into the dump. Where the aerial extent of the PAF waste rock dump is large, or where suitable clayey material is in short supply, it may be difficult to source sufficient suitable clayey material to form the cover. The paper describes a laboratory-based investigation of combining inert waste rock and tailings to form an alternative seal or cover material. The inert waste rock was sourced from the trafficked surface of a non-acid forming (NAF) waste rock dump, with a maximum particle size of about 100 mm. This was combined with NAF thickener underflow tailings slurry in various mass ratios, and the resulting mixtures tested for their particle size distribution, compaction characteristics, soil water characteristics (relationship between suction and volumetric moisture content), and saturated hydraulic conductivity. The mixtures tested ranged in consistency from those dry enough to be compactable, to those with the consistency of wet concrete that lend themselves to placement without the need for compaction. The laboratory test results showed that the suitability of the mixtures as seal or cover materials is very dependent on the particle size distribution of the mixture, with well-graded mixtures having substantial fines performing best.

Jan 1, 2003

By Chugh Y. P

A simplified, three-dimensional, time-dependent, mechanistic model of the overburden-coal seam-floor interaction has been developed and validated at two Illinois coal mines. The model based on the thin plate theory can involve any complex layout of mine workings, time-dependent sequence of extraction and, rheological properties of immediate floor strata. The model output data consist of spatially distributed surface subsidence and its slope and curvature, as well as load acting on pillars in one or more panels. A comparison of calculated and monitored surface subsidence or in- mine convergence measurements has proven the model's effectiveness for surface subsidence and load transfer Prediction.

Jan 1, 1992

By Smith KS

Mineral-deposit geology, geochemical processes, and biogeochemical processes are fundamental controls on the environmental conditions that exist naturally in mineralized areas prior to mining, and that result from mining and mineral processing. Input from economic geologists and geochemists is therefore crucial to effectively predict, assess, mitigate, and remediate the environmental effects of mineral-resource development. Recent open pit gold mining at Summitville, Colorado, has received intense public scrutiny for a variety of environmental problems, most important of which has been extreme acid drainage. Now a Superfund environmental cleanup site, Summitville exemplifies how economic geology and geochemistry principles (1) could have been better utilized to first predict and minimize the environmental problems, and (2) can now be used to optimize the environmental cleanup.

Jan 1, 1995

The authors are looking at the behaviour of the mineral processing circuits by means of the simulators operating under random disturbance. The present paper deals with the fuzzy control systems in comparison with PID controllers. A series of tests are conducted on simplified prototype processes with (1) dead time plus first-order lag model and (2) diffusive model. In the next series of tests the self-sustained process model was introduced to improve control against dead time. In both cases fuzzy and PID controllers are optimised by EVOP method. Particular attention is paid to the effect of observation noise to analyse for the problems which can be fatal to practical applications in mineral processing. Finally the methods developed are applied to a closed-circuit wet grinding system simulator operating under random disturbance.

Jan 1, 1993

By Johnson M, Wooltorton B

A programme of hydraulic fracture stress measurements conducted in surface drill holes along the alignment of the King River Power Tunnel has provided information of importance to the assessment of the extent of steel lining requirements for the tunnel. A significant horizontal stress field has been detected at a location remote from the power station site, with a corresponding absolute minimum stress magnitude approximating the overburden pressure based on depth of cover. Measurements made closer to the power station site (located toward the bottom of a valley) have revealed an apparently relatively destressed region with minimum stress magnitude less than overburden pressure. The implications of these results are discussed.

Jan 1, 1987

Three methods of gold analysis are briefly described highlighting some of the problems and advantages of each. The variation of results between samples and splits and due to method preparation are illustrated. The mean percent difference of the fire assay values from the means of sample split values for three cases is 15%. Finally, a comparison of the aqua regia atomic absorption spectroscopy and fire assay fusion AAS techniques is made. This shows that the mean precision, the ability to obtain the same value, of the methods at 98% confidence are +30% and +15% respectively. The fire assay fusion atomic absorption spectroscopy method is relatively more accurate than the aqua regia method.

Jan 1, 1982