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By Paula Ana Paiva

The high economic value and unique technological properties of the platinum-group metals (PGMs), plus their growing scarcity in the Earth’s crust, justify the crucial importance of developing recycling practices for PGMs end-of-life materials. Examples of top devices relying on the use of PGMs are automotive and industrial catalysts, and electrical and electronics equipment. This article critically describes the most recent research on the use of solvent extraction to recover one PGM, palladium, from spent catalysts. Some groups focus on the development of schemes involving commercial extractants, while others prefer to design specific molecules to efficiently and selectively recover palladium from these particular complex leaching solutions. Examples of commercial extractants proposed for the former schemes are Alamine® 308, TBP and LIX® 84I; while on the other hand, sulfur-containing diamides, thioamides, thiocarbamates, and dithioethers have recently been developed. Ionic liquids have to be mentioned too.

By R. S. Kalyoncu

Materials demands by the advancing process technologies, desire for higher performance and durability, and improved efficiency in combustion processes, such as applications in heat engines, heat exchanges, and batteries have added to the driving force fueling R&D efforts for the development of components with the combined characteristics of metals and non-metals. These new materials involve refined and specialized microstructures that can lead to improvements in the performance characteristics and durability new technological applications require. Fabrication and sintering methods, once believed to be sufficient, alone, have been found to be inadequate in the manufacture of such advanced components. Realization of the importance of the starting powders has led to efforts to produce materials of ultrahigh purity and ultrafine particle size with very narrow particle size distributions. Such powder characteristics are essential for the fabrication of components with high density and with the desired mechanical, electrical, or magnetic properties called for by the specific application. Novel ultrafine and ultrapure powder preparation techniques are discussed and effects of impurities on the powder characteristics, particle size and morphology, sintering behavior and properties of the finished product are elucidated.

Jan 1, 1992

By G. Gao

Flyash from municipal solid waste (MSW) incinerators is frequently classified as a characteristic hazardous waste due to its lead and cadmium content. Extensive investigation has therefore been carried out to detoxity the flyash by leaching and to recover lead, cadmium and zinc. Detoxification can be accomplished by leaching in HCI/NaCI solutions. Optimization of leaching conditions for effective detoxification and subsequent metal recovery can be achieved by controlling the acidity of the lixiviant and flyash to lixivaint ratio. Lead and cadmium In the leaching solution is recovered by cementation with zinc dust. Leaching and cementation experiments have shown that zinc concentrations suitable for electrowinning, > 15 g/liter, can be achieved. Experiments have also been performed to determine the effects of pH, particle size of the zinc dust used, quantity of zinc added and dissolved impurities on the cementation kinetics. After recovery of lead and cadmium, electrowinning or electrowinning coupled with solvent extraction can be used to recover zinc. A process flowsheet is presented.

Jan 1, 1991

This United States Bureau of Mines study is based on a review of U.S. mine fire accidents that occurred from 1970 through 1989. Information on these accidents was obtained through investigative reports written by Mine Safety and Health Administration personnel. For this study, 260 mine fire accident reports were examined. A previous Bureau research effort established that fires causing fatalities were more likely to occur in haulage entries than at any other underground location. This study has found that the most prolific source of haulage entry fires was the inadvertent grounding of trolley wires. The largest segment (15 out of 40 trolley wire fires) resulted from not maintaining adequate clearance between the trolley wire and the vehicle. Several novel fire prevention and control ideas have evolved in response to frequently occurring fire-related problems. These included; discriminating power isolation devices, wire cutting devices, more accessible fire extinguishers, vehicle overcurrent protection, and vehicle fire suppression.

Jan 1, 1994

By J. Gao, H. O. Gekonde, S. V. Subramanian

"The functional role of inclusions at low cutting speeds is to promote ductile fracture in chip formation process, whereas the role of inclusions at high cutting speeds is to prevent tool crater wear by suppressing the tribological phenomenon of seizure at the tool-chip interface. Glassy oxide inclusions are engineered into the workpiece to form a viscous layer in-situ at the tool-chip interface at high cutting speeds. The viscous layer lubricates the tool-chip interface to prevent the seizure. In comparison with the large volume fraction of inclusions needed for promoting ductile fracture at low cutting speeds, the amount of inclusions required for lubricating the toolchip interface at high cutting speeds is very small and is in the range that is typical of clean steels. The chip fracture process at high cutting speeds is aided by strain rate hardening of the matrix, which facilitates chip disposal of relatively clean steel.Inclusion engineering for high speed machining involves the control of the rheology and composition of inclusions to meet target viscosity at the tool-chip interface. The application of thermodynamic models in controlled production of inclusions in steels designed for high speed machining is discussed."

