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By Breno Totti Maia

This work was a continuous and multidisciplinary development. Through studies of the blowing process and its parameters results, evolutions, improvements and adjustments were made on the lance’s hot face with Slagless® technology, as well in the process parameters and mitigating actions of the projection of materials out of the converter. The main results are the increase in the nozzle’s life with a “record mark” of 1785 heats, and water leakage occurrence in the cartridge decreased considerably reaching the mark of one year without any occurrence.

Oct 30, 2017

By Gustavo Borges Tiboni

The erosive wear caused by the impact of solid particles against a surface is a tribological phenomenon present in many segments of the industry, such as transportation, aerospace, mining, power generation, among others. The most usual method to set the wear rate is by measuring the mass loss of the material. In order to apply one technique with potential to determine the rate of erosion wear, this study developed a dedicated equipment and conducted preliminary erosion tests monitored by non-destructive testing known as acoustic emission technique (AE). This can be defined as a technique able to detect mechanical waves generated by the release of elastic energy accumulated in the material. Erosion tests were performed in order to evaluate the ability of equipment to collect data from AE and to correlate these data with the wear of the samples. Samples of low carbon steel eroded by the impact of angular aluminum oxide particles suspended in air at three different velocities: 45, 57 and 67 m/s. The impact angle between the particles and the sample was set at 30 degrees and the test temperature at approximately 20°C. The wear rate has changed with the velocity in accordance with the kinetic energy of the particles and the AE parameter RMS showed sensitivity to the variation of particle impact velocity and to the wear of the sample eroded. The rate of AE signals collected over time correlated with the flow of particles striking the sample, and with the parameters of energy, rise time and duration of the signal.

Jul 31, 2018

By Bernardo Siqueira

This paper presents a unique stirred milling technology, Outotec HIGmill™, a modern, flexible and energy efficient grinding solution for fine and ultra fine grinding being tested in an industrial scale level. The test was performed at an iron ore pellet producing plant in Sweden (for confidentiality reasons, it will be referred to only as “the client”) where a pilot HIGmill™ unit (HIG25) was installed parallel to a conventional regrind circuit to compare its performance to the existing ball mill. By using a continuous test run procedure and evaluating the parameters of F80, P80, mill shaft rotation speed and power drawn it was determined its grinding capabilities, operational flexibility and energy efficiency. Outotec HIGmill™ outperformed the existing ball mill in the plant proving its capabilities to grinding finer, with steeper particle size distribution (PSD) and much higher energy efficiency. The tests performed showed that, with further refining of its operation, it is capable of consistently deliver the required PSD with up to 30% higher grinding efficiency.

Aug 16, 2017

By Roman Vaynshteyn

In places where Blast Furnaces are usually located, climatic factors may be unfavorable. Raw materials may be exposed to e.g. rain during transport/storage, bringing moisture into the process with consequences for stability and hot metal cost. This paper describes a technology for drying and pre-heating pellets and coke in the stockhouse. It does not require additional handling or logistical equipment and does not introduce extra transfer steps and degradation. Not only can moisture content be reduced, it can be controlled to a stable level by the operator.

Aug 16, 2017

By Rodrigo Sanchotene Silva

Currently the industries of paint have directed their efforts on cleaner production of products that provide effective performance in corrosion protection of metallic materials. This work search introduce a new alternative of organic coating, without the presence of hazardous metals and replace equipments commercials used method of anodic protection for protection of oxidized metals. From this it, was produced Smart Paint (SP), consisting of Paint Acrylic Commercial (PAC) mixed the 1 % of binder, compound by the conducting polymer, Polyaniline Emeraldine Base (PAni EB) and plasticizer 4-chloro-3-methylphenol. The SP and PAC were applied to plates of carbon steel AISI 1010, with the aid of dip coat technique and then were subjected to drying for 48 h. The SP was characterized by thermals and physicochemical analyzes in order to verify possible changes in chemical properties of the ink produced, beyond perform electrochemical tests of Open Circuit Potential and Electrochemical Impedance Spectroscopy, employing equipment Potentiostat/Galvanostat Autolab PGSTAT302 Ecochemie, and aqueous 2 mol.L-1 of H2SO4. The results obtained allow us to state that the plasticizer does not alter the electrochemical properties of PAni and application of binder PAni EB to PAC does not alter the physicochemical properties of commercial coating. The binder PAni EB adds to PAC the capacity to induce the formation or maintenance of protective oxides in oxidizable metals submitted to harsh environments, method known as anodic corrosion protection.

