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By Francisco Belmino Romero, Walney Silva Araújo, Vitória Lima de Souza, Edilberto Rocha Silveira, Adriana de Oliveira Sousa Leite

O uso de inibidores verdes na corrosão do aço carbono SAE J403 1020 configura-se como uma alternativa econômica e ambientalmente acessível, pois, em relação aos inibidores comerciais geralmente utilizados, são de fácil obtenção, já que são adquiridos a partir de vegetais, portanto, não oferecem risco ao meio ambiente. Assim, o presente trabalho tem como objetivo avaliar o uso das folhas de aroeira como inibidor de corrosão para o aço carbono SAE J403 1020, o qual é bastante utilizado na indústria e possui baixa resistência à corrosão. A escolha da aroeira se deu devido ao fato de a planta ter origem no Brasil e abundância no Nordeste do País, principalmente no Ceará. Para análise, foram utilizados como meio corrosivo: H2SO4 0,1 M, NaCl 3,5% e NaCl (ph = 4,0); as concentrações do inibidor foram: 50, 200, 500 e 1000 ppm. Em relação aos ensaios eletroquímicos, utilizou-se: Potencial de Circuito Aberto (OCP), Espectroscopia de Impedância Eletroquímica (EIE) e Curvas de Polarização Linear (CP). Dessa forma, por meio da análise das técnicas mencionadas, conseguiu-se obter o comportamento do inibidor em relação ao material e ao meio, bem como avaliar qual o melhor meio para a utilização da aroeira como inibidor verde de corrosão.

Mar 1, 2019

By Maciej Korecki

Pyrowear®Alloy 53 steel is an excellent material for the construction of drive transmission components (gears, shafts, etc.) which have to operate in difficult conditions primarily in the aviation industry (Fig. 1.). Among the properties of such items is a high case hardness and abrasion-resistance, while the core remains flexible and is capable of carrying large impact loads. They can work at elevated temperatures with limited lubrication. The thermal treatment of such materials is based on case hardening by means of carburizing. This paper presents the technology of vacuum carburizing of Pyrowear® Alloy 53 steel. It discusses the methods of establishing different profiles of carbon concentration in a layer and their influence on the hardness profile. The effects of sub-zero treatment and tempering on the properties of the hardened case are also considered. It also presents a SimVaC® simulator of vacuum carburizing, designed especially for Pyrowear® Alloy 53 steel, which provides highly accurate predictions of the outcome of the process as the profile of carbon concentration in the layer, or vice versa: establishes the process parameters which will guarantee the required profile.

Aug 16, 2017

By Rodrigo Abreu, Nilson Luiz Biccas, André Luiz Bonelar dos Santos, Odilon José da Silva

A Coqueria no contexto siderúrgico é a área responsável pela produção de coque metalúrgico para os Altos-Fornos. O coque geralmente é obtido em fornos verticais, que tem a finalidade de aquecer a mistura dos carvões minerais até a temperatura de pirolise, através da queima controlada de um combustível. O objetivo deste trabalho é apresentar as alterações realizadas no Controle de Combustão das Baterias de Coque da ArcelorMittal Tubarão para garantir a estabilidade operacional e o maior controle do tempo líquido de coqueificação. O aprimoramento do modelo matemático ajustado as condições atuais do processo, trouxe benefícios tais como a obtenção de uma melhor distribuição de calor ao longo das paredes de aquecimento e consequentemente a redução das resistências aos desenfornamentos, consumo de calor e emissões de poluentes, preservando a estabilidade operacional das baterias de coque e contribuindo para o prolongamento da vida útil.

Oct 1, 2019

By Verônica Scarpini Candido

Este estudo tem por objetivo caracterizar o pó de balão proveniente de uma siderúrgica do estado do Pará visando a sua incorporação em argilas para produção de blocos. O resíduo passou pela etapa de beneficiamento e, depois, foi realizada a difração de raios-X (DRX) e fluorescência de raios-X (FRX). Além disso, realizou-se também a análise morfológica por microscopia eletrônica de varredura (MEV). Os resultados mostraram que hematita, magnetita, goethita são as fases predominantes. A análise química por FRX mostrou que o resíduo apresenta baixos teores de sílica (SiO2) e alumina (Al2O3) associados a elevados teores de óxido de ferro III (Fe2O3). Dessa forma, a caracterização do pó de balão mostrou que esse resíduo apresenta-se como um potencial constituinte mássico cerâmico e que os elevados teores de óxido ferro podem contribuir para melhorar a cor dos produtos finais.

