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By M. G. Mena, M. S. Mena-Junio

Silver (Ag) filler is the most attractive choice among all the conductive fillers of die attach materials for the attachment of silicon devices because of its balanced properties and relatively low cost. However, a major problem of silver is that it electrochemically migrates in the presence of moisture and applied bias. In microelectronic devices, silver migration can occur between adjacent conductors/electrodes, which leads to the formation of dendrites and eventually results in short-circuit failure. In order to assess the reliability of these conductive fillers, an investigation for two types of Agfilled die attach materials was done using the water drop test at room temperature and using a 1000 hour temperature-humidity-bias (THB) test under 85 ºC and 85% RH conditions. Four different bias/voltages and six different electrode distance spacing were used. Both dendrite and cloud/lace-like growths were observed as a result of the electrochemical migration of silver, Water drop test results revealed that increasing the applied bias/voltage and decreasing electrode spacing causes migration to occur faster, thus resulting into shorter time to fail (TTF). It was also observed that the growth rate of the dendrites from the cathode increased linearly as the dendrite approached the anode, probably due to a combination of increased ion availability and electric field. A minimum applied bias of 3 volts was required for migration to occur in Epoxy A as compared to 2 volts for Epoxy C. The higher migration voltage requirement for Epoxy A was attributed to the higher volume resistivity of the said epoxy. In addition to the minimum voltage requirement, it was observed that a minimum electric field of about 1 volt/mm is required for migration to occur. The 1000 hour THB testing did not result into any failures. It is surmised that the presence of condensed moisture is another requirement for migration. Such condition is not present during the THB testing.

Jan 1, 2012

By M. G. Manzone

Approximately two-thirds of the annual 210,000 tons at copper refined by AMAX Inc. at the United States Metals Refining Company in Carteret, New Jersey, comes from a wide variety of copper scrap ranging from low-grade smelter scrap to wirebar-grade material. The equipment and methods used to effect such large-scale metal recycling in an urban area and the measures taken to collect and recover metal values from smelter and refinery byproducts while protecting the environment from pollution are described and discussed.

Jan 1, 1977

By M. Tiedtke, T. Crary, P. MacPhail, M. Ounpuu

"The SGS carbon-in-pulp (CIP) / carbon-in-leach (CIL) model was used to evaluate and optimize the carbon circuit at Alamos Gold’s Young-Davidson Mine. Plants samples (pulp and carbon) were tested in a series of small scale batch experiments to determine rates of gold leaching and adsorption on carbon from a combined flotation concentrate/tailing product. The testwork data, along with existing plant data were then used to model the performance of the existing CIL plant and optimize the circuit to improve performance and overall recovery. The primary purpose of the modelling exercise was to determine the most cost effective way to lower solution losses at the plant. The modelling was also used to learn how the various parameters in the CIL circuit affect solution losses and the gold inventory tied up on the carbon. This resulted in recommendations for minor changes in the CIL flowsheet, which were successfully implemented in the plant. The approach, results and plant changes are presented.INTRODUCTION This paper presents the details from testwork conducted on samples from Alamos Gold’s Young- Davidson gold mine which is located near the town of Matachewan, approximately 60 km west of Kirkland Lake in Northern Ontario, within the southwestern part of the Abitibi Greenstone Belt. The objective of the test program (completed by SGS Canada in 2013) was to investigate and model the combined flotation concentrate / tailing carbon-in-leach (CIL) circuit and suggest ways to improve gold recovery. The metallurgical test program included mineralogy, rheology, and carbon modelling testwork. Plant information was provided during the test program and used in the optimization process. Upon completion of the testwork, plant changes were recommended and implemented at site (October 2014). Plant results from 2014 to 2017 confirmed the modelling results."