Aug 8, 2018

By Felipe Beluche Lima, Caio Augusto Silva Santos

Brazil is the largest producer of crude steel in the Americas by BOF process and many challenges come along with the increasing market demand. In the BOF, a tubular wall hood structure has been showing premature failures related to the overlay welded tube technology placed in the hood wall. The main root causes were: thermal fatigue at 1800°C, hot spot formation, high heat-affected zone (HAZ) leading to susceptibility of stress cracking, carburizing corrosion and superficial wearing. Based on that, co-extruded tube technology (named composite tube by Sandvik) was the alternative chosen to enhance hood performance without compromising BOF process. In order to rises safety and productivity, composite tube has 100% metallurgical bond assuring stable expansion, high heat exchange efficiency, better corrosion resistance and less rough surface finishing. It was highly suggested to many others mills due to similar and already existing reported cases.

Oct 1, 2019

By Hiroshi Ichikawa

In 2013, Nippon Steel & Sumikin Engineering Co., Ltd. (hereafter referred to as NSENGI), Tenova HYL and Danieli have entered into an agreement to combine ENERGION DR technology into blast furnace technology and/or with syngas technologies. This new alliance will allow the three companies to combine research and development activities with their respective expertise in ENERGIRON DR technology, Blast Furnace technology and Syngas (by-pro gas and coal gasification) technology, with the ultimate objective to develop breakthrough iron making technologies and create such EPC projects. This paper introduces the concepts and the features of our breakthrough technologies of combining of ENERGIRON DR technology, Blast Furnace technology and Syngas technology.

Aug 16, 2017

By Charles Sóstenes Assunção

A mathematical model of heat transfer and solidification for a continuous casting of round billets was developed. The water flux density of the secondary cooling zone was experimentally measured, using an apparatus in industrial scale with two types of nozzles, flat jet and full cone jet. The profiles of water distribution were applied on the mathematical model. The results showed that the water distribution is not uniform in both longitudinal and angular directions owing to the unevenness of the spray and to the curvature effect of the round billet. This non-uniformity causes important variation of the heat transfer coefficients and superficial temperature of the billet, especially in the first cooling zones, where the temperature is higher. The mathematical model was used to simulate a change of nozzle type in the first cooling zone. The results showed that the heat flux and superficial temperature variations were reduced with a full cone jet nozzle in comparison with the flat jet nozzles.

Aug 16, 2017

By Elham Kordzadeh

As the world’s reserves of coarse and high-grade iron ores continue to shrink, beneficiation is becoming increasingly important. The resulting concentrates cannot be used directly as feedstock for iron making, but require an additional agglomeration step. Pelletizing is preferred, because the uniform chemical, physical, and metallurgical characteristics of pellets make them a more desirable feed for the iron making processes. The heat hardening or induration of pellets is typically done in shaft furnaces, grate-kiln systems or on straight grates. Rotary kilns were originally developed in the late 19th century for Portland cement production [1]. The main development work for the successful adaptation of the process to the thermal treatment (induration) of green balls from iron ore was performed by Allis Chalmers in Milwaukee, Wisconsin, USA in the 1960’s [2].The straight grate process, which was first used in 1955 at Silver Bay, Minnesota, was a dedicated development with the aim to pelletize and indurate magnetite (taconite) concentrate [2]. There are various important technical and economical distinctions between the two pelletizing technologies. The most important differences include that a grate-kiln has three distinct pieces of equipment, a preheat grate, a rotary kiln and an annular cooler, whereas in the case of a straight grate, the entire indurating process is done on one piece of equipment only. In addition, both technological solutions have differences in their recuperation systems, direction of air flow in drying, number of burners, form of pellet movement, etc., which cause differences in raw material suitability, process control, economical aspects, plant operation and product pellet quality.