Oct 30, 2017

By Adriana Amaro Diacenco

O presente trabalho propõe-se a analisar a influência do amortecimento estrutural inerente de tais materiais submetidos a perturbações estáticas e dinâmicas as quais afetam as características de resposta. A importância deste trabalho insere-se no contexto do controle de vibrações de sistemas de engenharia. Para tanto, é empregada uma técnica de modelagem baseada em elementos finitos. A análise numérica é desenvolvida utilizando a Teoria da Deformação Cisalhante, a qual é implementada em um elemento Serendipity retangular contendo oito nós. O amortecimento é incluído empregando o modelo histerético. As respostas dinâmicas são representadas por funções de resposta em freqüência e autovalores complexos. Simulações numéricas são realizadas visando quantificar os níveis de amortecimento obtidos no tocante às vibrações transversais de placas retangulares e verificar a possibilidade de se aumentar tal amortecimento.

Aug 7, 2018

By Armando Vazquez

This paper will provide an overall technology update on Tenova’s modular i BOF® technology package for improved endpoint detection (Carbon and Temperature), slop detection and auto-tapping control, with a primary focus will be on Tenova's Slop Detection System (SDS). Accurate Slopping prediction is a critical tool in the operation of a BOF. It provides the steelmaker with an additional protective system to increase yield & productivity while reducing operating costs. Tenova Goodfellow's i BOF® slop-detection technology uses lance vibration analysis with real-time alerts to give steel makers advance warning of the onset of a slop and a measurement of the slop severity. The system is designed to provide direct feedback control of lance position and oxygen flow rate, for rapid mitigation of potential slopping events. This paper will provide a summary on how the i BOF® technology package has been implemented, including trials and general results.

Jul 30, 2018

By Charles de Abreu Martins

An experimental investigation was conducted using laboratory-processed, 0.12C–1.70Mn–0.2V steels with different Cr or Mo additions aiming to evaluate this influence on the microstructure and mechanical properties hot rolled steels. Steels were processed in a pilot rolling equipment, simulating a typical thermomechanical processing, with finishing rolling steps above Ar3, followed by accelerated cooling and 723 K (450 Celsius) coiling temperature. Microstructures and precipitates were analyzed using OM, SEM and TEM, while mechanical properties were evaluated by tensile and hole expansion tests. Since Cr and Mo increase hardenability of austenite, and as a consequence, the volume fraction of the acicular constituents increases with gradual additions of Cr or Mo. Moreover, Cr or Mo impacted V precipitation process, reducing average size of particles. At 0.50%Mo, V precipitation was inhibited. Effects of this microstructure evolution on the final mechanical properties were also analyzed, as well as a comparison between Cr and Mo effects, with Mo presenting more effective influence.

Jul 30, 2018

By Rodrigo Ribeiro de Andrade, Túlio César Nogueira, Ed Juarez Mendes Taiss, Nilton José Lucinda de Oliveira

The objective of this study was to determine the effects of an eventual slab central macro-segregation in microalloyed steels with low Mn content (0.80%) and high Nb content (0.08 to 0.10%) on the kinetics of recrystallization of austenite during its rolling, on its critical temperatures, that is, of non-recrystallization (Tnr), start Ar3 and finish Ar1 of ferrite transformation and its response to a simulated industrial thermomechanical processing. The determination of the austenite recrystallization kinetics was made through isothermal double compression tests using a dilatometer, while the critical temperatures were determined through hot torsion tests in a Gleeble® 3800. It was found that austenite recrystallization kinetics, Ar3 and Ar1 temperatures did not present significant changes for the samples extracted both at ¼ of the thickness and at the core of the plate, indicating that, as expected, the central segregation in this type of steel was not intense to the point of affecting this phenomenon. The Tnr values determined for the samples extracted in the core of the plate were, on average, 30°C lower than those obtained from specimens extracted at ¼ thickness, which suggests that a significant portion of the carbonitrides present in the core of the slab are eutectic and coarse, not having completely dissolved during the reheating of the specimens. This occurred despite the fact that the austenitization temperature adopted in this treatment theoretically leads to the total dissolution of Nb, as seems to have occurred in the case of specimens extracted at ¼ of thickness, where carbonitrides have a finer size.

Oct 1, 2019

By Jorge Madias

O trabalho está centrado na análise comparativa de normas de vinte paises/regiões sobre vergalhão, escolhidos levando em conta os principais paises productores, exportadores, e consumidores deste produto para a construção civil. São comparadas as propriedades mecânicas: limite de escoamento, resistência à tração, elongamento à rotura, elongamento uniforme, relação escoamento/tração), a análise química, testes especiais como fadiga e adherência e outros ítens. Tambén é tida em conta a evolução dos quesitos das normas ao longo do tempo. O foco é o comportamento anti seismo do vergalhão.