Jan 1, 1998

By Peter R. Drummond

THE paper consists of four sections: (1) a discussion of early work; (2) presentation of the results of a chemical investigation of Falcon-bridge nickel-copper blast-furnace matte; (3) application of the results of this investigation to mattes in general; and ( 4) a summary of conclusions. All general discussion will be confined to the fundamental system of ferrous-cuprous sulphides (FeS-Cu2S). Nickel-, lead-, and zinc-bearing mattes will be treated as minor varieties of the parent system. DISCUSSION OF EARLY INVESTIGATIONS Matte investigations may be divided into three classes: first, those treating the sulphides as alloys-theoretical studies of the system FeS-Cu2S, such as those of Hofman (ll)t or Carpenter and Hayward (2); second, chemical research on mattes made under smelter conditions, such as that carried out by Hawley (3) or Avetision ( 4); third, combinations of the . above, such as the investigations of Gibb and Philp (5) or Fulton and Goodner (6). Much research in the first of these classes, including determinations of . freezing points and of data for structure-composition diagrams of the system FeS-Cu2S, was carried out in the period 1890-1910. LeChatelier and Ziegler (1, 13) proved that FeS, when heated alone above its melting point, dissociated in part, and Friedrich ( quoted by Fulton, 6) showed the same for Cu2S. The reactions may be expressed by the following equations: [xFeS yFe + yS (volatilized)+ (x -y)FeS xCu2S )'Cu+ yS ( vohtilized) + (x -)')Cu,S ] Sulphur is lost by volatilization, leaving a melt of metallic iron plus ferrous sulphide in the one case, and of metallic copper plus cuprous sulphide in the other. If the mixed sulphides are heated far above their melting points, there results either an iron-rich matte containing Fe-FeS-Cu2S or a copper-rich matte containing FeS-Cu2S3-Cu, depending on the relative amounts of each sulphide in the mixture.

Jan 1, 1940

By A. Bozorgzadeh, B. M. Jensen, B. N. Koelling, B. R. Murtaugh

"The Service Base mooring system originally consisted of two general types of structures, 19 timber piles cabled together and steel three-legged pipe piles. The St. Louis District fleet moored to the fleet barges which were tied off to shore-side concrete deadman and supported on the landward side by the timber and steel piles. The purpose of this project was to replace the existing floating wharf mooring system at the St. Louis Service Base. The Marine Design Center of the U.S. Corps of Engineers developed a three pile cluster system concept. The clusters consisted of one vertical pile and two batter piles. Piles in rock sockets were selected to resist the uplift loads due to high wind loads on the tall, spare lock gates stored at the floating wharf. This paper focuses on the design of the rock sockets for steel pipe piles with large uplift loads and the lessons learned during the design and construction of this system.INTRODUCTIONBackgroundThe U.S. Army Corps of Engineers’ St. Louis District is located at the critical transition point on the Mississippi River where it is a “locking river” north of St. Louis and an “open river” to the south. The St. Louis District is responsible for maintaining navigation channels on the Mississippi River, the Illinois River and the Kaskaskia River. It is also responsible for the operation and maintenance of five locks and dams within its geographic boundaries.The St. Louis District utilizes a fleet of vessels (dredges, crane barges, motor vessels, and barges) to support the navigation mission identified above. The St. Louis District Service Base, located in St. Louis, Missouri, serves as the base of operations for the district fleet. This riverfront facility originally consisted of a floating wharf, a railroad trestle, and a walkway down the river bank to the floating wharf. Historically, there have been two fleeting areas at the Service Base. The main fleeting area was approximately 965 feet long and consisted of six fleet barges (Figure 1). This area supported the Dredge Potter and its attendant fleet. The upper fleeting area was approximately 1,050 feet long and consisted of various stop log, crane and work barges, dredge pipe pontoons and work flats."

