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By Zhisong Chai, Wei Xu

Q&P steels undergo continuous multiple processes, including hot rolling, intermediate heat treatment, cold rolling and continuous annealing etc. The inheritant effect of initial microstructure could affect the final microstructure and mechanical properties of Q&P steels. In this work, effects of different hot rolled microstructure/texture on the final microstructure and properties subjected to Q&P process were investigated in Fe-0.38C-1.58Mn-1.6Si system. Different initial microstructures were generated combing different TMCP and cooling strategies. The microstructure and texture of hot rolled materials were characterized in detail. The hot rolled material was subsequently processed by intermediate annealing, cold rolling and continuous annealing. The comparison reveals great effects of the initial hot rolled microstructures, i.e. inheritance effect. The faster reverse transformation would lead to more sufficient austenitization and it would greatly weaken the inheritant effect of the initial microstructure. Although the difference of final phase fraction for different initial microstructures was not significant, the inheritance effect was mainly reflected in the effect on austenite morphology. For the mechanical properties, no obvious difference in strength was shown for the samples with different initial microstructures after Q&P heat treatment, but there was fluctuation in elongation.

Oct 1, 2019

By Andrea Pezza

The paper describes the recent new installation and start-up of the second RH (Recirculation Degasser) in Rio de Janeiro plant of thyssenkrupp CSA Siderúrgica do Atlântico. The new plant is installed as part of the existing RH, the twin solution increases the overall melt shop production in the area of quality plates especially for deep drawing grades. With this new equipment, CSA is able to increase degassed grades production with a state of art asset that has the ultimate technology in operation, safety and automation. The description of the main components parts and the operational concept gives an overview of the latest experience in RH plant engineering combined with best operational practice of world class steel producer.

Oct 30, 2017

By Foluke Salgado de Assis

Natural fibers are attracting the interest of engineering sectors owing to specific advantages such as lightweight and lower cost as well as for their inherent condition of being renewable, biodegradable, recyclable and environmental correct material with respect to CO2 emission. The banana fiber is nowadays recognized by its mechanical properties. It is known that with the increase of fibers volume fraction the composite significant increases its tensile strength. This was obtained with amounts up to 30% in volume of banana fiber. However no higher volume of fibers was able to be molded in a composite plate until now. Thus the present work aims to study higher volumes of fiber in terms of the influence on the tensile strength of specimens prepared under 5 tons of pressure. The fibers were previously washed and dried in an oven at 60ºC, after that poured together with the epoxy resin and catalyst mixture in the metal molds bone-shaped, and pressured to ensure specimens quality. The tensile strength increased significantly with higher amounts of banana fiber incorporated in the epoxy matrix. This better performance can be directly related to the fracture obstacle imposed by the fibers as well as the type of cracks resulting from the fiber/matrix interaction.

Aug 16, 2017

By Marcela Gotelip Barbosa

Pellets are the main iron input to the blast furnace at ArcelorMittal Lazaro Cardenas iron and steel making facility in Mexico. Pellets are made at this facility using the concentrates generated and shipped from their captive mines viz., Las Truchas, Pena Colorada, Volcan Sonora. The concentrating plants, after grinding the ore to the liberation size, use magnetic separation and flotation to reject the silica, sulphur and phosphorous impurities. At Volcan Sonora Mines, the ore is contaminated with phosphorous minerals, and hence, after magnetic separation, the phosphate minerals are floated using anionic carboxylate collector (sodium oleate). Apart from floating the phosphate minerals, the sodium oleate also has some tendency to smear on the iron bearing mineral surfaces leaving a hydrophobic surface, which is expected to reduce the green pellet strength due to absorption of ultrafine sized air bubbles on these surfaces, and further generate higher levels of dust during the induration process. In order to alleviate this industrial problem, comparative studies were carried out on the concentrates from magnetic separation using reagents from synthetic sarcosinate and carboxylate family collectors. Results have indicated that the sarcosinate family members not only were found as replacement to carboxylate collectors, but also reduce the phosphorous content below the values achieved with oleate, thus have considerable benefits in the downstream steel making process. Based on the results, plant runs are being taken up at Volcan Sonora. In this article, the laboratory results obtained on iron grades and recoveries, and phosphorous rejection using both the reagents are presented.