Oct 30, 2017

By Mário César Mantovani

The steel for gas turbine compressor discs (26NiCrMoV14.5) requires some mechanical properties like strength, impact, toughness, fatigue, and creep resistance in order to be used in such application. To achieve the properties required for the gas turbine compressor discs, the material should have very low contents of sulfur, phosphorus, antimony, tin and arsenic. The level of cleanliness should also be very high and this is possible by achieving low oxygen content keeping the deoxidation elements like silicon, manganese and even the aluminum in very low percentages. The main problem in refining such steel is to adjust a sufficiently low oxygen content to have a good desulfurization and at same time a good cleanliness without using silicon, manganese or aluminum as deoxidizers. Combination of initial selection material, steelmaking process control, forging sequence and heat treatment cycles can provide uniform mechanical properties throughout the gas turbine compressor discs. Villares Metals SA as a big player on special steels with complex process has been developing this kind of material for several years. The objective of this work is to show the process technology evolution involved in the production of this kind of steel under the discussed preconditions.

Aug 17, 2017

By Felipe Fardin Grillo

The aim of this work was to study the use of slags to desulfurization of cast iron. It was proposed to use alumina instead fluorspar. In addition, marble waste was used instead lime. Simulations applying Thermo-Calc software were performed in order to obtain the theoretical phases thermodynamic data. Then, a comparison between theoretical data and experimental tests were performed. The cast iron was melting in induction furnace at 1550°C. Slags composed mainly for CaO and Al2O3 were used to cast iron desulphurization. It was observed that increasing liquid phase, the desulphurization reaction was favored. Besides, it was found that cast iron desulfurization occurs by top slag mechanism.

Aug 17, 2017

By Carlos Gonzalez-Rivera

An alternative cooling curve analysis method focused on the experimental determination of the latent heat of phase changes and phase transformation kinetics is proposed in this work. The method analyses the cooling process of a metallic sample, initially liquid that is contained into a cylindrical metallic mold, both of known weight, thermally isolated at its top and bottom. The method is based on an energy balance associated with the experimental measurement of the temperature change of the sample and the mold during their cooling process. From the numerical processing of the cooling curves, are obtained approximate values of the acting global heat transfer coefficient as a function of temperature in order to describe quantitatively the energy exchange of the metal/mold system with its surroundings. These relationships and other experimental data are used to process the cooling curve of the sample and the mold during solidification, in order to obtain the latent heat of solidification.The method was applied experimentally to zinc and tin of commercial purity, initially liquids and contained into stainless steel molds in order to determine its ability to measure the latent heat of solidification. The obtained results suggests that this method shows a good potential to characterize the solidification of metals.

Oct 30, 2017

By Rudolf Hubmer

In October 2013 JSW Steel decided to place an order to Primetals Technologies Austria (former Siemens VAI Metals Technologies) for the installation of a comprehensive Level 2 process optimization system for more than 20 existing production facilities of various suppliers. For SMS-I new L2 systems are provided for two hot metal pretreatment stations, three hot metal desulphurization stations, three ladle furnaces, two 1-strand slab casters, a ladle tracking system as well as a shop supervisory system. Additionally the existing L2 system for one 1-strand slab caster is being upgraded in the course of the project. In SMS-II new L2 systems for the 7 hot metal desulphurization stations, 4 ladle furnaces, 1 new RH vacuum degasser, ladle tracking system and a shop supervisory system are supplied. Despite of the challenging time schedule the commissioning of the single facilities started within less than 12 month after contract effectiveness. The installed Level 2 process optimization systems together with the achieved results are described in this paper.

Aug 16, 2017

By Mühlböck Marlene

Increasingly stringent global environmental regulations are forcing steel producers to continually improve the efficiency of sinter waste gas treatment. With the Selective Waste Gas Recirculation (SWGR) system from Primetals Technologies, lower production costs can be achieved and the size of downstream waste gas cleaning units can be reduced for investment savings. SWGR features the extraction and reuse of hot sinter off gas from selected wind boxes along the sinter strand, which contributes to improved energy efficiency and off gas treatment in the sintering process. With the next generation of SWGR, Primetals Technologies can provide an energy optimized, emission optimized and environmentally friendly solution that meet customer requirements and country specific regulations. This paper demonstrates the latest developments in selective waste gas recirculation, especially results from pot grate tests and comparison from lab to real plant data. Furthermore theoretical finding and mathematical modelling is presented.

Aug 16, 2017

By JOSÉ RONALDO SILVEIRA JÚNIOR

O objetivo deste trabalho é de identificar estratégias para avaliação da conta de energia de unidades industriais, que sirvam de subsídio para o processo de tomadas de decisão e que eventualmente forneçam benefícios econômicos imediatos, sem investimento. Para esse fim, aplica-se uma metodologia simples que consiste em três aspectos: avaliação da demanda contratada, análise de modicidade tarifária e averiguação de excesso de consumo de energia reativa. Apresenta-se um estudo de caso da aplicação dessa metodologia em uma unidade produtiva de distribuição de aço. Nesse estudo, observa-se redução de custos por se evitar penalidades tanto de ultrapassagem de demanda quanto de excesso de energia reativa, representando uma economia de aproximadamente 15% do valor total da conta de energia elétrica da unidade.

