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By R. Holmwood, M. Faris, P. Holloway, M. Collins

Sulphuric acid addition is a major driver of the economics in the processing of nickel laterite ores by high pressure acid leaching (HPAL). Understanding the optimal acid addition rate is essential for the success of any HPAL operation, and this is especially true at Ambatovy, where the composition of the feed tends to vary significantly on a day-to-day basis. Most studies on the effect of acid on nickel extraction in HPAL have used laboratory testwork as their basis. Although these studies are invaluable in assessing the economics of a new project, they are limited by the range of ore composition that can be tested and the differences between the operation of the laboratory equipment and the commercial plant. To enable optimization of the acid addition at Ambatovy, operating data from the HPAL operation were obtained using OSISoft’s PI system and the data from several periods were examined to develop relationships between acid addition and nickel extraction. The initial relationships from 2014 focused on the acid required to achieve a target nickel extraction of 95%, with aluminum and magnesium in ore and feed slurry solids content as the major variables. As Ambatovy ramped up through 2015 and 2016, the calculated acid requirement was further refined to address the effects of HPAL temperature and retention time, and the oxidizing/reducing characteristics of the ore, and to generate acid requirement relationships as a function of ranges of nickel extraction. These relationships supported raising the target nickel extraction to 96% and enabled the development of an economic model between acid addition and nickel extraction.

Jan 1, 2017

By D. J. Zuliani

A mass and energy balance for a modern electric arc furnace ("EAF") indicates that about 70% of the process energy losses are contained in the off-gas as chemical energy in the form of uncombusted CO and H2 and as thermal energy. Given the magnitude of the off-gas energy losses, improved EAF energy efficiency needs to focus first on controlling furnace practice to maximize "in-EAF" energy utilization and second, on recovering residual energy in the off-gas existing in the fume system. This paper focuses on the application of off-gas analyzers, sensors and process models to control and optimize "in-EAF" energy utilization efficiency. The paper will also discuss the application of heat recovery technology to EAF steelmaking.

Jan 1, 2015

By R. D. Brown

In the spring of 1977, Revenue Canada announced its intention to proceed in 1978 with a plan to impute a taxable benefit on interest-free and low-interest loans provided to employees. Such loan arrangements are often an important aspect of the compensation packages provided by many companies to their employees. Since the original announcement, there have been many submissions to Revenue Canada opposing this change, and the Finance Minister has now brought down a compromise solution with the introduction of a proposed amendment to the Income Tax Act. The amendment, which would not take effect until the 1979 taxation year, would require an employee, a shareholder or a related person to include a benefit in income measured as the difference between the interest on any such loan computed at bank prime rate and any interest actually paid. Only the amount of such a benefit in excess of $500 in a particular year would be required to be included in income. Of particular interest is the exclusion from these benefit rules of loans up to $50,000 in respect of the purchase of a house on the relocation of an employee and loans provided for the purchase of shares of an employer corporation.

Jan 1, 1978

By Robert E. Kirby

The potash mine and refinery of AMAX Chemical Corporation is located 26 miles east of Carlsbad on the north end of the potash producing areas. This property was developed between 1949-1952 and production of muriate began in August 1952. Two shafts, located 400 feet apart, were sunk to the ore zone 900 feet below the surface. A 15-foot diameter ore hoisting shaft equipped with a 1000-ton ore pocket, crusher and automatic skip loading equipment plus a 20-foot diameter service shaft with a curtain wall for exhausting air were provided. Sylvinite production to date has been from the first ore zone, stratigraphically, the lowest of ten identified mineralized zones in the salt section. This first ore zone has been the top producer of Muriate of Potash over the years. In our area we do have some very marginal mineralization in the third ore zone some 35 feet above the first. We have not mined from this seam as yet but we are investigating the economics very closely with access slopes and an experimental mining panel. Our ore seam is generally flat lying but does have local gentle rolling with grades from 2% to 5%. The mine was designed and developed from the beginning with conventional mining practices and rail haulage from the mining section to the ore pocket. As mining progressed in the early years, production increased from less than one million tons annually to a maximum of 3,935,000 tons in 1964. Efficiency also kept pace with the increasing production and continually improved until the efficiency of the production crews reached an average of 100.3 tons per manshift in 1964.