Jan 1, 2018

By J. E. Hawley

This paper constitutes a report from the Committee on Geological Research to the Geology Division of the Institute. Two years have elapsed since a formal report was made containing several resolutions aimed at assisting geological research, a review of research equipment available, a summary of research projects suggested for consideration, and a list of research then in progress (see July, 1947, Bulletin, pp. 351-370). At this time we may note what action has been taken on the various resotions and suggestions of the Committee, indicate the more important accomplishments of independent investigators, and present a summary of the rather imposing volume and variety of research currently being carried on throughout the country. I.-Committee Resolutions and Suggestions 1.-A National Advisory Committee on Research in the Geological Sciences The original resolution adopted on the setting up of this Committee was approved with despatch by Council and was forwarded to the Minister of Mines and Resources. Due to a reorganization in the Department and possibly other reasons, no action on this important matter has yet been taken, but we are assured that some time this year such a Committee will be established by the Department of Mines and Resources. Unquestionably, it will give a fresh impetus to research in the geological sciences. When the noteworthy progress made by the research committees on Geophysics and on Soil and Snow Mechanics, established by the National Research Council, is considered, it is indeed regrettable that the Department of Mines and Resources has not acted more decisively in this matter.

Jan 1, 1949

By J H. Dressel, J. E. Williams

This paper presents a brief review of what coal gasification is, procedures that are available today and processes that may be available in the future. Examples are given as to how the process might be used in power plant applications, the effect on pollution level and power costs, and some thoughts on the added burden that might be placed on mining and coal preparation.

Jan 1, 1973

By Roger Lacroix

L?arrivée de nouvelles technologies sur le marché des foreuses portables combinée au besoin des mines à mieux consommer l?énergie électrique ont permis d?identifier le potentiel de deux nouveaux type de foreuses présentement utilisées en Afrique du Sud, à savoir les foreuses électriques et les foreuses hydrauliques actionnées à l?eau. Grâce à la collaboration de mines Niobec et Géant Dormant de Cambior Inc., ainsi que d?Hydro-Québec, le potentiel réel d?économie énergétique des foreuses portables hydrauliques et électriques par rapport aux foreuses conventionnelles à air comprimé a été évalué pour des roches dures et moles. Ainsi, cet article a pour objectif d faire ressortir ces potentiels d?économie énergétiques. En outre, les résultats pour une mine mécanisée et une autre mine de type filonien, dans lesquelles on retrouve des conditions de terrain différentes, seront présentés. Les résultats montrent un potentiel d?économie énergétique d?environ 70% pour la foreuse électrique et d?environ 50% pour la foreuse actionnée à l?eau. Ces résultats montrent qu?il est possible d?obtenir une meilleure efficacité énergétique par mètre foré. Ainsi, il apparaît maintenant intéressant de poursuivre les travaux de développement des deux technologies pour les applications de forage vertical et de tensionnement des boulons, et de viser à accroitre le taux de pénétration de la foreuse électrique pour le rendre équivalent à celui de la foreuse à air comprimé.

May 1, 2007

By L. E. Djingheuzian

Introduction For many years the immense deposits of bituminous sands of northern Alberta have been attracting the attention of our governments, engineers and .scientists ( 6). Undoubtedly these bituminous sands represent one of the greatest potential resources of liquid fuels in the world. However, their commercial development has been retarded by the complexities of the technological problem and by the economic factors involved in the processing of the sands. The technological problem has been attacked from several angles ( 2, 3, 1, 11), and cold water separation of bitumen is one of them. To the ore dressing engineer, the cold water process is of utmost importance since, by the use of standard ore dressing machinery, it accomplishes most efficiently and economically the separation of bitumen from bituminous sands. The significance of using ore dressing equipment was especially enhanced by the fact that the scientific principles which underlie the design of standard machines were demonstrated in the cold water separation process with an extraordinary clarity. This greatly facilitated the analysing of limitations and advantages of different machines during-the pilot plant investigations and helped to complete the investigations practically in the allotted time.