Aug 1, 2018

By Beatriz Pereda, Ana Clara Fonseca da Silva, Tiago Seixas Bittencourt

Reinforcing steel bars are usually specified based on mechanical properties with flexibility in chemical composition and processing. Most developments, in these steels, are normally focused on alloy and process design to reach minimum cost and conformity to specification. Processing routes using quenching and self-tempering (QST) and accelerated cooling are the most common. Microalloying with V and Nb have been used in rebar. When acicular constituents must be avoided, a combination of Nb microalloying with judicious control of cooling is one of the preferred options. Niobium can contribute to improvement in tensile properties through austenitic grain size control during hot working, precipitation hardening due to carbonitrides or clusters, and hardenability increase. In the present work the alloy design and development processes of a Nb microalloyed steel for rebars are presented. The designed steel has fulfilled the required specification and is under regular production. Austenitic grain size refining – when comparing with the “basic composition” normally used was observed, even without any change in the thermomechanical processing cycle. There are indications that precipitation hardening may also occur. Results indicate that Nb is a good alternative as a microalloying element in rebars.

Oct 1, 2019

By Jan Lampke

Increasingly pelletizing discs are used for the recycling of dust and sludge. The applied pellet feed is highly variable, for example in terms of chemical composition, grain size distribution and raw density. These raw materials related factors lead to a destabilized pelletizing process, which initially must be homogenized through special mixtures, as well as the use of binders or additives. There are many possibilities to reach stringent restriction of material related target factors. On the one hand it is helpful to be flexible by changing the process parameters of the pelletizing disc. On the other hand, it is necessary to use a material-binder-formulation, which leads to a highly stable pelletizing process. The paper deals with an example of the use of agglomerating device, pelletizing disc, to prepare different dusts and sludges for material recycling. These dusts und sludges are mostly generated in metallurgical processes, e.g. sinterplant, blast furnace and steelworks.

Aug 16, 2017

By Martin Dirks

Nowadays the sinter cooler often becomes the bottleneck of the sinter production, with outdated equipment leading to low productivity and high operation and maintenance costs. Furthermore valuable energy is simply destroyed in the cooler, which is not compatible anymore with a cost efficient and environmentally friendly sinter production. Paul Wurth has developed and improved two types of coolers, the annular cooler and the shaft cooler which offer flexible solutions to the specific situation of each client. The classic design of the annular cooler was completely revised and is now composed of a rigid ringframe construction as opposed to the traditional design with individual sintering cars, avoiding the typical problems of centering. Additional features of the PW annular cooler are the low air leakage rate and the increased effective cooling surface due to the removal of dead areas. This leads, in addition to the lower weight, to lower operating costs and a smaller space requirement. The shaft cooler stands out with an even smaller space requirement and a lower sinter outlet temperature because of a very long residence time of the sinter inside the shaft. Its development into a pure counter flow cooler aims at maximizing its energy efficiency, as it is designed as a system with a very low demand for cooling air, high air discharge temperatures and highly reduced dust emissions. For both cooler types flexible heat recovery solutions can be offered. These solutions include the supply of hot combustion air to the ignition hood burners and the sinter strand, the production of steam for the clients steam grid or the production of electric energy.

Aug 16, 2017

By Martin Chabicovsky, Milan Hnizdil

Emulsions are frequently used for the cooling and lubrication of working rolls during the cold rolling. The fact that the lubrication and cooling are not separable makes the optimization of both functionalities difficult. The higher emulsion temperature decreases the cooling efficiency compared to cold water. Heat transfer and fluid flow laboratory (Czech Republic), CRM (Belgium), Tata steel (Netherlands) and Henkel (Germany) cooperated on the increasing of a cooling efficiency during cold rolling. Part of this research was focused on an influence of the emulsion composition on a cooling intensity. The cooling efficiency was laboratory investigated. The stainless steel sample with thermocouple was heated and then it was cooled by a nozzle. Tests were performed with various emulsions and pure water. The heat transfer coefficient was computed from measured temperatures. The cooling intensity (heat transfer coefficient) of all tested emulsions was similar but an increase of the cooling intensity was found with water. Further various emulsions concentrations were tested. Results showed decreasing cooling intensity with increasing oil concentration. Adding additives therefore is thought to cause a noticeable decrease of the cooling intensity.