Jan 1, 1974

By David A. Milligan

This paper describes the Darwin Silver Recovery project, located 66 km (40 miles) outside of Lone Pine, near Darwin, Inyo County, California. A lead-zinc mine and a flotation concentrator were operated there from 1945 to 1957. By the time the mine was shut down, 1.53 Tg (1.69 million short tons) of tailings had been stored in ponds. An average silver assay of 47 mg/kg (1.38 troy oz/st) of tailings stimulated interest for commercial silver recovery. A heap leach process was developed in 1981 at the Tucson Research Center of Anaconda Minerals Company, a division of Atlantic Richfield Company. Agglomeration techniques were used on the ore since the fine grind did not allow direct heap leaching. Lime and cement were required as binders, Early laboratory tests showed that recoveries equal to those from an agitated leach could be achieved at lower capital and operating costs. Laboratory tests determined cyanide requirements, lime and cement usages, and percolation or leach rates, as well as confirming that a zinc precipitation step could recover the silver from the leach solution.

Jan 1, 1983

By J Wheeler

The objective of this paper is to examine the operation of high frequency screens in closed circuit grinding, where the outcomes achieved indicate favourable economic gains at the comminution stage and downstream processes, including flotation, dewatering, and filtration operations. The classification process in grinding circuits has been slowly evolving within the last century. The history of classification devices brings to mind rake classifiers and spiral classifiers, which although having higher efficiencies compared to hydrocyclones, were not able to keep pace with the evolution of concentrator equipment treating higher tonnages. This higher tonnage throughput has tended to drive the concept of utilising hydrocyclones as the classification stage in closed grinding circuits. The comminution process is commonly the most energy intensive stage of mineral processing. Researchers have determined that the classification stage in the comminution process has the greatest potential for improvement. This paper is intended to inform mineral process engineers of the benefits that high frequency screens offer over hydrocyclones. This will be done by reviewing the purpose for the evolution of classification in the comminution process, documenting past and recent studies, and explaining the modern technology that is currently available.

Aug 8, 2011

By Magnus Ek

After the installation of three new converters as part of the recent expansion of the Rönnskär smelter completed in 2000 work continues to further improve the converter operation. The converter upgrade led to an increase in blister copper taps from 150 tons per batch to more than 300 tons. The total cathode copper production increased from 130,000 tons in 1999 to 230,000 tons in 2001, the first year in full production. In recent years focus has been to improve operating practise, maximize the blowing time, extend the converter campaigns hence to reduce the specific brick consumption and improve the converter slag composition.

Jan 1, 2005

By Mark Ward

The Rincon del Tigre (RdT) complex is one of South America’s largest and best-developed mafic-ultramafic layered intrusions. It is set in the SE Bolivian lowlands, about 50 km from the Brazilian border.The BGS (British Geological Survey) and GEOBOL (Servicio Geologico de Bolivia) carried out an initial investigation of the RdT complex from 1976 to 1986. In this sense, the paper point out the geology background of The Rincon del Tigre, economical potential, typical ore secuence in laterite nickle deposit and pega pega erosional surface (Oligocene).

Apr 24, 2001

By Arash Khosravifar Ph. D. P. E., Thomas Torkelson P. E., Milad Souri Ph. D. P. E.