Jan 1, 1952

By T. J. Fee

Introduction The International Nickel Company have been pioneers in mine rescue work in Ontario. Following the fire in the Hollinger mine in the spring of 1928, the Company purchased ten self-contained oxygen breathing outfits, ten all-service gas masks, an oxygen high-pressure pump, life line, inhalator, ten cap-lamps with batteries, and a complete stock of spare and accessory parts. An instructor from the U.S. Bureau of Mines, Pittsburgh, came to the Creighton mine for one week and trained twenty men in the use and limitations of all equipment. Monthly training courses were commenced in the fall, and have continued to the present time. Of the original twenty men trained, ten are still on the Creighton mine rescue teams. In the meantime, and as an aftermath of the Hollinger fire, the Work-men's Compensation Board of Ontario and the Ontario Department of Mines established a central mine rescue station at Timmins. This was completed in the spring of 1930. It was then decided, in view of the great expansion in mine development in the Sudbury district, to build and equip a similar station to serve all the mines there, namely, Creighton, Frood, Garson, Falconbridge, Sudbury Basin, and Errington. An extensive survey was made and a central location selected opposite the Frood mine. The International Nickel Company donated a site, and the station was completed in the fall of 1930. The station is a two-storey brick building, 27 ft. by 47 ft., with a large garage adjoining it. The ground floor is used for equipment and for training the crews. On the second floor are living quarters for the superintendent and his family. The garage houses a closed truck, in which all necessary equipment can be taken to any desired point for training purposes or for actual mine rescue work, if and when necessary. The garage is also used as a gas room, where the men are trained in an irrespirable atmosphere. A gas-tight observation window between it and the training room enables the superintendent to see and direct the men undergoing training, weight exercisers and other devices being used.

Jan 1, 1935

By Mark W. Masson, David B. Stevenson, David W. Broughton, Douglas R. Cruji, Steven E. Parry

"Abstract-The Amalgamated Kirkland gold deposit is located at Kirkland Lake, Ontario, within the Archean Abitibi Greenstone belt of the Canadian Shield. It lies on a fault or "break", termed the Cyprus Break, which is a splay off a regional structure termed the Cyprus-Battle Mountain Break. The Cyprus Break merges with the Cyprus - Battle Mountain Break above the -250 m level, as it was not encountered in shallow drilling or surface exploration. These structures lie 1.5 km south of the 727 000 kg (23 million ounce) Kirkland Lake Main Break and 0.5 km north of the 872 000 kg (30 million ounce) Larder Lake Break.The deposit is hosted by alkalic Timiskaming Group volcanic and sedimentary rocks which are overthrust by older Larder Lake Group tholeiitic and komatiitic flows along the Larder Lake Break. Timiskaming syenitic intrusives, similar to the host rocks for the Kirkland Lake Main Break gold deposit, intrude both suites.The Amalgamated Kirkland deposit consists of lode-style gold mineralization which is mainly hosted by altered and pyritized Timiskaming trachytic volcanics which wedge out or thin at depth, between two sedimentary units. The intersection of the Cyprus - Battle Mountain and Cyprus Breaks, in conjunction with the westward plunge of the volcanic wedge, appears to control the westerly plunge of the Amalgamated Kirkland deposit at approximately 50º.Mineralization is characterized by blue-gray brecciated and "wormy" quartz-ankerite veins which contain up to 10% fine-grained pyrite and, in decreasing order of abundance, minor galena, chalcopyrite, sphalerite, molybdenite and visible gold. The sulfides and gold commonly occur along fractures and wallrock inclusions within the veins. Native gold occurs as fine pinpoints distributed in 1-mm to 5-mm size clusters of up to ten or more grains.The auriferous veins occur within a quartz-ankerite-sericite-pyrite alteration assemblage which is enveloped by a broader zone of ankerite-sericite±hematite±quartz-pyrite alteration up to 60 m wide. This latter assemblage overprints the regional greenschist-facies chlorite-calcite assemblage.The Amalgamated Kirkland property has had a long history of exploration activity beginning with the first discovery of mineralization in 1911 on the Hunton Shaft claim located in the northeast corner of the property. Since that time various prospecting, mapping, trenching, geophysical surveys and diamond drilling programs have concentrated on either carbonate zones along the Larder Lake Break or quartz veins along the northern side of the property in association with complex trachyte flows and syenite dikes.Battle Mountain Canada Inc. located the Cyprus - Battle Mountain Break through a prospecting, trenching and geophysical program in 1989. Drilling by Battle Mountain and Cyprus Canada under the surface showing, coupled with several revisions to the structural interpretation of the Cyprus - Battle Mountain and Cyprus Breaks, resulted in delineation of the Amalgamated Kirkland deposit. Location of an auriferous structure through basic surface exploration within 1 km of a world-class orebody demonstrates both the subtle nature of Archean gold deposits and the potential for finding new mineralization in heavily prospected camps."