Oct 1, 2019

By Richard Harvey, Robert Paul Mawer

In recent times there has been an increase in the demand from Steel plants for a technology that offers the most economical environmentally sustainable solution. In terms of blast furnace off gas cleaning this has seen a drive towards Cyclone technology replacing the older Dustcatchers. Cyclone technology can achieve dust removal efficiencies as high as 95% increasing the dust yield at the primary stage of gas cleaning. The dry dust (rich in Fe and C) can then be recycled to the Sinter Plant or Blast Furnace. Capture of dust at this stage also has the benefit that sludge generation from the secondary stage is also reduced meaning less waste to landfill and / or recovery of some of the by-products for further use. Primetals Technologies already offer a state of the art Tri-Axial Cyclone installed on many sites world-wide, however, this paper focuses on a hybrid of this technology, the DustClone. The DustClone is a low CAPEX unit that is essentially a Cyclone housed inside the Dustcatcher. This unit is aimed at operators who may be carrying out smaller scaled shutdowns / repairs that normally have a reduced CAPEX. This paper describes the technology that Primetals Technologies have developed.

Oct 1, 2019

By Horacio Destaillat

Desde hace aproximadamente 15 años se encontró por experiencia empírica que se puede “neutralizar” el efecto del plomo sobre la maleabilidad en caliente de cobre proveniente de la refinación térmica de chatarras mediante control de la composición química. Este hallazgo ha resultado de aplicación industrial. Si bien el contenido porcentual de plomo se reduce por refinación convencional y con cierta facilidad hasta 0,02 – 0,03 %, este valor es elevado [1] para laminar en caliente. Bajar el nivel de plomo hasta los valores exigibles por normas, requiere procedimientos especiales y costosos. La técnica cuyo mecanismo aquí se investiga, consiste en ajustar el contenido de plomo y estaño dentro de ciertas proporciones, ya que el balance de estos elementos, permite proceder sin problemas de fisuraciones a la colada y laminación en línea del cobre. Con el control de la composición química del sistema se logra que el plomo y el estaño se adhieran [2] sobre las partículas de eutéctico Cu-Cu2O. Esta disposición micro estructural en borde de grano explica la acción favorable del estaño en la maleabilidad. El procedimiento que aquí se describe no es aplicable a cualquier caso pues no funciona en materiales con contenido elevado de oxígeno (“Tough pitch”) ni en cobres desoxidados. Solamente lo hace en formas de baja sección que hayan sufrido enfriamiento rápido.

Aug 7, 2018

By Norbert Asamer

At various stages during the hot rolling process, the different rolled products – blooms, billets, bars, respectively sections, but also slabs or plates – need to be cut. While the cross sections of these products are being reduced during each rolling pass, the lengths are being increased accordingly. Thus, it becomes necessary to cut the products to shorter lengths suitable for the next steps of production by state-of-the-art designed dry abrasive cut-off machines.

Jul 30, 2018

By Masahiro Shimura, Yoshiki Takahama, Toshiyuki Shiraishi, Daisuke Kasai

When advanced high strength steel (AHSS) is rolled at a high reduction ratio, the forward slip ratio in cold rolling tends to be lower than that of the other softer strips such as low-carbon steels, and the work roll sometimes skids the strip. To identify why forward slip ratio of AHSS at a high reduction ratio becomes smaller than that of low-carbon steel, the relationship between the reduction ratio and forward slip ratio was investigated by a rolling experiment. For this trial, a 4Hi laboratory cold mill was used. AHSS and low-carbon steel coils were rolled by two different rolls that were set to 0.3 and 0.6 μmRa to create two types of friction conditions. Furthermore, the rolling conditions were numerically analyzed to determine the influence of friction coefficient and flow stress on the relationship between forward slip ratio and reduction ratio. The experimental investigation and numerical analysis revealed that the forward slip ratio reduced with increasing rolling reduction ratio in a low friction state; contrarily, it increased with increasing rolling reduction ratio in a high friction state. This feature was clearly visible when harder materials were rolled.