Jan 1, 2017

By Ricardo Oliveira Gallart de Menezes, Claudio Gerheim Porto, Reiner Neumann

The Jiboia heavy mineral sands deposit is a new discovery associated with the São Francisco River delta on the northern coast of Sergipe state. The identified resources are part of the much larger mineralized trend. Mineralization is hosted in paleodunes deposited on Holocene marine terraces (Fig. 1). The dunes are up to 30 m above sea level, and mineralization occur from 6 m above sea level upward. The main ore minerals constitute pseudorutile, ilmenite, zircon, rutile and monazite. This work presents a thorough characterization of the mineralogy and granulometric distribution of the Jiboia orebody.

Apr 1, 2024

By A. T. Harris

Ground quartzite, known in the industry as amorphous silica, is produced from a quartzite deposit near Honey Brook, Pa., by George F. Pettinos, Inc., of Bala-Cynwyd, Pa. The quartzite is mined by the open pit method and processed in a mill at the mine. The operation regularly produces five standard grades of sand and one grade of crushed stone; however, the company accepts special orders and will produce material to meet the customer's specifications. Beneficiation (chiefly crushing and screening) is controlled by laboratory screen tests on samples taken during preparation of the sand. The chief uses of the sand are for foundry operations, furnace lining, concrete aggregate, and Other specialized uses. The quartzite in this deposit is of uniform composition and does not require control by chemical analysis. However, for special purposes, analysis will be furnished.

Jan 1, 1965

By Brian E. Ladd

"A load test program was performed on two auger cast piles constructed in the Inner Coastal Plain geology of North Carolina. Both test piles were installed through Coastal Plain deposits and into underlying Piedmont residual soils; one test pile was embedded into partially weathered rock (PWR). The recommended 100-ton design load was confirmed by a test program that included instrumenting the piles with strain gages. The two piles performed differently during the load tests due to the effect of embedment into PWR. Loading Test Pile No. 1, which was not embedded into PWR, to failure at about 230% of the design compressive load allowed for evaluation of the mobilization of the ultimate shaft and end bearing resistances. Mobilization pile resistance was evaluated by comparing shaft and end bearing resistances to top of pile deflection (d) normalized by the pile diameter (D). For Test Pile No. 1, the ultimate average shaft resistance was achieved at d /D of about 7.5% and ultimate end bearing resistance at d /D of about 9.5%. Test Pile No. 2, embedded into PWR, achieved a d /D of only about 4% at 200% of the design load and was not loaded to failure. Shaft resistance was mobilized at a different rate within each individual geologic layer, i.e. ultimate shaft resistance did not occur simultaneously for all geologic layers. As the available total shaft resistance was exceeded and end bearing mobilized, the unit shaft resistances reduced from the peak values. A modified Davisson offset using d /D of about 6.5% appears applicable for evaluating the ultimate capacity of auger cast piles in the Inner Coastal Plain.INTRODUCTIONAuger-cast-in-place (ACIP) piling was developed in the 1940’s and patented in 1956 (Neely, 1991). Since patent expiration in 1973, ACIP piles are abundantly used in the United States, particularly in the southeast. However, most literature addresses driven piles constructed in sand and clay with lesser discussion of drilled piles. Conventional design methodologies (a- method, ß-method, SPT or CPT correlations, etc.) are based on data derived from numerous projects in a great variety of geologies. O’Neil (2001) notes that there are significant levels of uncertainty in the “universal” databases as evidenced by coefficients of variation of 0.35 to 0.40 for geotechnical parameters (su, SPT-Nvalue, etc.) used to estimate pile capacities.There is a need to develop local databases developed from data obtained from load tests that measure shaft resistance and end bearing. This paper presents the results of load tests conducted on axially loaded auger-cast-in-place piles constructed in the Inner Coastal Plain geology of North Carolina. Shaft resistance, end bearing, and movements that initiated mobilization of these resistances are described. The information presented herein can be used to refine geotechnical correlations and parameters applied in auger cast pile design methodologies."