Jan 1, 1995

By Mark W. Masson, David B. Stevenson, David W. Broughton, Douglas R. Cruji, Steven E. Parry

"The Amalgamated Kirkland gold deposit is located at Kirkland Lake, Ontario, within the Archean Abitibi Greenstone belt of the Canadian Shield. It lies on a fault or “break”, termed the Cyprus Break, which is a splay off a regional structure termed the Cyprus-Battle Mountain Break. The Cyprus Break merges with the Cyprus – Battle Mountain Break above the -250 m level, as it was not encountered in shallow drilling or surface exploration. These structures lie 1.5 km south of the 727 000 kg (23 million ounce) Kirkland Lake Main Break and 0.5 km north of the 872 000 kg(30 million ounce) Larder Lake Break.The deposit is hosted by alkalic Timiskaming Group volcanic and sedimentary rocks which are overthrust by older Larder Lake Group tholeiitic and komatiitic fows along the Larder Lake Break. Timiskaming syenitic intrusives, similar to the host rocks for the Kirkland Lake Main Break gold deposit, intrude both suites.The Amalgamated Kirkland deposit consists of lode-style gold mineralization which is mainly hosted by altered and pyritized Timiskaming trachytic volcanics which wedge out or thin at depth, between two sedimentary units. The intersection of the Cyprus – Battle Mountain and Cyprus Breaks, in conjunction with the westward plunge of the volcanic wedge, appears to control the westerly plunge of the Amalgamated Kirkland deposit at approximately 50º.Mineralization is characterized by blue-gray brecciated and “wormy” quartz-ankerite veinswhich contain up to 10% fne-grained pyrite and, in decreasing order of abundance, minor galena,chalcopyrite, sphalerite, molybdenite and visible gold. The sulfdes and gold commonly occur alongfractures and wallrock inclusions within the veins. Native gold occurs as fne pinpoints distributed in 1-mm to 5-mm size clusters of up to ten or more grains.The auriferous veins occur within a quartz-ankerite-sericite-pyrite alteration assemblage which is enveloped by a broader zone of ankerite-sericite±hematite±quartz-pyrite alteration up to 60 m wide. This latter assemblage overprints the regional greenschist-facies chlorite-calcite assemblage.The Amalgamated Kirkland property has had a long history of exploration activity beginning with the first discovery of mineralization in 1911 on the Hunton Shaft claim located in the northeast corner of the property. Since that time various prospecting, mapping, trenching, geophysical surveys and diamond drilling programs have concentrated on either carbonate zones along the Larder Lake Break or quartz veins along the northern side of the property in association with complex trachyte flows and syenite dikes.Battle Mountain Canada Inc. located the Cyprus – Battle Mountain Break through a prospecting, trenching and geophysical program in 1989. Drilling by Battle Mountain and Cyprus Canada under the surface showing, coupled with several revisions to the structural interpretation of the Cyprus –Battle Mountain and Cyprus Breaks, resulted in delineation of the Amalgamated Kirkland deposit. Location of an auriferous structure through basic surface exploration within 1 km of a world-class orebody demonstrates both the subtle nature of Archean gold deposits and the potential for finding new mineralization in heavily prospected camps."