Kinematic demands from lateral ground deformations can be a major cause of damage to maritime and highway transportation structures such as wharves, piers, and bridges. These kinematic demands are different from the ground deformations in the free field in that the resisting forces from piles will reduce the ground deformations to some extent (i.e., pile pinning effect). Current design codes for wharf structures allow the beneficial resisting forces from pile pinning effects to be incorporated in pseudostatic slope stability analysis (e.g., ASCE/COPRI 61-14). While design guidelines that are specifically developed for bridge foundations provide recommendations on how to incorporate the pile pinning effects (e.g., Caltrans 2012), their applicability to wharf structures need to be evaluated. This study uses the results of a large-scale centrifuge test on a pile-supported wharf structure to evaluate the accuracy of available Newmark sliding block analysis in estimating the lateral ground deformations. Pile pinning effects are incorporated based on the approach outlined by Caltrans. The results of this study support the use of existing pile pinning methods that were primarily developed for bridge foundations in maritime structures (e.g., wharves and piers). It was found that median Newmark displacements provide a good estimate of the permanent end-of-shaking displacements and that the median plus 1 standard deviation Newmark displacements provide a good estimate of the peak transient displacements. Design considerations for use in the Newmark sliding block analysis to estimate the kinematic demands on piles are discussed.

Oct 1, 2022

By P. O. Lindahl

The U.S. Bureau of Mines initiated research to improve the safety and efficiency of transporting coal from deep underground mines using a balanced air-lift hydrohoist. A 50-m-high pilot-scale model was constructed and tested to evaluate the feasibility of hydraulically hoisting a coal-water slurry in a U-tube pipeline from the mine level to the surface with the assistance of compressed air. A prototype screw feeder is used to continuously compact and inject 5-cm or less run-of-mine coal into a pressurized 20-cm-diam pipeline. Production rates up to 40 metric tph at an airflow of 1.5 m3/min were achieved with the model, and coal size degradation was relatively minor. Modifications are in progress to achieve 100 tph at an airflow of 2.8 standard m3/min injected into the riser pipe. Pilot-scale results indicate that an air-lift hydrohoist system is a feasible, cost-effective alternative to conventional skip hoisting that can be installed in existing shafts or surface-drilled holes closer to the face area. Air-lift hydrohoisting offers advantages of infinitely adjustable slurry flow rates, reduced pressure at the point of coal injection, and flexible design that can be combined with hydraulic pumping. Proposed design changes are discussed for coal transport, mine layouts, ventilation, fire control, and escapeways using this system.

Jan 1, 1995

By G. Bitsianes

An experimental procedure was developed for studying magnetic roasting on a accurately-controlled laboratory scale. The loss-in-weight method was used and the course of reduction could be followed under a reducing gas atmosphere containing as many as five different components. Some important variables of the operation were checked on a marginal Mesabi iron ore containing porous and dense varieties of hematite as well as pure goethite. The conditions simulated were those for the grate roasting of a coarsely-sized ore burden. Temperature was maintained at 600°C; gas composition at 4.25% CO, 4.25% H2, 17.0% CO2, 15.0% H20, and 59.5% N2,, and gas flow rate at about 1,5 lineal feet per minute. The ore charge was composed of quarter-inch cubes. Under these conditions, the ore porosity was found to be one of the governing variables of the operation. Results showed that an ore size limitation existed as a function of this ore porosity. For efficient magnetic conversion, the size limit was 3/8 inch for very porous ores and about 65 mesh for very dense ores. An anomaly was noted in the weight losses incurred during actual magnetic conversion. For goethitic ores, these were generally about 13 per cent higher than could be accounted for theoretically. The effect was attributed to possible non-stoichiometric structures forming during the reduction process.

Jan 1, 1960

By J. H. Kelley

In this paper, we show that the methane emission and the dust generation in under-ground mining currently and in the future pose operational, health and safety conditions which adversely Impact face productivity and worker satisfaction. One solution is the use of a dual-aircourse system of ventilation. In this concept, one aircourse captures and exhausts to the surface the dust generated and the methane emitted in coal/mineral fragmentation while a second aircourse provides workers with cleaner air for breathing and comfort. Various dual-aircourse configurations adapted to the Variable Wall Miner are analyzed and compared with conventional mining in gassy seams, indicating a marked reduction in the required air quantity and the number of aircourses.