Oct 30, 2017

By Christoph Aichinger

The optimization and improvement of a modern integral iron and steel works gets more and more difficult as each individual plant is already operated at its best efficiency and at the lowest operational expenditures. However very often the individual plants are considered as stand-alone units and there are losses and inconsistencies on interfaces and take over points, which could be avoided and by that improving the overall performance of the iron and steel works as a holistic unit. Primetals Technologies looked into this subject extensively in the recent years and is now ready to offer new tools and services in order to assist operators to find further potential for improvement in processes, which seem to be fully developed at first sight.

Aug 17, 2017

By Patrick Tassot

Increased worldwide highly competition in steel market imposes innovative measure for the steelmaker targeting cost reduction and climate-friendly steelmaking process in order to have the ability to withstand the pressure of the market. At the same time the demand for high purity and highest quality steels continues to grow from year to year, especially in the sector automotive in transportation of oil and gas, in the construction Industry and in the manufacture of heavy plate. As they allow producers to be up to the requirements while allowing expanding their product mix, new secondary metallurgical treatments have become a must additionally to standard equipment elements of steel plants modern. Most of these treatments occurs in the steel ladle increasing the pressure to ensure a reliable and as possible neutral reactor. Intelligent solutions for refractory lining ladles should integrate better adaptation to the operational process parameters and the high reliability/availability at the best cost/performance. This challenge has conducted Refratechnik to develop new concepts to overcome the frontier between shaped and unshaped materials and that’s what will be covered in this paper.

Aug 17, 2017

By Ismar Antônio Sardinha

Usually outer straight steel tubes are used to blow supersonic oxygen into LD converters (BOF) to make liquid steel, although conical tubes are used too. Inner tube for oxygen blow and intermediary tube for water IN and water OUT are normally straight steel tubes. Present paper shows the influence of outer tube shape and metal used to in lance cooling and, consequently, a skull retention on lance surface. There are two parameters more important related to lance cooling: velocity of water out and the total lance cooling by addition of thermal conductivity of outer tube metal to it. For this comparison outer tubes are made of carbon steel or copper, and can be straight or conical. As related to velocity of water OUT, outer straight tubes have bigger efficiency than conical tubes. As related to total lance cooling, outer tube metal made of copper has much bigger efficiency than steel because of its thermal conductivity 7 to 12 times more depending on work temperature. The lance cooling has much bigger efficiency for the patented SKULLS3® technology with no skulls on the lance and no skulls into the mouth of LD converters (BOF).

Aug 17, 2017

By Günther Staudinger

Danieli Linz Technology has been honored at 4.1.2013 with the first contract for the exchange of a 350 t BOF converter for ArcelorMittal Poland Dabrowa Gornicza on a turnkey basis. This paper describes the new design features of this converter based on the development of a new Danieli converter suspension system. The issue was to install a new converter (incl. trunnion ring, suspension system and bearings) with maximum volume but keeping most of the existing equipment unchanged. So, the big tilting drives on both sides had to be reused and the existing foundation, pedestals as well as the bearing distance had to be maintained. Further on the welded coreequipment (vessel shell, trunnion ring, pedestals, slag shields, etc.) was manufactured in-house within the pressure vessel division of Danieli Thailand. Due to the huge dimensions of these parts the delivery had to take place in parts which had to be welded together on site under full production conditions of the steel plant. But also the erection had to be applied under this condition. Additionally the main support bearings, parts of the screening (doghouse) as well as an upgrade of the existing relining machine had to be delivered.

Jul 29, 2018

By Rodrigo Fina Ferreira, Jacek Kolacz, Luciana Gois, Neymayer Pereira Lima

The recent developments on the sensor detectors together with the higher capacity of the machines, due the high-speed computing recent advances, have made possible extending the application in the mining industry. The use of x-ray fluorescence, x-ray transmission and radiometric sensor based sorting can selectively remove gangue minerals in different size fractions for different minerals. This paper summarizes the potential application of SBS for an iron ore in three size fractions aiming to increase the %Fe after the removal of particles with main gangue minerals associated. Pilot plant tests were carried out with samples of iron ore in different size fractions and different content of hematite and gangues. The use of x-ray transmission sensor showed the possibility to increase the %Fe from about 63% to above 68% for particles below 80mm and 45mm, after the removal of low density particles. The presence of fines on the feed affected the performance of the SBS X-rays transmission machine, especially for the fine fraction feed. The mineralogical determination, carried out to know the association between hematite and gangue minerals, and the density of the particles on the feed, can be used to preview the quality of products of the x-transmission sorting process.

Oct 3, 2019