Jan 1, 1995

By G. A. Pinsky, Pickard M. K

"IntroductionTWO METHODS of mucking have been used in sinking C shaft, the five-compartment production shaft of the Yellowknife property of Giant Yellowknife Gold Mines, Limited:(a) Band mucking during the original sinking in 1949 and 1950 (l); and(b) Mechanical mucking with the Cryderman shaft mucker during the recent deepening in 1954.This paper briefly describes the recent deepening and compares the performance figures of the two sinking operations.PlanningProduction planning in 1952 showed that it would be advisable to deepen C shaft in 1954 to provide for three new production levels and the installation of an underground crusher. To complete the required shaft work it would be necessary for a shaft crew to deepen the shaft about 500 feet, to partly excavate three level stations and a crusher station, and to cut a station for the loading pocket. Figure 1, a vertical section of the lower part of the shaft, shows the details of the deepening programme.During the planning period, Giant had a rather small supervisory staff and at the same time was experiencing a heavy labour turnover. As it was obvious that production would suffer if the sinking crew were recruited at the mine, it was decided that the merits of contracting-the shaft sinking to an independent contractor should be investigated."

Jan 1, 1955

By H. J. Glass, J. G. L. Bekkers

"In order to determine the feasibility of a hydraulic ore hoisting installation, the optimal operating conditions were calculated for applying such a system at the Detour Lake Mine of Placer Dome Ltd. Next, a financial analysis was conducted in order to estimate the cost per tonne for hydraulic hoisting of the ore. Subsequently, the cost per tonne was compared with the hoisting costs associated with a new borehole hoist. Installing a hydraulic ore hoist at Detour Lake Mine was found to be feasible with considerably lower costs per tonne of ore. The applied research method appears to be very functional and can be used to do similar research for other mining operations. IntroductionThe principle of hydraulic ore hoisting is well known, yet hardly accepted in hard rock mining. Application of the system would result in a smaller diameter shaft requirement and a flexible, easily expandable system. However, underground ore size reduction might be necessary and practical experience with the system is limited. Following recent innovations in the field of pumping hardware, e.g. new GeHo and Siemag Transplan equipment, hydraulic ore hoisting should be seriously considered for certain mining operations. As a case study, a design was made for the development of the newly found QK-Zone at Placer Dome Ltd.’s Detour Lake Mine. Hydraulic ore hoisting has been compared with conventional skip hoisting by establishing the optimal operating conditions and pumping equipment requirements for similar capacities at a selected mining operation. Generally accepted equations for slurry transport were used to predict the variation of pressure and power requirements as a function of hourly production and pipeline diameter. These data are used to select suitable equipment and estimate cost figures in order to make a financial assessment."

Jan 1, 1998

By J. G. Ross

IN the paper entitled Block Caving at the King Mine (1), which was presented at the Annual General Meeting held in April, 1934, at Quebec, it was pointed out that, owing to certain conditions and financial restrictions, it was advisable to provide a temporary shaft. This was raised from the )00-ft. level to the bottom of the pit, and a 45-degree incline track was constructed up the face of the pit to surface. The temporary shaft and incline were within the ore-body, but were to be used only until such time as the new shaft-the subject of this paper-could be sunk and made ready for operation. After a careful study had been made of all available information pertaining to the ore-body, including examination of diamond-drill core records and geological data, a shaft location was selected well outside the ore-body. Further, since the crusher and dryer buildings are located over part of the ore-body, it was necessary to plan the removal of these buildings and to construct a new crushing and drying plant. This, and the new shaft, must operate in conjunction with the present mill and rock storage bin, which would continue robe used as formerly. No part of this programme, with the exception of drifting toward the shaft site, was started prior to 1937. More than usual detail on technical features is given in this paper in the hope that some parts of it may be of assistance to other members of the Institute who have to undertake somewhat similar work. The engineering and operating staff designed and supervised the work, while at the same time carrying on regular production in four mines at the rate of 12,000 tons of rock mined per day, the output at the King mine being at the rate of 140 tons per hour. No additional engineers were required.