Jan 1, 1996

By H. B. Salisbury

As a part of a research program designed to help minimize national requirements for new mineral commodities by maximizing recovery of metals from domestic secondary resources, the Bureau of Mines investigated the development of economic methods for recovering copper and associated metals from complex electronic scrap. Three types were selected for research: (1) multiple-pin plugs and connectors, (2) obsolete aircraft radio assemblies, and (3) the magnetic fraction of shredded electronic scrap furnished by the Bureau's Avondale Research Center. The plugs and connectors, after incineration to remove plastic components and melting, yielded a brittle ingot, as did the internal portion of the radio assemblies. The brittle ingots were ground to minus 35-mesh for processing, and the magnetic material was used in the as-received condition. A process using pretreated or raw scrap as a copper precipitant in various concentrations of acidulated copper sulfate solution was developed as a means of effecting an initial separation and upgrading in the form of high-grade cement copper containing all or most of the precious metals.

Jan 1, 1981

By A. R. Taylor

The Bureau of Mines has determined the heat capacity and enthalpy values for beryllium sulfate (BeS04) throughout the temperature ranges of 10° to 300° K in an adiabatic calorimeter, and 350° to 860° K in a Bunsen-type ice calorimter, The heat-capacity data were extrapolated to 0° K, and smooth values of heat capacity, entropy, enthalpy function, and free-energy function were reported at 10-degree intervals between 0° and 300° K. The method of least squares was used to fit the enthalpy data with an algebraic equation. The equation also was used to calculate values of heat capacity, entropy, enthalpy function, and free-energy function at 50-degree intervals between 300° and 900° K.

Jan 1, 1963

By W. D. Dietzman

This Bureau of Mines report presents a continuation of statistics pertaining to distribution of petroleum reservoirs (or fields), wells, and production by depth and producing rate classification in the United States. These statistics show the change that has occurred since results of a similar study were published by the Bureau of Mines in 1967. Data are presented in tabular form by State for the 18 principal oil-producing States and by subdivision for the two larges t oil-producing States, Texas and Louisiana, Tabular summations and graphical illustrations are presented for the Nation. The data are classified by 4-barrel-of-oil-per-day rate increments up to 36 barrels and one increment of greater than 36 barrels of oil per day and by 2,000-foot depth increments up to 8,000 feet and one depth increment of greater than 8,000 feet. The overall average producing rates for States and the Nation have been published for many years; although such rates are useful, they are very general descriptions of producibility. A breakdown of production, wells, and reservoirs by various depths and rates and by State or by State subdivision provides a more detailed description of producibility.

Jan 1, 1976

By Ian Sherrell, Christian Cardoso, Henri Vepsäläinen, Guillermo Bermudez

Performance of mixing mechanisms in flotation cells is paramount, as inefficiencies can lead to financial losses through valuable minerals lost to tailings. Technological advancements have been implemented in flotation cells to optimize performance, but regardless of the efficacy of these developments, room for improvement may persist. Since its launch in 2005, FloatForce® has set a high industry standard for flotation mixing mechanisms. However, current mining trends call for sustainability-driven developments while improving metallurgical performance. Metso has recently introduced FloatForce®+, the latest iteration of FloatForce, developed through extensive laboratory, pilot, and industrial testing, aligning with mining sustainability trends. It has been designed to maximize recovery, reduce power draw and optimize manufacturing materials. This development stems from a redesigned rotor profile paired with a harmonizing stator configuration. This paper presents the development journey of Metso’s latest patented flotation mixing mechanism, an advancement to improve metallurgical performance at a high sustainable standard in flotation cells. The theory, CFD modeling and test work are discussed in detail.

