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By W. R. Crane

Subsidence and ground movement are phenomena common to and attendant upon practically all large-scale mining operations, and under certain conditions may occur in all workings, large and small. The interpretation of the cause of failure in rock masses involves a study of the nature of plants of weakness common to all rocks. The dominating planes of weakness can readily be determined by observation in any given locality, and in order of importance in the study of subsidence are (1) faulting planes, (2) bedding planes, (3) joint planes, and (4) other prominent planes of weakness such as thrust and shear planes and contacts. This report has mainly to do with the third item, joint planes, and is a preliminary statement which t to be followed by a more complete report in bulletin form.

Jan 1, 1931

By James R. McVey

Tests during pillar robbing, longwall operations, and other mining activities indicate that roof-floor convergence rates can be used as an indicator of imminent roof failure. A large number of electrical-mechanical devices have been built to measure convergence as well as convergence rates, but most obstruct mine traffic and are costly and time consuming to install. The Bureau of Mines has designed and is evaluating three types of small ultrasonic units to make these measurements. The new instruments provide nonobstructing measurements up to 35 ft away. The ultrasonic transducers can be attached to a roof bolt, placed in an unsupported area (by means of a toss basket), or handheld. Total distance to the target and rate of closure are displayed digitally to 0.001 ft and 0.01 ft/min, respectively.

Jan 1, 1984

By A. D. Mah

To assist Bureau of Mines research in extractive metallurgy and to add to the thermodynamic data base useful to others, energy calculations were made for 63 reactions relating to investigations on the production of anhydrous aluminum chloride from chlorination of clay.

Jan 1, 1982

By R. Carson Dalzell

The use of nuclear fission for chemical process heat offers the special advantage of high temperature, limited only by materials of construction. The process heat may be supplied economically at elevated pressures, since no compression of combustion air is required. For the initial effort in developing a high-temperature reactor, the indirect cycle, using helium as the heat-transfer medium, was chosen. The major problems are the design of high-temperature fuel elements, construction of an exchanger to transfer heat to process streams in the range of 2,500° F., and development of compressors capable of recycling helium at 1,000° F. and above. A conceptual design of a nuclear reactor to furnish process heat for coal gasification has been made. Spherical fuel elements utilizing a graphite structure, impregnated with uranium carbide fuel, were chosen, as spheres offer the possibility of easier loading and unloading of the reactor. Calculations of pressure drop and gas-pumping power for the system are included.

Jan 1, 1959

By R. L. Grant

The Bureau of Mines applied automatic computational methods to analyze the degree of correlation between sound transmission and atmospheric conditions. Statistical analysis of data collected over a 5-month period indicated that the following weather variables, listed in order of decreasing importance) have a significant effect on the transmission of sound in the atmosphere: 1. Wind velocity and wind direction. Winds in the direction of travel of the sound wave increase the sound intensity and duration. 2. Barometric pressure. High pressures are related to low sound intensities and durations. 3. Atmospheric temperature. High temperatures are related to low sound intensities and durations. Inversion of the atmospheric temperature did not appear to affect sound transmission under the conditions of this study.

Jan 1, 1967

By W. L. Crentz

In Fayette County, the Pittsburgh bed has been the major source of production for almost two centuries. Although historical documentation is not available, there is evidence, that the Pittsburgh bed may have been discovered in Fayette County near Mt. Braddock, Pa., as early as 1753. The earliest known reference to coal in western Pennsylvania was recorded in 1758 by a Quaker trader, James .Kenny, who reported having seen coal in Fayette County. The production of coke from Pittsburgh coal was begun in 1841, when two 10-foot beehive ovens were erected in the Connellsville region to make coke .for shipment by river to the market. The Connellsville, region extends from Latrobe, Pa., in Westmoreland County to South of Uniontown, in Fayette County. Connellsville coke was used with great success in the Clinton furnace in 1859.