Jan 1, 1939

By Unknown

We are indebted to the Consolidated Mining and Smelting Company of Canada Limited for the several pictures in this issue showing the progress made in new construction at Tadanac and at Bonnington Falls, B.C. Plate No. 1 shows the down-stream side of the No. 1 hydro-electric station of the West Kootenay Power and Light Co. Limited at Bonnington Falls, on the Kootenay river, at which 17,500 k.v.a. will be developed to meet the requirements of the enlarged zinc and lead refineries at Tadanac. The generators, exciters and switch apparatus were supplied by the Canadian General Electric Company and the step-up transformers by the Canadian Westinghouse Company Limited. The plant throughout was designed, manufactured and erected by Canadians. Plate No. 2 shows the casting room of the new lead-plant and plate No. 3 the new tank-room of the electrolytic lead refinery at Tadanac. These additions will increase the capacity of the lead refinery by some 150 tons daily. The extensions also include practically doubling the zinc plant, and the gold and silver refineries. With the exception of the new stack, all designing construction and installation of the various plants is being done by the Company's own employees at Tadanac. Plate No. 4 shows the progress made in the construction of the new reinforced concrete stack at Tadanac. This stack, of 21 feet inside diameter at the top, will be brick lined and when completed will rise 400 feet above its foundations: the tallest of its kind in the world. The construction is in charge of the Rust Engineering Company of Pittsburgh, Pa. Plate No. 5 is a panorama of the Tadanac smelters and refineries. The photograph was taken from the roof of the lead smelter and gives an excellent idea of the size of the plant and its surroundings. Tadanac produces electrolytic lead, zinc and copper and fine gold and silver. During 1924 the company treated 1,333,523 tons of ore and produced: 161,400,- 769 pounds of lead; 92,197,824 pounds of zinc; l,382,750pounds of copper; 4,074,044 ounces of silver, and 26,976 ounces of gold.

Jan 1, 1925

By The Staff

THE property of McKenzie Red Lake Gold Mines, Limited, consists of eleven claims located on McKenzie island in Red lake. The mine is about 4,Y:l miles by water from the Howey townsite on the same lake, and about 95 miles north of Kenora, Ont. (see Figure 4). Mail and express are flown-in daily, winter and summer, from Sioux Lookout, Hudson, Kenora, and Winnipeg. All heavy supplies are freighted-in during the summer over a water route, using four marine railway portages, from Hudson, Ont., a distance of about 180 miles. During the winter, freighting over the same route is clone by tractor if necessary, but costs are three to four rimes the summer rate. Due to these conditions, large inventories of supplies must be kept on hand, varying from a spring minimum of $45,000 to a peak of $110,000 early in November. The average cost of all freight brought in from steel during 1937 was $0.01 per pound.

Jan 1, 1938

By Ray Holmes

This paper describes one approach in our search for greater stope efficiency and lower costs. The uppers technique with wagon drills in cut-and-fill stopes was commenced, on an experimental basis, in our Sudbury mines in 1961. To date, the method has developed into an accept-ed production operation. This technique minimizes the intermittent aspects of the drilling, blasting, mucking and filling operations associated with other cut-and-fill methods. However, studies show that not all cut-and-fill stopes are suitable for uppers, the governing factors being ore width, dip of the orebody, and ground conditions where large areas of unsupported back remain stable for ex-tended periods of time until rockbolting can be accomplished. Introduction F ALCONBRIDGE Nickel Mines Limited operates seven mines within a radius of 30 miles of the city of Sudbury, Ontario. These mines extend in depth from 1,500 to 6,300 ft. The ore consists of brecciated, massive and disseminated sulphides, and the ore minerals consist primarily of pentlandite, pyrrhotite and chalcopyrite. Widths are generally irregular and vary up to 150 ft. The ore dips at between 35 and 90 degrees.