Feb 1, 2025

By Weslei Viana Gabriel

O fluxo simétrico e distribuição de temperatura uniforme são de grande importância no processo de Lingotamento Contínuo de Beam Blank, porém a utilização de duas válvulas para alimentação do molde traz dificuldades operacionais relacionadas ao posicionamento das válvulas e controle de vazão. Neste sentido é interessante trabalhar com apenas uma válvula. Neste trabalho técnicas de modelagem física e matemática foram utilizadas para avaliar o fluxo de fluido no molde, comparando-se o caso em que se empregam duas válvulas tubulares, com aquele em que se utiliza apenas uma válvula. Verificou-se que esta última configuração resultou em uma mudança no comportamento do fluxo, aumento na profundidade de impacto, porém a velocidade na região do menisco não teve variação significativa em comparação com a utilização de duas válvulas tubulares.

Aug 16, 2017

By Priscila Graziela Melo Martins

O tamanho de grão austenítico é um parâmetro que influencia o desempenho de tratamentos térmicos em aços, assim como suas propriedades. Neste contexto, este trabalho investigou o uso de um reativo para ataque por imersão (240ml de água destilada, 2ml de HCl, 2g de ácido pícrico e 5 gotas de detergente neutro) para avaliar a influência da temperatura e do tempo de austenitização sobre o tamanho de grão austenítico de um aço ABNT1045 austenitizado nas temperaturas de 860ºC, 950ºC e 1100ºC por intervalos de tempo de 40, 90 e 180 minutos. As amostras austenitizadas foram temperadas em água, metalograficamente preparadas e atacadas com o reativo proposto com o objetivo de se revelar os antigos contornos de grãos austeníticos. Os tamanhos de grãos foram medidos com a utilização do software UMIAS de forma a possibilitar a determinação de distribuições estatísticas com quinhentas medidas para cada condição de tratamento. As amostras foram novamente preparadas e então atacadas com Nital 2%, sendo possível avaliar a influência do tamanho de grão austenítico sobre a morfologia da martensita. Pôde-se observar que, para o aço ABNT1045, a influência da temperatura de austenitização sobre o tamanho de grão austenítico é muito evidente e mais significativa do que a do tempo. Os valores de tamanho de grão se mostraram exponencialmente dependentes da temperatura, de forma que quanto maior o tamanho de grão austenítico, mais grosseira é a estrutura martensítica e menor é a dureza do material após a têmpera em água.

Aug 7, 2018

By J. I. Gazzarri

A model of solid oxide fuel cell AC impedance behaviour has been developed and is used to simulate the frequency response of a single cell with and without mechanical damage. The results indicate that the presence of mechanically induced damage within the components of a solid oxide fuel cell can be detected by comparing the frequency response of the undamaged cell with that of a cell in which in-plane cracking or delamination has occurred. The presence of such defects manifests itself as a new semicircle in the Nyquist impedance diagram of the full cell. A parametric study reveals the resolution capabilities of the method in terms of the geometrical characteristics of the defects.

Jan 1, 2005

By César Yuji Narita

Um dos problemas de aglomerados autorredutores utilizando cimento como aglomerante é a sua baixa resistência mecânica a temperaturas acima de 900°C levando-os à degradação durante a redução. Uma nova tecnologia propôs utilizar as propriedades de plasticidade térmica do carvão fóssil coqueificáveis como aglomerante, o que deu origem ao produto conhecido como CCB (Carbon Composite Iron Ore Hot Briquette). Este trabalho tem como objetivo propor uma rota alternativa para a fabricação dos briquetes autorredutores e estudar o efeito de variáveis de processo na resistência à compressão dos mesmos. O método utilizado na obtenção dos briquetes foi de compactação em matriz cilíndrica de misturas de finos de carvão fóssil coqueificável (log(máxima fluidez) = 2,48) e minério de ferro (pellet feed) seguida de tratamento térmico. Foram realizados testes variando granulometria do carvão, pressão de compactação, taxa de aquecimento e proporção entre carvão e minério e investigados os efeitos dessas variáveis em relação à resistência à compressão e à densidade dos briquetes produzidos. Foi observado que a resistência à compressão obtida nos briquetes produzidos via briquetagem a frio seguida de tratamento térmico são comparáveis com os CCBs.

Aug 1, 2018