Jan 1, 1951

By P. C. Good

High-purity chromium was prepared in massive form by the electrolysis of chromium trioxide solution at high temperatures. The metal thus obtained, containing 50 to 150 p.p.m. of oxygen, 20 p.p.m. of nitrogen, and traces of metallic impurities, could be hot-worked to rod and sheet and drawn to wire ductile at room temperatures. Optimum concentrations and operating conditions were established for the deposition of chromium from chromic acid baths containing sulfate, fluoride, and silicofluoride ions. Current efficiencies of 13 percent were attained with baths containing sulfate ion, and efficiencies of 40 to 44 percent with baths containing fluoride and silicofluoride ions. Cation exchange resins were used for removing metallic impurities from chromic acid solutions containing sulfate ion; solutions containing fluoride and silicofluoride ions were purified by recrystallization.

Jan 1, 1960

By Robert E. Barieau

This report gives the principles of the method used by the Helium Research Center of the Bureau of Mines when solving nonlinear-regression problems and contains the mathematical equations necessary to accomplish the following objectives: the evaluation of the parameters in such a way that the sum of the weighted squares of the residuals of an experimental observable is a true minimum, regardless of the functional relationship between the variables and these parameters; and the evaluation of all variances and covariances of the parameters by means of the usual approximation of the law for the propagation of errors.

Jan 1, 1967

By O. C. Blade

A summary of the characteristics of motor gasoline for the winter 1951-52 is presented in table I, and for comparison, a similar summary for the winter 1950-51 is shown in table 2. Trends of some of the more important characteristics over a period of years are shown in figures 1 and 2. The results of this survey show that octane numbers have risen slightly since the summer of 1951 but are below the record levels of the winter of 1950-51. The fractions of a unit change since the summer preceding have resulted in the research and motor-method octane values being virtually the same as the figures for the survey of summer 1950. In volatility characteristics the winter gasolines have changed very little. Average Reid vapor pressures are 10.5 pounds for both grades of fuel compared to 10.4 and 10.5 pounds for premium and regular-price gasolines, respectively, of the winter of 1950-51.

Jan 1, 1952

By Nicholls Harry R.

The Bureau of Mines studied the effect of varying the, diameter of explosive charges on the generation and propagation of strain waves. The parameters compared were strain amplitude, impulse, energy, and pulse shape. Three different explosives were detonated in three different charge diameters. Charges of cast 50/50 pentolite-detonated at the same velocity in 5-, 2.5-, and 1.5-inch diameters. Charges of ammonium nitrate-fuel oil prills and 45-percent semigelatin dynamite showed a strong detonation rate-diameter dependency. Detonation of these two explosives was considered nonideal. Differences in the diameter of the charge caused less difference in the strain-generating abilities of pentolite than in those of the other two explosives. This was also true for impulse and energy. Rise and fall times of the strain pulses for all three explosives were proportional to detonation time and cavity volume, respectively.

Jan 1, 1966

By M. S. Oudenhoven

This Bureau of Mines investigation was conducted to obtain an experimental solution of stress changes in the vicinity of a circular opening in an infinite plate. Plates were stressed biaxially in compression and subjected, by four different-length shoes, to a uniform pressure at opposing points on the opening periphery. The principal stresses along the vertical and horizontal axes, which result from peripheral pressure, were obtained from the photoelastic analysis of four frozen-stress epoxy models. These principal stresses were then super-imposed on the mathematically determined principal stresses (along the same axes) obtained from a theoretical biaxial stress field in which the magnitude of the lateral pressure was one-third that of the vertical pressure. The results indicate that an increase in shoe length increases the radial compressive stress and the tangential tensile stress (except tangential compression at r/a = 1, which exists for all shoe lengths). Also, a partial control of the stresses within one-half radius of the opening surface is accomplished by a change in the magnitude and placement of peripheral pressure.