Oct 1, 2019

By Marcelo Rebellato, Beatriz Pereda, Beatriz Lopez, Pello Uranga

The classical application of Nb microalloying in the development of thermomechanical processes for flat products has been related to its suitability to enhance strain-induced precipitation and get a pancaked austenite prior to transformation. As new steel grades or new lay-outs are being developed, more complex metallurgical conditions need to be evaluated. In this context, Nb microalloying, alone or combined with other microadditions, needs to intervene in a more controlled way in additional steps of the thermomechanical process, besides its conventional strain-induced precipitation role. For example, the hardenability enhancement associated with Nb to properly achieve lower temperature transformation products, demands a proper balance of the Nb amount precipitated during rolling and the one remaining in solid solution. Similar effects are also sought when the final available Nb is used to increase strength through precipitation hardening. This manuscript evaluates how changes in the rolling strategies affect the interaction between Nb(C,N) precipitation and austenite recrystallization at different steps of the rolling process. As the possible interactions between parameters intervening simultaneously are quite complex, the application of microstructural models helps to properly define the best austenite conditioning combined with the convenient amount of Nb in solution, as a function of the final property requirements. Along the manuscript, several strategies will be discussed for the case of hot rolling of flat products comparing both normal and coarse initial austenite grain sizes.

Oct 1, 2019

By Daniel Antonio Kapper Fabricio

A avaliação das propriedades de mecânica da fratura dos materiais é uma necessidade crescente, sobretudo no setor de óleo e gás. Esse cenário exige a garantia da qualidade na execução de ensaios de tenacidade à fratura. Esse trabalho tem como objetivo realizar uma comparação intralaboratorial para o ensaio de tenacidade à fratura KIC variando o executante do ensaio, visando atender ao requisito de garantia da qualidade da norma NBR ISO/IEC 17025. Os resultados foram comparados através de análise de variância. As diferenças entre os operadores não foram significativas frente ao erro residual a um nível de confiança de 95%, sendo tal resultado considerado satisfatório.

Aug 16, 2017

By Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Augusto Lachini Pereira, Antônio Cezar Faria Vilela

A minor change in the chemical composition and temperature affects the slag viscosity, which has a great extent of the physical properties in regarding refining slags. Optimizing those parameters may affect the steel cleanliness. The viscosity measurement process is considered expensive, so the cost-effectiveness does not favor the measures at high-temperatures. Alternatively, it is possible to apply mathematical models or thermodynamic softwares to obtain viscosities for a given range of chemical composition and temperature of slags. The present work contemplates a validation of the experimental data, collected in the literature, with a calculated data and proposes an accurate representation of iso-viscosity curves applied for secondary steelmaking slags, covering the composition ranges: 0–100 wt.% CaO, 0–80 wt.% SiO2, 0–77 wt.% Al2O3 and 0–15 wt.% MgO (CSAM) system at 1500ºC. The viscosity representation fields include fully liquid and a partially liquid slags in the CSAM system and the viscosities were calculated using the FactSage 7.2 (for Liquid Phase) and the Roscoe-Einstein equation (for Phase mixture) for a total of 5976 slags. The preliminary results indicated that there is a great convergence between the calculated and experimental viscosities data, promoting an efficient approximation of the iso-viscosity curves for the CSAM slag system in the high-temperatures.

Nov 1, 2019

By Gabriel Oliveira Glória

Due to growing concern about the ambient impacts, lignocellulosic fibers are been investigated to replace the synthetic ones in polymer composites The giant bamboo fiber, a relatively unknown lignocellulosic fiber with potential for composite reinforcement, still needs to characterize for possible engineer applications. However the giant bamboo fiber has low adhesion with the polymeric matrix. In order to understand the interaction that occurs between the bamboo fiber and the polymer matrix is necessary to evaluate its physical and chemical characteristics. Therefore, the present work analyzed the giant bamboo fiber by means of Fourier Transform Infrared (FTIR) spectroscopy. The spectrum revealed main absorption bands typical of giant bamboo fiber specific molecular interactions.