Jan 1, 2017

By P. Fawell, C. Castillo, C. Ihle

"The need to reduce fresh water consumption has pushed many Chilean mining companies to utilize seawater obtained from distant locations. At the same time, increasing amounts of fine particles in copper tailings raise new operational challenges, in particular, the thickening and transport of tailings featuring significant fine fractions, which are predominantly clays. In the present paper, we study the role of salinity – using seawater and NaCl – on the flocculation efficiency of copper sulphide tailings to which kaolinite was added. To mimic the water recovery stage in thickeners, flocculation has been induced in jar tests and the corresponding aggregate size distribution has been estimated from chord length distribution data obtained using a focused beam reflectance measurement (FBRM) probe, at various mean turbulence intensities. Results show that for constant flocculant dosing, a measurable influence of the salt on the resulting aggregation exists. For each case, resulting optimal turbulence levels are also reported, a particularly interesting feature when comparing flocculation efficiency of the coarse and fine fraction. INTRODUCTION The concentration of copper minerals through comminution and flotation is intensive in the use of fresh water. The need to reduce the consumption of fresh water and the environmental standards associated with increasingly demanding mining operations have driven improvements in the techniques of recovering water from tailings. The challenges are even greater when required to treat minerals with high clay contents. In Chile, kaolinite is one of the most important clays to consider due to its abundance in the tailings from many operations. The most common and highest throughput unit operation in the mining industry for the recovery of water from tailings is gravity thickening, with sedimentation of fine particles assisted by flocculation. Flocculation is the process of forming aggregates by contacting the suspended particles with a flocculant. The flocculant is typically a water-soluble synthetic long-chain polymer, where copolymers of acrylamide and sodium acrylate are the most common types used in the Chilean mining industry. The aggregation mechanism includes the following key steps: (1) flocculant distribution through the suspended particles, (2) flocculant adsorption onto particle surfaces, and (3) collisions between particles leading to polymer bridging to form aggregates, but concurrently (4) breakage of aggregates becomes a factor under prolonged shear (Gregory, 1988)."

Jan 1, 2018

By AIME AIME

In the present number of Mining and Metallurgy, issued on the fiftieth anniversary of the founding of the Institute, it appears appropriate to chronicle a few of the interesting incidents respecting its early life. We are fortunate in being able to cull the following notes from unpublished manuscripts of Doctor Raymond and Doctor Drinker, than whom no other members could have written with greater exactness and fidelity. THE seventh decade of the 19th century may be said to have marked an. era in the history of the world. Industrially and .commercially it was marked by the wide application and utilization of discoveries already made, which came to their full effect at this period in steamships, railways, telegraph and cable lines; the standardization of parts in machines, from watches to locomotives; the use of 'dynamite, antiseptic surgery, the open-hearth steel process, the compressed-air rock-drill, the electric generator, and the Gatling gun. Through the opening of the Suez canal in 1870 the maritime trade of the world was revolutionized, sailing vessels were supplanted by steamers, while ocean cables and ocean "tramps" brought about far more rapid movement of commerce than had before been experienced. Politically, this period was marked by the sudden birth of the German empire and the beginning of that intensive internal development of the national resources of that empire in preparation for colonial extension and war, the amazing result of which has been made evident by the recent world conflict. In the United States, the significance of this decade was peculiarly important. The re-admission to the union of Virginia, Mississippi, Texas and Georgia in

Jan 1, 1921

By Oscar A. Glaeser

INDUSTRIAL relations in the United States Smelting Refining and Mining Company's Western operations covers the field of personnel and labor relations, and the principal aims are to render service to the employes of the Company and to its operating departments. Accident prevention Safety is a primary function. A safety engineer is employed at each operation. The wholehearted support of Company officials, staff, and the working force has been most successful in preventing accidents. Constant vigilance has been combined with a policy of building safety into all operating activities whether these are in the construction of a new facility, the developmnt of a mining system, or the direction of the working force. That this policy has produced results is attested to by the fact that the accident frequency rate at the Company's major mining operations in Utah has been reduced approximately 75 per cent in the ten-year period ending Dec. 31. 1946.