Jan 1, 1965

By F. T. Rabbitts

Introduction When the investigation of radioactive ores began at the Mines Branch about five years ago it was at once evident that improved chemical methods for the determination of uranium were essential. The published methods available were time-consuming and insensitive and were lacking in accuracy and precision. It was desirable to obtain methods which would be rapid, sensitive, and accurate. They should also allow for the possible presence of any interfering elements and should be adaptable to routine analysis by technicians. Chemical methods are necessary to provide standard analysed samples for counting and to check analyses by counter methods. Moreover, counter methods cannot be used, and only chemical methods are suitable, when the sample is not in equilibrium, as with weathered minerals and leach residues. As leaching processes are improved, more sensitive chemical methods are required for the increasingly lower content of uranium in the leached residues. When the leaching process reaches the plant stage, speed of analysis becomes more important, without sacrificing accuracy. The purpose of this paper is to describe briefly .the methods used at the Mines Branch for the chemical analysis of uranium in ores. These methods represent the results of investigations by a number of groups in the United Kingdom, the United States, and Canada.

Jan 1, 1952

By C. E. Dowker

"IntroductionMechanization underground at the Buffalo Ankerite mine in Deloro township, Porcupine district, had reached a high level by 1944, both in equipment available, and in the use of this equipment, for all stoping operations. Power feed leyners and the latest type of stopers for drilling, slushers for moving ore and fill, and tugger hoists for all servicing, did much to halt rising stope costs, and in some cases decreased them. On the other hand, little beyond the use of mucking machines and power feed leyners had been adopted in the effort to reduce level development costs, or to increase the advance per man-shift.Faced with ever increasing level development costs, caused by rising prices of equipment and supplies, coupled with increasing wage demands for less physical effort, it was realized that more mechanization of development work was essential. The objectives of such further mechanization were:(1) Decreased development costs(2) Increased footage per man-shift(3) Less physical effort by development crews, with greater take-home pay (4) A more satisfied and stable labour force"

Jan 1, 1950

By M. Buarzaiga

High-pressure acid leaching (HPAL) of nickel laterite ores typically extracts 95% of the nickel and 91% of the cobalt. Impurity elements in the feed, such as iron, aluminium and chromium, also dissolve and can be detrimental to downstream processes. Rejection of impurities within the autoclave is highly desirable. Aluminium and iron hydrolyze, and then precipitate in the autoclave leaving only small amounts that are subsequently removed by precipitation in a neutralization step. The concentration of dissolved chromium can range from 200 to 2000 ppm, depending on the feed composition. Chromium in the liquid phase, usually in the hexavalent state, introduces many problems and can limit refining options. For example, chromium poisons the organics in solvent extraction making SX an expensive option. Also, hexavalent chromium must be converted to the trivalent state before it can be precipitated along with iron and aluminium. Bench-scale work confirmed that mixing small amounts of carbon-base additives, such as coke, with the autoclave feed significantly reduced chromium concentration in the autoclave discharge without any detrimental effects on paymetals recoveries and selectivity.

Jan 1, 2004

By J. Visman

"The Compound Water Cyclone is a concentrator for the wet processing, in bulk, of finely divided materials such as slack coal, fine ores and mineral sands. It was originally developed by the Fuels and Mining Practice Division of the Mines Branch, Department of Mmes and Technical Surveys, Ottawa, for the cleaning of friable slack coals and slurries.Since its introduction in the coal industry in 1962, its application to other materials has also been studied, with special emphasis on simplicity of operation and low over-all cost per ton of finished product .In this paper, a description is given of commercial two-stage units presently available for the processing of granular materials, including wastes a1:1d other low-grade products. A pneumatic control system is used for operating the cyclone under back pressure .and for automatic cut-point adjustment. An account is given of results obtained on coal mineral sands and ores in the Wes tern Regional Laboratory of the Department of Mines and Technical Surveys. Results of several industrial applications are discussed."

Jan 1, 1966