Aug 16, 2017

By Gabriel Oliveira Glória

In the context of changing culture, the society is increasingly looking for environmentally friendly materials, the natural fibers appear as an option to substitute the synthetic. Among these natural fibers, the PALF fiber may be considered an option, but there is limited information about the flexural strength of epoxy composites incorporated with PALF fibers. Therefore, the objective of this work was to investigate the mechanical properties in bending tests of epoxy composites incorporated with up to 30% in volume of PALF fibers. The results showed that the PALF fiber increase the flexural strength of polymer composites.

Aug 16, 2017

By Sander Mul, Michael Brandner, Armin Paar

Graphitic HSS roll grades such as ESW’s brand VANIMO can be considered as the latest developments for the last finishing stands in hot strip mills. These roll grades are developed on the basis of the alloying concept of (Carbide Enhanced) Indefinite Chill work roll materials. During the development of VANIMO, the amounts and types of carbide forming elements were increased and adjusted into the direction of cast HSS roll grades. The microstructure of graphitic HSS roll grades therefore consists of tempered martensite, cementite and several different carbide types as well as a well-defined amount of free graphite. The main purpose of graphitic HSS roll grades is to combine the high surface quality of Indefinite Chill alloys as well as the high wear resistance of HSS roll grades. Several systematic steps were taken to increase the wear performance from Carbide-Enhanced Indefinite Chill grades to the more advanced VANIC grade and further on to the highest alloyed roll grade VANIMO. In every development step, the surface quality of the roll grades was carefully monitored. The decision to invest in new testing equipment at ESW’s plant was driven by the wish to see microstructural effects of different alloys in a macroscopic dimension. Usually samples are taken from cast rolls and investigation is done in comparably small areas compared to the total surface of a roll. Rolling of strip is done with the entire barrel, so effects of alloy and microstructure can appear anywhere on the barrel surface. To ensure better understanding and deeper knowledge about influences of alloying trials we decided to install the last version of LRI (Lismar Roll Inspection). LRI includes the latest technology of Eddy Current with an enormous resolution. Depending on the formation of carbide precipitations, carbide network as well as matrix and free graphite, the EC test can detect smallest differences. The possibility to analyze the different results of EC and UT surface wave inspection will be discussed. A few examples of surface effects in the mill application will be discussed and improvement strategies explained.

Oct 1, 2019

By Juliano Braz Possatti, Arnaldo Carneiro Salles, Cleudson dos Santos Rego, Leandro de Lucas Mendes

The increase in customer demand for steels with higher surface requirements, associated with the need to increase ArcelorMittal Tubarão's HSM productivity, it was necessary the development of controls and actions to reduce scale losses within the scenario of high productivity. This article describes the path followed by the hot strip mill team in order to reduce the occurrence and severity of scales.

Oct 10, 2019

By Daniela Mota Paschoal Veloso da Silva, Gabriel Filinkoski, Suelen Silva Rocha, Jorge Luiz Valença Mariz

A previsão da fragmentação da rocha é essencial para otimizar a operação de desmonte de rochas. A fragmentação depende de muitos parâmetros, como propriedades estruturais e geomecânicas do maciço rochoso, geometria do plano de fogo das detonações e propriedades dos explosivos. Neste contexto, este trabalho objetivou realizar a previsão da fragmentação por simulação do desmonte de rochas da Mineração Megaípe considerando as características estruturais e geomecânicas inerentes à formação do maciço rochoso através da metodologia de Kuz-Ram. A metodologia consistiu no levantamento das propriedades geométricas das descontinuidades visíveis na face da bancada existente, realização da classificação geomecânica através dos sistemas Rock Mass Rating (RMR) e Q e aplicação dos resultados para predição da distribuição granulométrica da fragmentação. Obteve-se como resultado da simulação que cerca de 90% do material fragmentado deve passar na abertura do britador primário disponível na pedreira, além de resultados favoráveis quanto às análises de condições de estabilidade do talude operacional.

Oct 3, 2019