Jan 1, 1948

By Eugene Frey

"INTRODUCTION The Blue Bell fluorite deposits were examined in August and November 1944 by an engineer 3/ of the Bureau of Mines, and an underground project was set up. The Bureau of Mines began development of fluorite here February 10, 1945, and completed its survey on June 21, 1946.ACKNOWLEDGMENTSIn its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each exploratory project as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepared the final report. The Metallurgical Branch, C. C. Ralston, chief, analyzes samples and perform beneficiaticn tests. The exploratory project was under the direction of Paul T. Allsman, chief, Salt Lake City Division, Mining Branch. Acknow¬ledgment is due R. Thurston of the Federal Geological Survey for mapping the topography of the area, and to F. H. Gunnell and W. A. Young of the divisional office for detailed mapping of the surface and underground development and interpretation of the results.The chemical analyses included in this report was performed under the direction of H. E. Peterson, analytical chemist; the petrographic studies on the ore were written by LaMar Evans, petrographer; and the beneficiaticn section was written by C. H. Schack, metallurgist, under the direction of S. R. Zimmerley, chief, Salt Lake City Division, Metallurgical Branch."

Jul 1, 1947

By D. R. Hanson

This Bureau of Mines study examines the acoustic vibrational spectra of rock slabs in the range of 0 to 5,000 Hz. The power spectra of so-called drummy rocks were found to be diagnostically enhanced in the range of 200 to 1,000 Hz. Comparison of the power in this band with that in a band from 3,000 to 3,500 Hz provides a quantitative measure of rock stability. A prototype field instrument was designed, constructed, and field-tested. This battery-powered instrument computes the power contained in the two frequency bands mentioned, compares the magnitude of these two quantities, and displays a number that is related to the detachment of the block tested. Field tests show that this instrument is capable of giving reliable measurements of block stability under conditions of noise and dust that would seriously degrade the accuracy of normal sounding techniques.

Jan 1, 1985

When I was first asked to give a paper on work-life balance in the mining industry I was both excited and aware of the incongruity of my position. I have never worked in mining operations nor have I had any experience that approximates the on-site lifestyle. IÆm not really an adventurer or a traveller, I prefer writing and research to hands-on activities and IÆve never worked further than twenty minutes away from home. The perspective I offer is thus largely an objective one. I say largely since I grew up in a family where my parents work arrangements involved long-distance commuting; my dad continues to work FIFO at a coalmine in Blackwater until this day. Perhaps my tortoise-like existence is a rebellion against his flighty movements. The analysis I will be presenting today draws together a variety of sources, from member anecdotes and research on FIFO and work-life balance to the popular philosophy writings of a bald Englishman with a French name. I am speaking of the famous writer, Alain de Botton, whose television show æThe Consolations of PhilosophyÆ you may have seen on the ABC. Work-life balance is a term that gets a lot of mileage in corporate brochures and at breakfast seminars. But like many terms that get bandied around in the human resources circuit, from æteam synergyÆ to æperformance optimisationÆ, I am frequently perplexed as to what it actually means. Corporate websites are at pains to emphasise the high priority that they place on the needs of the whole person. Yet in terms of substantive content, a commitment to work-life balance often seems to translate into little more than the option to take a few morning yoga classes in exchange for working a seventy-hour week. As extended work hours have taken their toll, leading to high attrition of professionals across all industries, employers are increasingly expending resources to discover just what lies behind this buzz word. The challenge for companies is to find meaningful strategies to help employees better integrate different aspects of their lives in a new era of work, as employees are sending the message that they are not willing to play work, social life and leisure off against each other in a zero sum game.

Jan 1, 2005

By Ralillie Lopes Carvalho

O presente trabalho apresenta um estudo da influência do tratamento de nitretação a plasma sobre a dureza de lâminas utilizadas em prensa-facas de um picador de toras industrial. Tais peças são fabricadas em ligas com alto teor de Cromo e Carbono, assemelhando-se quimicamente aos aços para trabalho a frio AISI da série D. Para o estudo em questão, pequenas amostras das lâminas receberam tratamento térmico de têmpera e duplo revenido,e posteriormente foram nitretadas a plasma por 30, 90, 180, 360 minutos, em temperatura de 450°C, com pressão fixada em 2 Torr e mistura gasosa de 20%N2 e 80%H2. Logo após foram realizadas análises metalográficas com auxílio de microscópio óptico, ensaio de dureza superficial e perfil de dureza com microdurômetro em escala Vickers. Os resultados mostraram que para todos os tempos de tratamento houve endurecimento superficial em relação ao material não tratado, onde o tempo de 180 minutos propiciou a formação de camada com maior valor médio de dureza superficial “1171,20 HV”.