Oct 30, 2017

By Glaydson Simões dos Reisr

Micropore organosilicas (MOs) were synthesized using methyl-phenyl-polysiloxane as precursor. The MOs were characterized using several analytical and functional techniques. The materials were assigned as micropores materials, with specific surface area up to 642 m2 g-1 and yield up to 72.55%. The adsorbents have hydrophobic surfaces and were used for removal of diclofenac from aqueous solutions. The adsorption kinetic and isothermal data were well described by the general order and Sips models, respectively. Diclofenac exhibited a better affinity than NM and the mechanism of adsorption suggested that hydrophobic groups play a key role in the adsorption process.

Aug 17, 2017

By Johan Richaud

Achieving high surface quality steel in the continuous casting process requires optimal mould level control. The design of the casting channel from the tundish to the mould is crucial to prevent formation of undesired instabilities or biased flows that can cause level fluctuation. With the aid of CFD and with physical water models, the geometry of the stopper nose and the nozzle seat have been studied and optimized to improve the overall mould flow stability. A special stopper nose; Ripple Stopper (RST), has been developed that reduces the formation of large and unwanted eddies in the liquid steel that destabilize the port exiting jets. Instead, the RST produces a fast release of turbulence in the form of a large number of small eddies. The large sudden fluctuations in the mould level are reduced, which in turn reduces the occurrence of surface defects. An additional benefit is derived from the local pressure around the stopper nose region being greater which reduces the refractory erosion. For a tundish gate type flow regulation, a new design encompasses an offset in the Tundish Well Nozzle (TWN) that realigns the flow and reduces the bias flow that is common to tundish gate regulation. The steel recirculation regions below the throttling gate are decreased reducing the risk of oxide depositions. The RST and the Offset bore casting channel have been applied successfully leading to a superior flow control performance between the tundish and the mould.

Jul 30, 2018

By Filippo Verlezza

The 3-roll technology is a recognized process applied to SBQ production. The main aim of this paper is to show the latest developments on this technology including other equipment´s that also contributes for a better performance on SBQ coils production.

Jul 30, 2018

By Vitor Orlando Ferreira

The efficiency of an apparatus which uses a forced lubrication system, as well as the useful life of its components, is strongly related to the degree of contamination of lubricating oil. The presence of contaminants and the degradation of the oil itself cause it to release substances that fouling of the wall of the pipes. The cleaning and dialysis of the oil pipes, besides prolonging the life of the lubricant reduces wear of the components. There are several methods of cleaning in pipes, the problem is that some have abrasive characteristics, which could damage some types pipes. Among the non-abrasive methods stand the Flushing and Air scouring. Flushing uses the lubricating oil which circulates in temperatures alternating and high speeds, for generating turbulence to perform washing. The Air scouring method uses oil and filtered compressed air, injected into pipe, to generating higher flow, causing the power supply unit with fluid can work with lower power consumption and higher speeds, removing fouling of the pipe. The objective of this research is to evaluate the Reynolds number to correlate with the efficiency of cleaning the pipe. The method applied was the Air scouring and it was verified that the qualitative effects may occur when compared to Flushing. After testing, it was found that the chosen method brings significant changes in flow, and this flow regime varies considerably increasing the Reynolds number.

Jul 31, 2018

By Dr. Steven G. Jansto

The market demand for reduced fuel consumption and CO2 emissions in the automotive, energy and construction sectors have further increased the demand for new and advanced higher quality microalloyed grades produced via TMCP. The technological integration of the process and physical metallurgical advancements of value-added niobium (Nb) microalloyed thermo-mechanical controlled process (TMCP) steels continue to be developed and is an important element for these more demanding end user requirements and cost-effective steel production. The reheat furnace process step has a profound effect on the TMCP performance, final hot rolled steel quality and mechanical property consistency during the production of hot rolled steels. The uniformity of heating applied across the entire width, thickness and length of the slab or billet is essential in the successful achievement of consistent customer properties regardless of the chemistry. The resultant ferrite grain size in the final hot rolled product is significantly governed by the initial prior austenite grain size. However, the transition from laboratory melted and TMCP hot rolled heats to the production scale is often quite challenging. Aberrations in the reheating process step at the industrial furnace are often the root cause of mechanical property quality issues. These combustion process metallurgy parameters connect directly to the resultant TMCP product quality and is defined as Combustion Metallurgy