Jan 1, 1966

By K. O. Bennington

The thermodynamic properties of hedenbergite, of composition [(Ca0,9516) (Mg0,0583Fe2+0.7134 Fe3+0.0934 Mn0,1366) (Si206)], were experimentally determined at the Bureau of Mines. The standard enthalpy of formation determined by hydrofluoric acid solution calorimetry is AHf298 = -680.96±0.855 kcal/mol. The standard enthalpy of formation from the oxides is AR-96 = -24.55±0.485 kcal/mol. Low-temperature heat capacities were determined by adiabatic calorimetry from 12.3 to 300.1 K. The derived standard entropy is S-98 - 41.218±0.148 cal/mol-K. High-temperature heat capacities were measured with a differential scanning calorim¬eter from 397 to 1,147 K. These experimentally determined data were combined with data from the literature to calculate the Gibbs energies of formation and equilibrium constants of formation over the temperature range of measurements. Standard enthalpies of formation are given as a function of temperature. The standard Gibbs energy of formation at 298.15 K is AGf298 = -641.90±0.86 kcal/mol.

Jan 1, 1984

A new horizontal borehole packer for use in coal beds has been developed. This packer utilizes a principal of operation which has not previously been used. The resulting packer is less costly to purchase, can be easily repaired in the field with inexpensive expendable parts. This report describes the development and testing of the new packer and the evaluation of commercially available packers.

Jan 1, 1971

By Jr. Gabler

World resources of platinum-group metals appear ample for the foreseeable future; however, political and economic events in the last two decades have caused concern over the availability and reliability of an uninterrupted supply. Because of this concern, the U.S. Congress requested that the U.S. Bureau of Mines initiate a study of the flow of platinum-group metals in the economy that would delineate and quantify the production areas in which metal values are lost. As a result, the Bureau has developed a computerized commodity flow model for strategic and critical materials. Major attributes of this flow model are as follows: (1) it is generic and applicable to most commodities and (2) it can be updated as supply, demand, and/or production data change. The original model developed for cobalt, with slight modifications, was used to track the flow of platinum-group metals. This report follows the flow of platinum-group metals through their metallurgical, catalytic, and chemical applications and highlights areas in which significant losses occur because of downgrading, export, or disposal. The study indicates that materials containing about 63,426 kg of platinum-group metals were lost or could not be traced in 1989, representing about 63 pct of U.S. domestic consumption.

Jan 1, 1991

By M. N. Plis

This report describes the initial results of long-range research on bit life conducted by the Bureau of Mines. Three commercial bit designs -a round-nose radial, 60° conical, and 90° conical with tungsten carbide (WC) inserts -and five experimental bits were tested. Four of the experimental bits were radial designs using polycrystalline diamond compact (PDC) inserts. The fifth was a 90° conical with an oversize WC insert. Bits were worn on a high-silica sandstone typical of coal mine roofs. The bits were mounted on a 34-in-diam drum section that provided a bit speed of 565 ft/min. Cutting forces were measured on a modified vertical slotter using a three-axis force dynamometer and recorded on an FM magnetic tape recorder. Changes in cutting forces, bit weight, and airborne dust due to gradual abrasive wear and catastrophic insert failure are presented. Tabulated and graphed data, photographs of the progression of bit wear, and selected qualitative visual and auditory observations of the bits taken throughout the experiment are found in the appendixes. The results show that bit life ranged from approximately 16,000 ft for the WC round-nose radial bit to over 125,000 ft for a PDC round-nose radial. Performance, in terms of bit life, cutting forces, wear rate, frictional sparking, machine vibration, and noise was in general best with the PDC bits, followed by the rotating WC bits, with the nonrotating WC bits (round-nose radial and locked 60° conical) being the worst. The results show variations in the included tip angles of new conical bits have an insignificant influence on bit performance when the effects are averaged over the life of the bit. In addition, new bits were generally found to entrain more primary respirable dust for a given cutting distance than worn-out bits. It is hypothesized that this is due to the difference in frictional behavior between new and worn bits. The results from these tests are being used in the Bureau's cutting system model (CSM).