Aug 16, 2017

By S. Pastor, S. Hahn

"As the concept of autonomous haulage systems (AHS) moves from proto-types to production-ready applications, the operating performance of the haul road will become ‘mission critical’ to the overall success of autonomy in mining. Deterioration in road performance will require remediation, human intervention and significant, albeit temporary, changes to operating procedures, to accommodate road maintenance. With autonomous trucks comes the opportunity to reduce road formation and operating width, and therefore generating potentially significantly reductions in stripping ratios and improvements to mine economics, but only if the design of the road, and it’s associated deterioration rate, is predictable and manageable, based both on the materials used to construct the road and the maintenance interventions to be carried out on the road. This paper presents the assessment of a digital photogrammetric approach to the characterization of a mine haul road surfacing, or wearing course material. Design and maintenance parameters for these roads are currently determined from physical particle size distribution (PSD) assessments of ‘in-road’ material. However, this approach does not accommodate the need, nor leverage the benefits from, AHS. The digital imaging approach is assessed in this paper, using two standard digital analysis software tools, together with in-service mine haul road wearing course samples and images which are assessed to determine the applicability and reliability of the approach to deliver a real-time assessment of haul road surfacing conditions and thus to identify the road maintenance interventions required to address deterioration. INTRODUCTION Enhancements in mine road design, construction and management for the past 20 or more years has largely been focused on short-term tactical needs. These improvements have not been matched by advances in the fundamental technologies that underpin mine road design and management, and although the quality of mine roads have probably increased, many of fundamental and longer-term issues have yet to be addressed. With AHS’s evolving from prototype to production applications, any decision to implement these systems in a mine requires a thorough evaluation of impacts, not only operational improvements, but the inter-connectivity of this autonomy technology to other organizational processes. In developing an understanding, the full interactions that may affect autonomous truck behaviour due to changes in various sub-systems or external environments, haul road conditions and operating performance is a key consideration. This is as true in autonomous as well as in conventional mine truck-based hauling systems where the mine haul road network is a critical and vital component of the production process."

Jan 1, 2015

By J. D. Ramsdell

The purpose of this investigation was to determine the effects of the impurities, oxygen, nitrogen, carbon, and iron (in low percentages) on the mechanical properties of electrolytic titanium. The strength and hardness of binary Ti-O, Ti-N, and Ti-C alloys are linear functions of alloy content in the composition range investigated. Compared to oxygen and carbon, nitro-gen is the most effective strengthener and hardener, followed by oxygen, then carbon. When the carbon concentration is above 0.10 percent, carbides are present, and strength and hardness are relatively unchanged. For equivalent hardness levels, Ti-Fe alloys are stronger than binary titanium alloys containing oxygen, nitrogen, or carbon. However, the strengthening is related to the presence of transformed beta in the structure.

Jan 1, 1960

By Gary Cavanough

The spontaneous exothermic reaction of ammonium nitrate explosives with sulphide-containing rocks, commonly referred to as reactive ground, is a site-specific condition that can lead to spontaneous detonations. Mine sites typically carry out regular assessment of ground for reactivity. In Australia, reactive ground testing is conducted according to the Australasian Explosives Industry Safety Group (AEISG) Code of Practice. This paper presents a new method to assess reactive ground. The new method can be completed on the mine site or in the laboratory. The new method allows samples to be tested in hours not weeks, as required when using the method prescribed in the AEISG Code of Practice. The new method also provides an explanation of why ground is reactive or not reactive, Whereas the AEISG Code of Practice provides a reactive, not reactive or marginal results with no understanding of reason for these results. Case studies on the use of weathering agents, pH, sulphide content and carbonate content will be reported. These case studies identify instances where the testing as per the AEISG Code of Practice provides false positive and false negative results. A false positive result will require the use of inhibited products when they are not actually required which increases costs and reduces productivity due to the need to used multiple explosive products. A false negative result increases the risk of an unplanned initiation of a blast hole.

Feb 6, 2023