Oct 1, 2019

By Douglas Glenn Stalheim

Hot strip structural steel coil used in construction, engineering, transport, structural applications and other applications are widely used in yield strengths from 300 – 700 MPa. However, structural design engineers are now not only requiring various strength levels but also other mechanical properties, primarily good formability, toughness and weldability. To produce a balanced approach to a cost effective structural steel, hot strip coil requires an understanding of utilization of an optimized alloy composition designed for the layout/equipment capabilities of a given hot strip mill to produce the desired metallurgy for optimum mechanical property performance. The term “cost effective” does not just focus on alloy design, but also ease of overall processing from steelmaking, casting, rolling and cooling, stable mechanical properties with a statistically normal distribution, no downgrades/rejections and a product that the end user recognizes as being superior to others. The desired metallurgy is simply understanding what will be the optimum microstructure and cross sectional grain size/distribution needed to meet the mechanical property requirements. This paper is a follow up paper that previously described optimum base alloy designs along with steelmaking/casting processing considerations and will focus on proper reheating, rolling and cooling metallurgy/processing strategies to produce quality cost effective hot strip structural steel coil.

Aug 17, 2017

By Nicolás Ariel Zabala

During the make-up and break-out of the connections, threaded joints are exposed to intense mechanical and tribological solicitations. The connection performance is influenced by its geometry, material properties, surface treatments and thread compound. The aim of this work is to evaluate and characterize the tribological behavior of different thread compounds applied on manganese phosphated carbon steel under low speed and high pressure sliding contact. Four thread compounds were evaluated: one containing lead, zinc and graphite; other lead-free, containing copper and finally, the last two lead-free and containing non-metallic solids. The tribological behavior was analyzed by a block-on-ring tribotest. During the test, load varied linearly between 250 N and 7000 N; loading and unloading lasted 14 sec and were performed in opposite directions of rotation to simulate the make-up and break-out operations. Friction force and load as a function of time were registered. Upon completion of the test, wear surfaces were analyzed by SEM, optical microscopy and energy dispersive spectroscopy. The obtained results show that the lead and zinc containing thread compound displayed the best behavior, showing a wear reduction of approximately 20%. These results are in line with previously known oilfield experience. Average COF values around 0.15 were measured and no significant differences between dopes were observed; indicating that the wear behavior was influenced by the additive package.

Jul 31, 2018

By Maurizio Massimo

Danieli developed the “3Q” suite of process control technologies to address three critical principles: delivering the highest product Quality, in the required Quantity, with Quickness of response required for today’s casting machines. Ever increasing market demands for productivity and slab quality necessitate the latest advances/improvements in equipment design, process technology, and control software for all types of slab casters, and Danieli boasts a unique experience that extends from ultra high-speed thin slab casters to extra high-thickness conventional slab casters. The “3Q” system is monitored and controlled by a unique, intelligent HMI incorporating. Touch screen technology and Operator Assistant tablets. Operator Assistant is a tablet based system that guides the operator through the plant process, so that in the event of a process change or an alarm the operator is automatically presented with the choice of possible solutions / actions. The comprehensive range of technological packages cover all aspects of caster design and automation control, from feeding of liquid steel into the tundish to the final slab leaving the caster.

Aug 17, 2017

By Edmar de Souza Silva, Antonio Augusto Gorni, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Controlled rolling followed by accelerated cooling, known worldwide as TMCP, aims to increase mechanical properties without toughness deterioration. The process principle is to promote the plate cooling with water jets along the range of the austenite transformation temperatures. The accelerated cooling process is only fully effective when controlled in an integrated manner, as it alone cannot ensure significant improvements in the final properties of steels. Plate surface quality depends on some parameters that must be controlled before the start of the plate accelerated cooling. Good flatness is essential to avoid irregular water accumulations during cooling. After the reheating process, the slab should have uniform temperature, uniform austenitic grain size and easily removable scale. The slab thermal and microstructural heterogeneities are inherited by the rolled plate and tend to increase further during the accelerated cooling. This results in flatness problems, high level of internal stresses and mechanical property variations. The descaling strategy is an extremely important factor and must be determined with great caution. It is important that scale thickness and distribution is uniform to ensure homogeneous cooling over the entire plate surface. Otherwise, there will be an uneven temperature distribution, which can cause serious problems of flatness, surface quality and mechanical properties.

Oct 1, 2019

By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017