Jan 1, 1988

By H. D. Bemis

This paper describing the milling practice of the American Metal Co. at its Pecos con¬centrator is one of a series on milling methods and costs being prepared by the United States Bureau of Mines. ACKNOWLEDGMENT The author acknowledges the assistance rendered by Guy Martin, metallurgist, H. E. Brown and J. H. Hastings, chemists, and Thomas J. Fahey, accountant, in gathering and pre¬paring the data presented in this paper.

Jan 1, 1932

By Ann G. Kim

The Bureau of Mines investigated factors that influence the formation of methane and other hydrocarbon gases in coal, which is an integral part of the coalification process. Coalification begins with a biogenetic stage in which plant debris decomposes and peat is formed; methane and CO2 are the predominant gases produced during this stage. During the diagenetic stage of coalification hydrogen and the hydrocarbon gases methane, ethane, ethylene, propane, propylene, butene, iso- and normal butane, and pentane are formed by dissociation of the organic material. Methane may also be produced by a secondary reaction of hydrogen with unsaturates or by the reduction of CO2. The gas contained in coalbeds is a mixture of methane, C2 through C5 alkanes, CO2, 02, N2, H2, and H2; its heating value is equivalent to that of natural gas. The gas content of coal depends on many variables, but an empirical relationship between adsorptive capacity, rank, and depth has been observed.

Jan 1, 1978

By A. G. Starliper

Laboratory studies were made to produce whiskers of tungsten over a wide range of operating temperatures. Hydrogen reduction of tungsten hexachloride in a vacuum furnace at temperatures from 2,7000 to 3,3000 C yielded a small quantity of tungsten whiskers, provided a low degree of supersaturation was maintained. Direct measurements of 3,000,000 to 4,000,000 psi were obtained for the ultimate tensile strengths of individual whiskers averaging 3 to 4 microns in diameter with average aspect ratios of 1,000. This compares with strengths of 300,000 to 400,000 psi for 13-micron-diameter commercial filaments.

Jan 1, 1968

By R. D. Leitch

"INTRODUCTION The general program of the investigation of coal mine drainage which the Bureau of Mines is making includes, among its many phases and objectives, a study of the fate of the acid, content of drainage after it enters natural streams, and the effect of seasonal variations on the degree of contamination of streams. Opportunity for studying these under comparatively normal conditions and variations can readily be found, but there is only a chance opportunity for studying than under extreme conditions. The unusual drought that prevailed during the summer of 1930, however, created a condition of low water favorable to a study of one of the extremes.This report gives the results of an investigation of Bennett Branch of Sinnemahoning Creek, Pa., made under this condition.ACKNOWLEDGMENTSThis work was conducted under the direction, and with the advice, of Dr. R. R. Sayers, chief, Health and. Safety Branch, and of W. p. Yant, supervising engineer, Pittsburgh Experiment Station.DESCRIPTION OF BENNETT BRANCHBennett Branch, as shown in Figure 1, is a tributary to Sinnemahoning Creek. Its source is in Huston Township, northwestern Clearfield. County, from which it flows in a general northeasterly direction through Elk County, thenceeasterly in Cameron County to Sinnoning Creek at Driftwood. The total length is about 37 miles. There are nine towns along the stream that have an average population of about 350. There is no industrial pollution other that from coal mines and very little. domestic, pollution."

Jul 1, 1931

The performance of two large-capacity ventilation systems was compared through tests conducted in a large dead-end heading at a pilot oil shale mine in Colorado. Sulfur hexafluoride (SF6) tracer gas was used to measure the performance of the two systems: a free-standing jet fan and a reversible fan with rigid duct. The tracer gas was used to simulate the production of mine air pollut-ants, including blasting pollutants, hot diesel emissions, free methane from surrounding strata, and methane desorbing from muck piles. The test room was 55 ft wide, 30 ft high, and 320 ft long. The performance of the two fans was similar, but the jet fan used less power. The tests showed that either system could provide effective ventilation during oil shale mining.

Jan 1, 1986